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Systematic evaluation of selective fusion additive manufacturing based on thermal energy source applied in processing of titanium alloy specimens for medical applications

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Abstract

In this study, two selective metal fusion additive manufacturing (AM) technologies, electron-beam melting (EBM) and selective laser melting (SLM), were used to fabricate Ti6Al4V test specimens for a comprehensive evaluation, including physical-chemical properties and biological properties. The results indicated that the mechanical behaviors, for instance tensile strength and yield strength, of the processed metal devices could exhibit different outcomes with the use of fusion approaches with different thermal energies. Moreover, the relationship between mechanical properties and the crystal structure, α:β-phase ratio, was characterized systematically to evaluate the samples produced via these two powder bed methods. The corrected β-phase fractions of the EBM and SLM specimens were 0.12 and 0.10, respectively, which corresponded to a slight difference in mechanical strength. Furthermore, the EBM- and SLM-fabricated specimens presented excellent biocompatibility in an in vitro cellular evaluation. Consequently, our findings demonstrated that the AM-fabricated Ti6Al4V parts conformed to all of the international standard requirements, particularly in terms of the mechanical properties, chemical composition, and non-corrosiveness. Thus, we believe that our study can contribute to the further development of additive manufacturing processes.

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References

  1. Touri M, Kabirian F, Saadati M, Ramakrishna S, Mozafari M (2019) Additive manufacturing of biomaterials—the evolution of rapid prototyping. Adv Eng Mater 21:1800511

    Article  Google Scholar 

  2. Chua CK, Leong KF (2014) 3D printing and additive manufacturing: principles and applications (with companion media pack) of rapid prototyping fourth edition. World Scientific Publishing Company

  3. Mueller B (2012) Additive manufacturing technologies—rapid prototyping to direct digital manufacturing. Assem Autom 32(2)

  4. Namatollahi M, Jahadakbar A, Mahtabi MJ, Elahinia M (2019) Additive manufacturing (AM). Metals for Biomedical Devices. Elsevier, p. 331–53

  5. Zhang B, Goel A, Ghalsasi O, Anand S (2019) CAD-based design and pre-processing tools for additive manufacturing. J Manuf Syst 52:227–241

    Article  Google Scholar 

  6. Patel DK, Sakhaei AH, Layani M, Zhang B, Ge Q, Magdassi S (2017) Highly stretchable and UV curable elastomers for digital light processing based 3D printing. Adv Mater 29(15):1606000

    Article  Google Scholar 

  7. Ngo TD, Kashani A, Imbalzano G, Nguyen KT, Hui D (2018) Additive manufacturing (3D printing): a review of materials, methods, applications and challenges. Compos Part B 143:172–196

    Article  Google Scholar 

  8. Liu S, Shin YC (2019) Additive manufacturing of Ti6Al4V alloy: a review. Mater Des 164:107552

    Article  Google Scholar 

  9. Huang Y, Leu MC, Mazumder J, Donmez A (2015) Additive manufacturing: current state, future potential, gaps and needs, and recommendations. J Manuf Sci Eng 137(1):014001

    Article  Google Scholar 

  10. Sing SL, An J, Yeong WY, Wiria FE (2016) Laser and electron-beam powder-bed additive manufacturing of metallic implants: a review on processes, materials and designs. J Orthop Res 34(3):369–385

    Article  Google Scholar 

  11. De Pasquale G, Luceri F, Riccio M (2019) Experimental characterization of SLM and EBM cubic lattice structures for lightweight applications. Exp Mech 59:469–482

    Article  Google Scholar 

  12. Crupi V, Epasto G, Guglielmino E, Squillace A (2017) Influence of microstructure [alpha + beta and beta] on very high cycle fatigue behaviour of Ti-6Al-4V alloy. Int J Fatigue 95:64–75

    Article  Google Scholar 

  13. Prasad AR, Ramji K, Datta G (2014) An experimental study of wire EDM on Ti-6Al-4V alloy. Procedia Mater Sci 5:2567–2576

    Article  Google Scholar 

  14. Zhang Z, Qu S, Feng A, Hu X, Shen J (2019) Microstructural mechanisms during multidirectional isothermal forging of as-cast Ti-6Al-4V alloy with an initial lamellar microstructure. J Alloys Compd 773:277–287

    Article  Google Scholar 

  15. Pinkerton AJ (2016) Lasers in additive manufacturing. Opt Laser Technol 78:25–32

    Article  Google Scholar 

  16. Hinojos A, Mireles J, Reichardt A, Frigola P, Hosemann P, Murr LE, Wicker RB (2016) Joining of Inconel 718 and 316 stainless steel using electron beam melting additive manufacturing technology. Mater Des 94:17–27

    Article  Google Scholar 

  17. Galati M, Iuliano L (2017) A literature review of powder-based electron beam melting focusing on numerical simulations. Addit Manuf

  18. Xu W, Brandt M, Sun S, Elambasseril J, Liu Q, Latham K, Xia K, Qian M (2015) Additive manufacturing of strong and ductile Ti–6Al–4V by selective laser melting via in situ martensite decomposition. Acta Mater 85:74–84

    Article  Google Scholar 

  19. DebRoy T, Wei H, Zuback J, Mukherjee T, Elmer J, Milewski J et al (2018) Additive manufacturing of metallic components—process, structure and properties. Prog Mater Sci 92:112–224

