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Composite magnetic sorbents based on magnetic Fe3O4 coated by Zn and Al layered double hydroxide for U(VI) removal from aqueous media

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Abstract

Composite sorbents based on Fe3O4 and Zn-Al-LDH with different weight ratios of magnetic and sorbing phases were obtained by the precipitation method. The optimal weight ratio of Zn/Fe was 16, which resulted in a 62% increase in hydromechanical strength. The maximum sorption exchange capacity towards U(VI) was 268.65 ± 22.22 mg/g. The efficiency of U(VI) adsorption was not affected by the presence of Cl−, SO42−, NO3− and Na+, Ca2+. The distribution coefficient in a groundwater model solution was Kd(U(VI) = 0.5–3 × 105 mL/g. The materials possess high exchange capacity and selectivity, which makes them suitable sorbents for U(VI) removal.

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Data availability

Data will be made available on request.

Abbreviations

AAS :

Atomic adsorption spectroscopy

BET :

Brunauer–Emmett–Teller method

BJH :

Barrett-Joyner-Halenda Model

DFT :

Density functional theory

DTA :

Differential thermal analysis

EDS :

Energy-dispersive spectroscopy

LDH :

Layered double hydroxide

LRW :

Liquid radioactive waste

SEM :

Scanning electron microscopy

TG :

Thermogravimetric analysis

VSM :

Vibrating sample magnetometer

XRD :

X-ray diffraction

XRF :

X-ray fluorescence spectrometry

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Acknowledgements

The study was financially supported within the State Assignment of the Ministry of Science and Higher Education of the Russian Federation, topic No. FZNS-2023-0003. Equipment of interdisciplinary CUC in the field of nanotechnologies and new functional materials (FEFU, Vladivostok, Russia) used in the research is gratefully acknowledged.

Funding

State Assignment of the Ministry of Science and Higher Education of the Russian Federation, No. FZNS-2023-0003, Evgeniy Konstantinovich Papynov

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Authors and Affiliations

  1. Far Eastern Federal University, Russky Island, 10 Ajax Bay, 690922, Vladivostok, Russia

    N. P. Ivanov, A. N. Dran’kov, O. O. Shichalin, A. O. Lembikov, I. Yu. Buravlev, V. Yu. Mayorov, M. I. Balanov, K. A. Rogachev, G. D. Kaspruk, S. M. Pisarev, P. A. Marmaza, V. L. Rastorguev, V. A. Balybina, A. N. Fedorets & E. K. Papynov

  2. Institute of Physical Chemistry and Electrochemistry of the Russian Academy of Sciences, Bld.4, 31 Leninsky Prospect, 119072, Moscow, Russia

    V. O. Kaptakov

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Contributions

Ivanov N.P.: Conceptualization, Methodology, Investigation, Formal analysis, Writing—original draft. Dran’kov A.N.: Methodology, Conceptualization, Data curation, Supervision. Shichalin O.O.: Methodology, Supervision, Writing—editing. Lembikov O.O.: Investigation, Formal analysis, Software. Buravlev I.Yu. Methodology, Visualization, Software, Writing—editing. Mayorov V.Yu.: Investigation, Formal analysis, Software. Balanov M.I.: Investigation, Formal analysis, Software. Rogachev K.A.: Investigation, Formal analysis. Kaspruk G.D.: Investigation, Formal analysis. Pisarev S.M.: Investigation, Formal analysis, Validation. Marmaza P.A.: Investigation, Formal analysis, Validation. Rastorguev V.L.: Investigation, Formal analysis, Validation. Balybina V.A.: Investigation, Formal analysis, Validation. Fedorets A.N.: Investigation, Formal analysis, Visualization, Software. Kaptkaov V.O.: Writing—editing. Papynov E.K.: Project administration, Supervision, Funding Acquisition, Resources

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Ivanov, N.P., Dran’kov, A.N., Shichalin, O.O. et al. Composite magnetic sorbents based on magnetic Fe3O4 coated by Zn and Al layered double hydroxide for U(VI) removal from aqueous media. J Radioanal Nucl Chem 333, 1213–1230 (2024). https://doi.org/10.1007/s10967-024-09362-4

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