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Study of Aliphatic Polyurethanes by the Low-Field 1H NMR Relaxometry Method with the Inversion of the Integral Transformation

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Abstract

In this paper, the distributions of the 1H nuclear magnetic resonance (NMR) spin–lattice and spin–spin relaxation times are used to characterize the mobility of different sections of macromolecules of aliphatic polyurethanes and the cross-linking density of polymer chains. The NMR relaxometry method with inversion of integral transformation is applied to study the effect of poly (ethylene glycol) and glycerol phosphate calcium on the polymer dynamics.

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Acknowledgements

N. S. thanks the Russian Foundation for Basic Research (RFBR, project no. 18-03-00089a) for the financial support.

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Authors and Affiliations

  1. Gdansk University of Technology, Gabriela Narutowicza 11/12 Str, 80-233, Gdańsk, Poland

    J. Kucinska-Lipka & J. Haponiuk

  2. Immanuel Kant Baltic Federal University, 14 A. Nevskogo St., 236041, Kaliningrad, Russia

    Nikolay Sinyavsky, I. Mershiev & G. Kupriyanova

  3. Department of Physics and Chemistry, Baltic Fishing Fleet State Academy, Kaliningrad State Technical University, Molodezhnaya St. 6, 236029, Kaliningrad, Russia

    Nikolay Sinyavsky

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  1. J. Kucinska-Lipka
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  2. Nikolay Sinyavsky
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  3. I. Mershiev
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  4. G. Kupriyanova
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  5. J. Haponiuk
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Correspondence to Nikolay Sinyavsky.

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Kucinska-Lipka, J., Sinyavsky, N., Mershiev, I. et al. Study of Aliphatic Polyurethanes by the Low-Field 1H NMR Relaxometry Method with the Inversion of the Integral Transformation. Appl Magn Reson 50, 347–356 (2019). https://doi.org/10.1007/s00723-018-1067-1

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  • DOI: https://doi.org/10.1007/s00723-018-1067-1

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