A sample preparation method was elaborated to increase the precision and accuracy of the structural parameters during studies of differences in the crystal structure of carbon fibers after heat treatments using x-ray structure analysis. The method included grinding and sieving of carbon fibers and pressing of the fiber powder into a cuvette for studies on a diffractometer.
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References
A. A. Konkin, Carbon and Other Flame-resistant Fibrous Materials [in Russian], Khimiya, Moscow, 1974, 376 pp.
P. Morgan, Carbon Fibers and Their Composites, Taylor and Francis, London, 2005, p. 1166.
E. Frank, L. M. Steudle, et al., Angew. Chem., Int. Ed., 53, No. 21, 5262-5298 (2014).
S. J. Park, Carbon Fibers, Springer Series in Materials Science, Vol. 210, Springer Netherlands, 2015, p. 330.
B. A. Newcomb, Composites, Part A, 91, Part 1, 262-282 (2016); https://doi.org/10.1016/j.compositesa.2016.10.018.
V. P. Sosedov (ed.), Properties of Construction Materials Based on Carbon. Handbook [in Russian], Metallurgiya, Moscow, 1975, 335 pp.
A. S. Fialkov, Carbon, Interlayer Compounds and Composites Based on It [in Russian], Aspekt Press, Moscow, 1997, p. 588, 718.
Yu. A. Skakov (ed.), Laboratory Practicum “Crystallography, X-ray Diffraction and Electron Microscopy” [in Russian], Department of X-ray Diffraction and Metal Physics, MISiS, Moscow, 1986.
S. C. Bennett, D. J. Johnson, and W. Johnson, J. Mater. Sci., 18, 3337-3347 (1983).
I. A. Bubnenkov, V. M. Samoilov, et al., RU Pat. No. 2,685,440, Apr. 18, 2019; Byull., No. 11.
D. B. Verbets, V. M. Samoilov, et al., Izv. Vyssh. Uchebn. Zaved., Khim. Khim. Tekhnol., 61, No. 11, 10-18 (2018); https://doi.org/10.6060/ivkkt.20186111.17y.
V. M. Samoilov, A. V. Nakhodnova, et al., Kompoz. Nanostrukt., 11, No. 2, 42 (2019).
V. M. Samoilov, D. B. Verbets, et al., Perspekt. Mater., No. 2, (2018).
E. A. Belenkov, Izv. Chelyabinsk. Nauch. Tsentra, No. 3, 26-33 (1999).
F. Liu, H. Wang, et al., J. Mater. Sci., 43, 4316-4322 (2008).
D. Li, H. Wang, and X. Wang, J. Mater. Sci., 42, 4642-4649 (2007).
E. V. Shelekhov and T. A. Sviridova, Metal Sci. Heat Treatment, 42, No. 8, 309-313 (2000).
J. I. Langford, J. Appl. Crystallogr., 11, 10-14 (1978).
V. S. Ostrovskii, Principles of Materials Science of Synthetic Graphites [in Russian], Metallurgizdat, Moscow, 2011, pp. 44-49.
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Translated from Khimicheskie Volokna, No. 1, pp. 61-66, January—February, 2020.
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Verbets, D.B., Bubnenkov, I.A., Dzidziguri, E.L. et al. Sample Preparation Method for X-Ray Structure Analysis of Carbon Fiber Crystal Structural Parameters after Various Heat Treatments. Fibre Chem 52, 65–70 (2020). https://doi.org/10.1007/s10692-020-10153-2
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DOI: https://doi.org/10.1007/s10692-020-10153-2