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Synthesis, thermal behavior and FTIR study of some hydroxyapatite precursors doped with two metals

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Abstract

Hydroxyapatite is intensely studied not only for its bone repair applications but for many other applications, too. In this paper, hydroxyapatite obtained from calcium acetate and dimethyl phosphate was doped with two different metals, one being zirconium and the other one was chosen between M(II) and M(III) metals, under ultrasonication conditions. These types of compounds are not mentioned in the literature. The influence of the doped metals on the thermal behavior of hydroxyapatite precursors was studied using thermal analysis, UATR–FTIR spectrometry, energy dispersive X-ray analysis and ICPOS analysis.

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Authors and Affiliations

  1. Research Center for Thermal Analysis in Environmental Problems, West University of Timisoara, Pestalozzi Street 16, Timişoara, Romania

    Alexandru Pahomi, Gabriela Vlase, Nicolae Doca & Titus Vlase

  2. Faculty of Chemistry, Biology, Geography, West University of Timisoara, Pestalozzi Street 16, Timişoara, Romania

    Alexandra Toma & Gheorghe Ilia

  3. Institute of Chemistry “Coriolan Dragulescu” Timisoara, 24 Mihai Viteazu Bvd, 300224, Timisoara, Romania

    Gheorghe Ilia

  4. Faculty of Medicine, Pharmacy and Dentistry, West University “Vasile Goldis” Arad, Rebreanu Street 86, 310414, Arad, Romania

    Violeta Turcuş

  5. National Institute of Economic Research “Costin C. Kiritescu”, Montana EC-MONT, Romanian Academy, Vatra Dornei, Romania

    Violeta Turcuş

Authors
  1. Alexandru Pahomi
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  2. Gabriela Vlase
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  3. Alexandra Toma
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  4. Gheorghe Ilia
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  5. Violeta Turcuş
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  6. Nicolae Doca
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  7. Titus Vlase
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Correspondence to Gheorghe Ilia or Titus Vlase.

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Pahomi, A., Vlase, G., Toma, A. et al. Synthesis, thermal behavior and FTIR study of some hydroxyapatite precursors doped with two metals. J Therm Anal Calorim 138, 2175–2183 (2019). https://doi.org/10.1007/s10973-019-08550-9

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  • DOI: https://doi.org/10.1007/s10973-019-08550-9

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