Abstract
This study investigates the influence of hot rolling on the quench sensitivity and heterogeneous precipitation behavior of 7150 aluminum alloy using an end-quenching process combined with conductivity testing, hardness testing, scanning electron microscopy, electron backscatter diffraction, transmission electron microscopy, scanning transmission electron microscopy, and high-resolution transmission electron microscopy. The results reveal that hot rolling significantly increases the quenching sensitivity of the 7150 aluminum alloy, as evidenced by the enhancement in conductivity difference from 0.7 to 1.6% IACS and the rise in hardness drop from 5.5 to 12% at both ends after hot rolling. Microstructural analysis indicates the presence of equiaxed grains with low dislocation density and well-coherent Al3Zr particles in the primitive alloy, with small precipitates of the η phase on the Al3Zr particles. Subsequent to hot rolling, recrystallization occurs, thereby resulting in the generation of numerous high-angle grain boundaries (HAGBs), incoherent Al3Zr particles, dislocations, and coherent Al3Zr particles. Consequently, this leads to increased variety, nucleation sites, sizes, and quantities of heterogeneous precipitates. HAGBs, characterized by high interfacial energy, are found to be the most favorable for the nonuniform nucleation and precipitation of the η phase, followed by low-angle grain boundaries. Significant precipitation of the η and T phases is observed on the noncoherent Al3Zr dispersoids within the recrystallized grains and some subgrains (SGs). Furthermore, the high-dislocation-density SGs not only facilitate the precipitation of the η and T phases but also result in the precipitation of the S and Y phases.
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Acknowledgements
This study was finally supported by the National Natural Science Foundation of China (52205421), Guangxi Science and Technology Major Project (AA23023028), the Key Laboratory Open Project of Guangdong Province (XF20230330-XT), the School-Enterprise, Industry-University-Research Cooperation Project (2023XF-FW-32), and the Science and Technology Innovation Program of Hunan Province, China (2021RC2087, and 2022JJ30570).
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CP: Investigation, Visualization and Writing—original draft. LC: Conceptualization and Methodology. ZD: Writing—original draft and Funding Acquisition. ZC and XB: Data curation and Formal analysis. XG: Software and Supervision.
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Cao, P., Li, C., Zhu, D. et al. Effect of hot deformation on quenching sensitivity and heterogeneous precipitation behavior of 7150 aluminum alloy. J Mater Sci 58, 16550–16564 (2023). https://doi.org/10.1007/s10853-023-09089-9
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DOI: https://doi.org/10.1007/s10853-023-09089-9