    Article  Google Scholar 

  20. ASTM F3001-14 (2014) Standard specification for additive manufacturing titanium-6 aluminum-4 vanadium ELI (extra low interstitial) with powder bed fusion, ASTM International, West Conshohocken, PA. www.astm.org

  21. ASTM F746-04 (2014) Standard test method for pitting or crevice corrosion of metallic surgical implant materials. ASTM International, West Conshohocken www.astm.org

    Google Scholar 

  22. ASTM E8/E8M-16a (2016) Standard test methods for tension testing of metallic materials. ASTM International, West Conshohocken www.astm.org

    Google Scholar 

  23. ASTM E9-09 (2018) Standard test methods of compression testing of metallic materials at room temperature. ASTM International, West Conshohocken www.astm.org

    Google Scholar 

  24. ASTM E384-17 (2017) Standard test method for microindentation hardness of materials. ASTM International, West Conshohocken www.astm.org

    Google Scholar 

  25. Wataha JC, Lockwood PE, Noda M, Nelson SK, Mettenburg DJ (2002) Effect of toothbrushing on the toxicity of casting alloys. J Prosthet Dent 87(1):94–98

    Article  Google Scholar 

  26. Lütjering G (1998) Influence of processing on microstructure and mechanical properties of (α + β) titanium alloys. Mater Sci Eng A 243(1–2):32–45

    Article  Google Scholar 

  27. Pederson R, Babushkin O, Skystedt F, Warren R (2003) Use of high temperature X-ray diffractometry to study phase transitions and thermal expansion properties in Ti-6Al-4V. Mater Sci Technol 19(11):1533–1538

    Article  Google Scholar 

  28. Galarraga H, Warren RJ, Lados DA, Dehoff RR, Kirka MM, Nandwana P (2017) Effects of heat treatments on microstructure and properties of Ti-6Al-4V ELI alloy fabricated by electron beam melting (EBM). Mater Sci Eng A 685:417–428

    Article  Google Scholar 

  29. Sidambe AT (2014) Biocompatibility of advanced manufactured titanium implants—a review. Materials 7(12):8168–8188

    Article  Google Scholar 

  30. Khorasani A, Gibson I, Goldberg M, Littlefair G (2017) Production of Ti-6Al-4V acetabular shell using selective laser melting: possible limitations in fabrication. Rapid Prototyp J 23(1):110–121

    Article  Google Scholar 

  31. Heakal FE-T, Awad KA (2011) Electrochemical corrosion and passivation behavior of titanium and its Ti–6Al–4V alloy in low and highly concentrated HBr solutions. Int J Electrochem Sci 6:6483–6502

    Google Scholar 

  32. Murr L, Quinones S, Gaytan S, Lopez M, Rodela A, Martinez E et al (2009) Microstructure and mechanical behavior of Ti–6Al–4V produced by rapid-layer manufacturing, for biomedical applications. J Mech Behav Biomed Mater 2(1):20–32

    Article  Google Scholar 

  33. Rafi H, Karthik N, Gong H, Starr TL, Stucker BE (2013) Microstructures and mechanical properties of Ti6Al4V parts fabricated by selective laser melting and electron beam melting. J Mater Eng Perform 22(12):3872–3883

    Article  Google Scholar 

  34. Shunmugavel M, Polishetty A, Littlefair G (2015) Microstructure and mechanical properties of wrought and additive manufactured Ti-6Al-4 V cylindrical bars. Proc Technol 20:231–236

    Article  Google Scholar 

  35. Vrancken B, Thijs L, Kruth J-P, Van Humbeeck J (2012) Heat treatment of Ti6Al4V produced by selective laser melting: microstructure and mechanical properties. J Alloys Compd 541:177–185

    Article  Google Scholar 

  36. De Formanoir C, Michotte S, Rigo O, Germain L, Godet S (2016) Electron beam melted Ti–6Al–4V: microstructure, texture and mechanical behavior of the as-built and heat-treated material. Mater Sci Eng A 652:105–119

    Article  Google Scholar 

  37. Azevedo C, Rodrigues D, Neto FB (2003) Ti–Al–V powder metallurgy (PM) via the hydrogenation–dehydrogenation (HDH) process. J Alloys Compd 353(1–2):217–227

    Article  Google Scholar 

  38. Srivastava D, Chang I, Loretto M (2001) The effect of process parameters and heat treatment on the microstructure of direct laser fabricated TiAl alloy samples. Intermetallics. 9(12):1003–1013

    Article  Google Scholar 

  39. Wanying L, Yuanhua L, Yuhai C, Taihe S, Singh A (2017) Effect of different heat treatments on microstructure and mechanical properties of Ti6Al4V titanium alloy. Rare Metal Mater Eng 46(3):634–639

    Article  Google Scholar 

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Funding

The investigation was supported by Taiwan Food and Drug Administration, Ministry of Health, Labor, and Welfare (MOHW105-FDA-B-114-000542).

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Correspondence to Chun-Chieh Tseng or Pei-Weng Tu.

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Huang, JY., Chang, CH., Wang, WC. et al. Systematic evaluation of selective fusion additive manufacturing based on thermal energy source applied in processing of titanium alloy specimens for medical applications. Int J Adv Manuf Technol 109, 2421–2429 (2020). https://doi.org/10.1007/s00170-020-05797-7

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  • DOI: https://doi.org/10.1007/s00170-020-05797-7

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