Summary
Penstemide and serrulatoloside, two iridoids of similar molecular structure, were separated by stepwise gradient TLC in a straight-phase systems (silica-ethyl acetate+isopropanol) and by HPLC in a reversed-phase system (ODS-silica — water+methanol).
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References
S. D. Jolad, J. J. Hofmann, R. M. Wiedhopf, J. R. Cole, R. B. Bates, G. R. Kriek, Tetrahedron Lett. 4119, (1976).
S. R. Jensen, B. J. Nielsen, C. B. Mikkelson, J. J. Hofmann, S. D. Jolad, J. R. Cole, Tetrahedron Lett. 3261 (1979).
B. Gering, P. Junior, M. Wichtl, Phytochemistry26, 753 (1987).
P. Junior, Planta Med.47, 161 (1983).
P. Junior, Planta Med.50, 438 (1984).
H. Wysokińska, L. Świątek, I. Marciniak, M. Rózga, Acta Polon. Pharm.45, 83 (1988).
R. U. Schenk, A. C. Hildebrandt, Can. J. Botany50, 199 (1972).
E. Soczewiński, in: Planar Chromatography, Vol. 1 (R. E. Kaiser, Ed.) Hüthig, Heidelberg 1986, p. 79.
E. Soczewiński, T. Wawrzynowicz, Chromatographia11, 466 (1978).
G. Matysik, E. Soczewiński, J. Chromatogr.355, 363 (1986).
G. Matysik, E. Soczewiński, J. Chromatogr.369, 19 (1986).
G. Matysik, E. Soczewiński, J. Chromatogr.446, 275 (1988).
B. L. Karger, J. N. Le Page, N. Tanaka, in: High-Performance Liquid Chromatography, Vol. 1 (Cs. Horváth, Ed.), Academic Press, New York, 1980, p. 113.
C. Horvath, W. R. Melander, J. Chromatogr. Sci.15, 393 (1977).
E. Soczewiński, C. A. Wachtmeister, J. Chromatogr.7, 311 (1962).
L. R. Snyder, J. J. Kirkland, Introduction to Modern Liquid Chromatography, Wiley-Interscience, New York, 1973.
E. Soczewiński, G. Matysik, J. Liq. Chromatogr.8, 1225 (1985).
E. Soczewiński, G. Matysik, K. Glowniak, Instrumental High Performance TLC, Proc. 3rd Intern. Symp. Würzburg, 1985, Institute for Chromatography, Bad Dürkheim, 1985, p. 413.
K. Glowniak, G. Matysik, M. Bieganowska, E. Soczewiński, Chromatographia,22, 307 (1986).
E. Soczewiński, B. Psionka, J. Kuczmierczyk, J. Liq. Chromatogr.3, 1829 (1980).
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Dzido, T., Matysik, G., Soczewiński, E. et al. Chromatographic analysis of penstemide and serrulatoloside by high-performance liquid chromatography and gradient thin-layer chromatography. Chromatographia 27, 24–26 (1989). https://doi.org/10.1007/BF02290399
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DOI: https://doi.org/10.1007/BF02290399