Summary
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1.
Methyl-2∶3∶4-trihydroxy benzoate was formylated by the action of hexamethylene-tetramine in glacial acetic acid and methyl-2∶3∶4-trihydroxy-5-formyl benzoate was obtained. Several derivatives of the formyl ester were prepared and the structure established.
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2.
Formylation of several hydroxy compounds was also attempted.
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References
Desai and RadhaProc. Ind. Acad. Sci., A, 1940,11, 422.
Robinson and ShahJ., 1934, 1497.
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Desai, R.D., Radha, K.S. & Shah, R.C. The action of hexamethylene tetramine on phenols and the methyl esters of phenol carboxylic acids. Proc. Indian Acad. Sci. (Math. Sci.) 23, 179 (1946). https://doi.org/10.1007/BF03170934
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DOI: https://doi.org/10.1007/BF03170934