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Thermal stability and sintering behaviour of hydroxyapatite nanopowders

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Abstract

Hydroxyapatite (HA) nanopowders were synthesised following two different precipitation routes: (a) from calcium nitrate and diammonium hydrogen phosphate solutions and (b) from calcium hydroxide suspension and phosphoric acid solution. The influence of precipitation process, concentration, and synthesis temperature on HA particle size and morphology, phase composition, thermal stability, and sintering behaviour was investigated by means of: thermogravimetry and differential thermal analysis (TG-DTA), induced coupled plasma–atomic emission spectroscopy (ICP-AES), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), electron microscopy (TEM, SEM) and dilatometry.

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Authors and Affiliations

  1. Dept. of Chemical Sciences and Technologies, INSTM Research Unit Tor Vergata, University of Rome Tor Vergata, Roma, Italy, 00133, Via della Ricerca Scientifica 1

    Alessandra Bianco, Ilaria Cacciotti & G. Gusmano

  2. Dept. of Materials Science and Chemical Engineering, INSTM Research Unit Politecnico di Torino: LINCE Lab, Politecnico of Torino, Torino, Italy, 10129, Corso Duca degli Abruzzi 24

    Mariangela Lombardi & Laura Montanaro

Authors
  1. Alessandra Bianco
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  2. Ilaria Cacciotti
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  3. Mariangela Lombardi
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  4. Laura Montanaro
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  5. G. Gusmano
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Correspondence to Alessandra Bianco.

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Bianco, A., Cacciotti, I., Lombardi, M. et al. Thermal stability and sintering behaviour of hydroxyapatite nanopowders. J Therm Anal Calorim 88, 237–243 (2007). https://doi.org/10.1007/s10973-006-8011-6

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  • DOI: https://doi.org/10.1007/s10973-006-8011-6

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