Skip to main content
Log in

The determination of tin in biological samples

  • Published:
Journal of Radioanalytical Chemistry Aims and scope Submit manuscript

Abstract

A rapid method is described for the determination of tin in biological material, using123Sn (T=40 m). The chemical procedure is based on the nearly quantitative extraction of tetravalent tin into toluene from an acid 1.3M iodide solution. The recovery is determined by spiking the solution with113Sn and measuring the activity of the113mIn daughter in the counting sample. The lower limit of the determination is ≃0.01μg. Results are given for standard kale powder and dried animal blood.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. K. Schwarz, Proc, Symp. on Nuclear Activation Techniques in the Life Sciences, Bled, Yugoslavia, 1972, IAEA, Vienna, 1972, p. 3.

  2. E. B. Sandell, Colorimetric Determination of Traces of Metals, Interscience, New York, 1959, p. 852.

    Google Scholar 

  3. E. Schroll, M. Weniger, A. J. McDonald, R. E. Stanton, Mikrochim. Acta, (1965) 378; Analyst, 87 (1962) 600.

  4. R. F. Tattle et al.: IAEA Symp. on the Use of Nuclear Techniques in the Measurement and Control of Environmental Pollution. Salzburg, Oct. 1970. Paper SM-142/4.

  5. H. A. Das J. G. van Raaphorst, H. J. L. M. Umans, J. Radional. Chem., 4 (1970) 21.

    CAS  Google Scholar 

  6. H. Steiner, W. Kiesl, F. Kluger, F. Hecht, J. Radioanal. Chem., 7 (1971) 235.

    Google Scholar 

  7. H. Hamaguchi, et al., Geochim. Cosmochim. Acta, 26 (1962) 503; 28 (1964) 1039; 33 (1969) 507; Anal. Chim. Acta, 30 (1964) 335.

    Article  CAS  Google Scholar 

  8. H. J. M. Bowen, Analyst, 97 (1972) 1003.

    Article  CAS  Google Scholar 

  9. B. M. Tejam, B. C. Haldar, Radiochem. Radioanal. Letters, 13 (1972) 25.

    Google Scholar 

  10. D. Schmidt, K. Strabe, Radiochim Acta. 11 (1969) 197.

    CAS  Google Scholar 

  11. A. R. Byrne, D. Gorenc, Anal. Chim. Acta 59 (1972) 81.

    Article  CAS  Google Scholar 

  12. A. R. Byrne, Radiochem. Radioanal. Letters, 7 (1971) 287.

    CAS  Google Scholar 

  13. J. J. M. de Goey, J. J. Kroon, Report IRI 133-73-08.

  14. A. R. Byrne, Personal communication.

  15. H. J. M. Bowen, Advances in Activation Analysis, Vol. 1, Academic Press, London, 1970, p. 101.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Ooms, P.C., van Woerkom, R. & Das, H.A. The determination of tin in biological samples. J. Radioanal. Chem. 23, 33–41 (1974). https://doi.org/10.1007/BF02514342

Download citation

  • Received:

  • Issue Date:

  • DOI: https://doi.org/10.1007/BF02514342

Keywords

Navigation