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Electrochemical determination of levofloxacin drug at poly(clayton yellow)/carbon paste electrode

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Abstract

An effortless and quick analytical method was proposed for the determination of levofloxacin at poly(clayton yellow)/carbon paste electrode. It was fabricated by facile electro-polymerization manner using cyclic voltammetry. The proposed poly(clayton yellow)/carbon paste electrode and carbon paste electrode were characterized by field emission scanning electron microscope, electrochemical impedance spectroscopy, energy-dispersive X-ray spectroscopy, and electrochemical methods. It generates a clear and intense peak for levofloxacin (0.1 mM) by regulating over-potential as compared to carbon paste electrode. Under optimized conditions, differential pulse voltammetry was applied for the determination of levofloxacin in the range from 0.2 to 5.0 µM with a low detection and quantification limits of 17.1 nM and 57.5 nM, respectively. Finally, real-time analysis was performed in blood serum sample with excellent recovery.

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Authors and Affiliations

  1. Department of Chemistry, FMKMC College, A Constituent College of Mangalore University, Madikeri, Karnataka, India

    Girish Tigari, J. G. Manjunatha, Edwin D’ Souza, C. Raril, N. Hareesha & M. M. Charithra

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  1. Girish Tigari
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  2. J. G. Manjunatha
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  3. Edwin D’ Souza
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  4. C. Raril
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  5. N. Hareesha
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  6. M. M. Charithra
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Correspondence to J. G. Manjunatha.

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Tigari, G., Manjunatha, J.G., Souza, E.D. et al. Electrochemical determination of levofloxacin drug at poly(clayton yellow)/carbon paste electrode. Monatsh Chem 153, 311–319 (2022). https://doi.org/10.1007/s00706-022-02910-2

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  • DOI: https://doi.org/10.1007/s00706-022-02910-2

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