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Sodium dispersions in elementary analysis

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Summary

Gently warming the compound with a dispersion of sodium in a suitable organic solvent reduces nitrogen to ammonia and sulfur, to sulfide.

Zusammenfassung

Stickstoff wird zu Ammoniak und Schwefel zu Sulfid reduziert, wenn die organische Verbindung vorsichtig mit einer Dispersion von metallischem Natrium in einem geeigneten organischen Lösungsmittel erwärmt wird.

Résumé

En chauffant doucement le composé avec une dispersion de sodium dans un solvant organique convenable, l'azote est réduit en ammoniac et le soufre en sulfure.

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References

  1. R. L. Menville andW. W. Parker, Analyt. Chemistry31, 1901 (1959).

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  2. F. Schneider, Organic Qualitative Microanalysis. New York: Wiley. 1946. p. 79.

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  3. F. Schneider, 1. c, p. 81.

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Authors and Affiliations

  1. C. W. Post College, Brookville, N. Y.

    John Patrick & Frank Schneider

Authors
  1. John Patrick
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  2. Frank Schneider
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Additional information

On the occasion of the hundredth return ofFriedrich Emich's birthday.

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Patrick, J., Schneider, F. Sodium dispersions in elementary analysis. Mikrochim Acta 48, 970–972 (1960). https://doi.org/10.1007/BF01216087

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  • DOI: https://doi.org/10.1007/BF01216087

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