Abstract
This study takes a benchmarking approach to the processing of 17-4 PH using selective laser melting by having two facilities that use their own best practices to process materials. Hot isostatic pressing (HIP) is used by both facilities as part of the thermomechanical processing following printing to explore whether it can improve the consistency of mechanical properties. Results revealed that HIP reduced average porosity of 17-4 parts and that the yield strength of parts following solutionization and aging met wrought material property targets. Strain to failure of one of the facilities parts was less than 5% compared to greater than 9% for the other facility. Inspection of failure surfaces revealed this discrepancy was caused by pores (2-4% area fraction) on the failure surfaces of the low ductility parts. These results are viewed with respect to the intended application of this material as a structural element for wind tunnel testing.
Similar content being viewed by others
Notes
Does not constitute or imply the endorsement, recommendation, or favoring of the U.S. Government.
References
D. Cahill, F. Steinle, and S. Richardson, Evaluation of Wind Tunnel Internal Force Balances from Multiple Vendors, in Aerospace sciences meetings (American Institute of Aeronautics and Astronautics, 2004). https://doi.org/10.2514/6.2004-1292
L.E. Murr, E. Martinez, J. Hernandez, S. Collins, K.N. Amato, S.M. Gaytan, and P.W. Shindo, Microstructures and Properties of 17-4 ph Stainless Steel Fabricated by Selective Laser Melting, J. Mater. Res. Technol., 2012, 1(3), p 167–177. https://doi.org/10.1016/S2238-7854(12)70029-7
H.K. Rafi, D. Pal, N. Patil, T.L. Starr, and B.E. Stucker, Microstructure and Mechanical Behavior of 17-4 Precipitation Hardenable Steel Processed by Selective Laser Melting, J. Mater. Eng. Perform., 2014, 23(12), p 4421–4428. https://doi.org/10.1007/s11665-014-1226-y
B.C. Salzbrenner, J.M. Rodelas, J.D. Madison, B.H. Jared, L.P. Swiler, Y.-L. Shen, and B.L. Boyce, High-throughput Stochastic Tensile Performance of Additively Manufactured Stainless Steel, J. Mater. Process. Technol., 2017, 241, p 1–12. https://doi.org/10.1016/j.jmatprotec.2016.10.023
B. AlMangour and J.-M. Yang, Improving the Surface Quality and Mechanical Properties by Shot-Peening of 17-4 Stainless Steel Fabricated by Additive Manufacturing, Mater. Des., 2016, 110, p 914–924. https://doi.org/10.1016/j.matdes.2016.08.037
B. AlMangour and J.-M. Yang, Integration of Heat Treatment with Shot Peening of 17-4 Stainless Steel Fabricated by Direct Metal Laser Sintering, JOM, 2017, 69(11), p 2309–2313. https://doi.org/10.1007/s11837-017-2538-9
B. Farber, K.A. Small, C. Allen, R.J. Causton, A. Nichols, J. Simbolick, and M.L. Taheri, Correlation of Mechanical Properties to Microstructure in Inconel 718 Fabricated by Direct Metal Laser Sintering, Mater. Sci. Eng. A, 2018, 712, p 539–547. https://doi.org/10.1016/j.msea.2017.11.125
M. Aydinöz, F. Brenne, M. Schaper, C. Schaak, W. Tillmann, J. Nellesen, and T. Niendorf, On the Microstructural and Mechanical Properties of Post-treated Additively Manufactured Inconel 718 Superalloy Under Quasi-Static and Cyclic Loading, Mater. Sci. Eng. A, 2016, 669, p 246–258. https://doi.org/10.1016/j.msea.2016.05.089
