The reaction of sodium sulfide and thiols with formaldehyde and acetone in a solution of sodium hydroxide or in ethanol gave 1,1'-{3-[(alkylsulfanyl)methyl]tetrahydro-2H-thiopyran-3,5-diyl}dietha-nones.
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L. A. Baeva, A. D. Ulendeeva, O. V. Shitikova, and N. K. Lyapina, Khim. Geterotsikl. Soedin., 1494 (2009) [Chem. Heterocycl. Compd., 45, 1197 (2009)].
A. D. Ulendeeva, L. A. Baeva, T. S. Nikitina, L. V. Spirikhin, E. V. Vasil’eva, and N. K. Lyapina, Neftekhimiya, 44, 388 (2004).
A. D. Ulendeeva, L. A. Baeva, E. G. Galkin, E. V. Vasil’eva, and N. K. Lyapina, Neftekhimiya, 38, 214 (1998).
A. D. Ulendeeva, L. A. Baeva, N. K. Lyapina, V. N. Nesterov, and E. V. Vasil'eva, Neftekhimiya, 40, 311 (2000).
A. D. Ulendeeva, T. S. Nikitina, L. A. Baeva, L. V. Spirikhin, L. T. Karachurina, R. Yu. Khisamutdinova, N. S. Makara, F. S. Zarudii, and N. K. Lyapina, Khim.-Farm. Zh., 38, No. 12, 15 (2004).
I. A. Rubinshtein, Z. A. Kleimanova, and E. P. Sobolev, in: Methods of Analysis of Organic Petroleum Compounds, Their Mixtures and Derivatives [in Russian], Moscow (1960), p. 74.
V. I. Dronov, R. F. Nigmatullina, L. V. Spirikhin, and Yu. E. Nikitin, Zh. Org. Khim., 14, 2357 (1978).
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Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 646-650, April, 2012.
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Baeva, L.A., Biktasheva, L.F., Nikitina, T.S. et al. Synthesis of 1,1'-{3-[(alkylsulfanyl)methyl]-tetrahydro-2H-thiopyran-3,5-diyl}diethanones from sodium sulfide and thiols. Chem Heterocycl Comp 48, 601–605 (2012). https://doi.org/10.1007/s10593-012-1032-0
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DOI: https://doi.org/10.1007/s10593-012-1032-0