Skip to main content
Log in

Extraction of ferulic acid from sugar beet pulp by alkaline hydrolysis and organic solvent methods

  • Original Paper
  • Published:
Journal of Food Measurement and Characterization Aims and scope Submit manuscript

Abstract

Extraction of ferulic acid from sugar beet pulp was carried out using three extraction solvents, sodium hydroxide (0.5, 1, 2 M), methanol and their mixture (alkaline methanolic solvent). The Ferulic acid extracted by each solvent was identified and quantified by HPLC method and the effects of solvent type, concentration and reaction time on ferulic acid solubilisation were assessed. There were differences in the contents of products extracted in the experiment conditions. The minimum amount of ferulic acid was obtained from methanolic extract while the highest concentrations (957.4 mg/L ferulic acid) were obtained employing the highest NaOH concentration (2 M), and reaction time (12 h), so phenolic compounds are better released with alkaline hydrolysis than in methanol conditions. Finally a simple procedure for the purification of ferulic acid from the alkaline extracts is presented and evaluated by FT-IR spectrum.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2

Similar content being viewed by others

References

  1. C.D. Stalikas, J. Sep. Sci. 30, 3268–3295 (2007). doi:10.1002/jssc.200700261

    Article  CAS  Google Scholar 

  2. D.R. Rose, G.E. George, S.X. Liu. J. Sci. Food. Agr. 90, 519–524 (2010)

    Google Scholar 

  3. H.Z. Zhao, M.H. Moghadasian, Food Chem. 109, 691–702 (2008). doi:10.1016/j.foodchem.2008.02.039

    Article  CAS  Google Scholar 

  4. J.M. Cruz, J.M. Dominguez, H. Domınguez, J.C. Parajo, J. Agr. Food. Chem 49, 2459–2464 (2001). doi:10.1021/jf001237h

    Article  CAS  Google Scholar 

  5. J. Gonzalez, J.M. Cru, H. Dominguez, J.C. Parajo, Food Chem. 84, 503–510 (2004). doi:10.1016/S0308-8146(03)00208-5

    Article  CAS  Google Scholar 

  6. C.B. Faulds, B. Bartolome, G. Williamson, Ind. Crops Prod. 6, 367–374 (1997)

    Article  CAS  Google Scholar 

  7. P. Jankovska, J. Copikova, A. Sinitsya, Czech. J. Food. Sci. 19, 4 (2001)

    Google Scholar 

  8. B.A. Acosta-Estrada, J.A. Gutierrez-Uribe, S.O. Serna-Saldivar, Food Chem 152, 46–55 (2014). doi:10.1016/j.foodchem.2013.11.093

    Article  CAS  Google Scholar 

  9. D. Couteau, P. Mathaly, Ind. Crops Prod. 6, 237–252 (1997)

    Article  CAS  Google Scholar 

  10. G.H. Lu, K. Chan, K. Leung, C.L. Chan, Z.H. Zhao, Z.H. Jiang, J. Chromatogr. A 1068, 209–219 (2005)

    Article  CAS  Google Scholar 

  11. N.B. Dar, S. Sharma, Am. J. Food Tech. 6, 12 (2011)

    Article  CAS  Google Scholar 

  12. M. Bunzel, J. Ralph, C. Funk, H. Steinhart, Eur. Food Res. Technol. 217, 128–133 (2003). doi:10.1007/s00217-003-0709-0

    Article  CAS  Google Scholar 

  13. L. Zheng, Pu Zheng, Z. Sun, Y. Bai, J. Wang, X. Guo, Bioresour. Technol. 98, 1115–1119 (2007). doi:10.1016/j.biortech.2006.03.028

    Article  CAS  Google Scholar 

  14. B. Max, A. M. Torrado, A. B. Moldes, A. Converti, J.M. Domingueza, Biochem. Eng. J., 43 (2009). doi:10.1016/j.indcrop.2006.11.001

  15. H. Barberousse, O. Olivie Roiseux, C. Robert, M. Paquot, C. Deroanne, C. Blecker, J. Sci. Food Agric. 88, 1494–1511 (2008). doi:10.1002/jsfa.3242

    Article  CAS  Google Scholar 

  16. A.U. Buranov, G. Mazza, Food Chem. 115, 1542–1548 (2009). doi:10.1016/j.foodchem.2009.01.059

    Article  CAS  Google Scholar 

  17. L. Kunst, A.L. Samuels, Prog. Lipid Res. 42, 51–80 (2003)

    Article  CAS  Google Scholar 

  18. D.S. Oufnac, Z. Xu, T. Sun, C. Sabliov, W. Prinyawiwatkul, J.S. Godber, Cereal Chem. 84, 2 (2007)

    Article  CAS  Google Scholar 

  19. P. Torre, B. Aliakbarian, B. Rivas, J.M. Dominguez, A. Attilio Converti, Biochem. Eng. J. 40, 500–506 (2008). doi:10.1016/j.bej.2008.02.005

    Article  CAS  Google Scholar 

  20. M.S. Noor Hasyierah, M.D. Mohamed Zulkali, A. Dachyar, A.M. Syarhabil, K.I. Ku Syahidah, Ind. Crops. Prod. 34, 1635–1640 (2011). doi:10.1016/j.indcrop.2011.06.010

    Article  CAS  Google Scholar 

  21. J.L. Bauer, B. Harbaum-Piayda, K. Schwarz, LWT- Food Sci. Technol. 47, 246–254 (2012). doi:10.1016/j.lwt.2012.01.012

    Article  CAS  Google Scholar 

  22. Y. Yongyue Sun, W. Wang, J. Chin. Inst. Chem. Eng, 39, 653–656 (2008). doi:10.1016/j.jcice.2008.05.012

    Article  CAS  Google Scholar 

  23. K.W. Waldron, N. Annie, L.P. Mary, J.P Adrian, J. Sci. Food Agric. 74, 221–228 (1997)

    Article  CAS  Google Scholar 

  24. M.S. Robert, X.W. Francis, Text Book of Spectrometric Identification of Organic Compounds (Wiley, New York, 1998)

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Masoud Honarvar.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Aarabi, A., Mizani, M., Honarvar, M. et al. Extraction of ferulic acid from sugar beet pulp by alkaline hydrolysis and organic solvent methods. Food Measure 10, 42–47 (2016). https://doi.org/10.1007/s11694-015-9274-z

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11694-015-9274-z

Keywords

Navigation