A. Kreitcberg, V. Brailovski, and S. Turenne, Effect of Heat Treatment and Hot Isostatic Pressing on the Microstructure and Mechanical Properties of Inconel 625 Alloy Processed by Laser Powder Bed Fusion, Mater. Sci. Eng. A, 2017, 689, p 1–10. https://doi.org/10.1016/j.msea.2017.02.038
H.V. Atkinson and S. Davies, Fundamental Aspects of Hot Isostatic Pressing: An Overview, Metall. Mater. Trans. A, 2000, 31(12), p 2981–3000. https://doi.org/10.1007/s11661-000-0078-2
S. Cheruvathur, E.A. Lass, and C.E. Campbell, Additive Manufacturing of 17-4 ph Stainless Steel: Post-processing Heat Treatment to Achieve Uniform Reproducible Microstructure, JOM, 2016, 68(3), p 930–942. https://doi.org/10.1007/s11837-015-1754-4
T. LeBrun, T. Nakamoto, K. Horikawa, and H. Kobayashi, Effect of Retained Austenite on Subsequent Thermal Processing and Resultant Mechanical Properties of Selective Laser Melted 17-4 ph Stainless Steel, Mater. Des., 2015, 81, p 44–53. https://doi.org/10.1016/j.matdes.2015.05.026
B.L. Bramfitt and A.O. Benscoter, Metallographer’s Guide: Practices and Procedures for Irons and Steels, ASM International, Materials Park, 2002
M. Murayama, K. Hono, and Y. Katayama, Microstructural Evolution in a 17-4 ph Stainless Steel After Aging at 400 C, Metall. Mater. Trans. A, 1999, 30(2), p 345–353. https://doi.org/10.1007/s11661-999-0323-2
B.L. Boyce, B.C. Salzbrenner, J.M. Rodelas, L.P. Swiler, J.D. Madison, B.H. Jared, and Y.-L. Shen, Extreme-Value Statistics Reveal Rare Failure-Critical Defects in Additive Manufacturing, Adv. Eng. Mater., 2017, 19(8), p 1700102. https://doi.org/10.1002/adem.201700102
Y. Sun, R.J. Hebert, and M. Aindow, Non-metallic Inclusions in 17-4 ph Stainless Steel Parts Produced by Selective Laser Melting, Mater. Des., 2018, 140, p 153–162. https://doi.org/10.1016/j.matdes.2017.11.063
Z. Hu, H. Zhu, H. Zhang, and X. Zeng, Experimental Investigation on Selective Laser Melting of 17-4 ph Stainless Steel, Opt. Laser Technol., 2017, 87, p 17–25. https://doi.org/10.1016/j.optlastec.2016.07.012
L. Carneiro, B. Jalalahmadi, A. Ashtekar, and Y. Jiang, Cyclic Deformation and Fatigue Behavior of Additively Manufactured 17-4 ph Stainless Steel, Int. J. Fatigue, 2019, 123, p 22–30. https://doi.org/10.1016/j.ijfatigue.2019.02.006
A. Yadollahi, N. Shamsaei, S.M. Thompson, A. Elwany, and L. Bian, Effects of Building Orientation and Heat Treatment on Fatigue Behavior of Selective Laser Melted 17-4 ph Stainless Steel, Int. J. Fatigue, 2017, 94, p 218–235. https://doi.org/10.1016/j.ijfatigue.2016.03.014
D.F. Susan, T.B. Crenshaw, and J.S. Gearhart, The Effects of Casting Porosity on the Tensile Behavior of Investment Cast 17-4 ph Stainless Steel, J. Mater. Eng. Perform., 2015, 24(8), p 2917–2924. https://doi.org/10.1007/s11665-015-1594-y
Acknowledgments
This work was supported by NASA’s Aerosciences Evaluation and Test Capabilities (AETC) Project. Thanks to Clara Mock at the Army Research Laboratory for performing the x-ray computed tomography work.
Author information
Authors and Affiliations
Corresponding author
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Burns, D.E., Kudzal, A., McWilliams, B. et al. Investigating Additively Manufactured 17-4 PH for Structural Applications. J. of Materi Eng and Perform 28, 4943–4951 (2019). https://doi.org/10.1007/s11665-019-04206-9
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-019-04206-9