Skip to main content
Log in

Analysis of dimerized fatty acids by TLC/FID

  • Technical
  • Published:
Journal of the American Oil Chemists’ Society

Abstract

A rapid method is described for the analysis of the monomer, dimer and trimer components of polymerized fatty acids by thin layer chromatography (TLC) with flame ionization detection (FID) on the Iatroscan. The short- and long-term precisions of the method are discussed, as is the correlation of TLC/FID data with the gas-liquid Chromatographic (GLC) data for dimerized fatty acids. The TLC/FID method is shown to be the superior technique for process control applications.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Leonard, E.C.,The Dimer Acids, Humko Sheffield Chemical, Memphis, TN, 1975.

    Google Scholar 

  2. Firestone, D.,J. Am. Oil Chem. Soc. 40:247 (1963).

    Article  CAS  Google Scholar 

  3. Frankel, E.N., CD. Evans, H.A. Moser, D.G. McConnell and J.C. Cowan,Ibid 38:130 (1961).

    Article  CAS  Google Scholar 

  4. Chang, T.L.,Anal. Chem. 40:989 (1968).

    Article  CAS  Google Scholar 

  5. Harris, W.C., E.P. Crowell and B.B. Burnett,J. Am. Oil Chem. Soc. 50:537 (1973).

    Article  CAS  Google Scholar 

  6. Veasey, R.L.,Ibid. 63:1043 (1986).

    Google Scholar 

  7. Payler, R.A.L., R. Feinland and N.H. Conroy,Anal. Chem. 40:1358 (1968).

    Article  Google Scholar 

  8. Arlt, H.G. Jr., U.S. Patent 3,367,952 (1968).

    Google Scholar 

  9. Nelson, J.P., and A.J. Milun,J. Am. Chem. Soc. 52:81 (1975).

    Article  CAS  Google Scholar 

  10. Padley, F.B.,J. Chromatogr. 39:37 (1969).

    Article  CAS  Google Scholar 

  11. Cotgreave, T., and A. Lynes,Ibid. 30:117 (1967).

    Article  CAS  Google Scholar 

  12. Szakasits, J.J., P.V. Peurifoy and L.A. Woods,Anal Chem. 42:351 (1970).

    Article  CAS  Google Scholar 

  13. Ackman, R.G.,Methods Enzym. 72:205 (1981).

    Article  CAS  Google Scholar 

  14. Ranger, H.O.,American Laboratory 13:146 (1981).

    CAS  Google Scholar 

  15. Sebedio, J.L., and R.G. Ackman,J. Chromatogr. Sci. 19:552 (1981).

    CAS  Google Scholar 

  16. Newman, J.M.,Lipids 20:501 (1985).

    Article  Google Scholar 

  17. Zeman, I., M. Ranny and L. Winterova,J. Chromatogr. 354:283 (1986).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

About this article

Cite this article

Fritz, D.W., Amore, F. & Rashmawi, K. Analysis of dimerized fatty acids by TLC/FID. J Am Oil Chem Soc 65, 1488–1492 (1988). https://doi.org/10.1007/BF02898314

Download citation

  • Received:

  • Accepted:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02898314

Keywords

Navigation