Summary
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1.
By the action of 1,3-propanediol and of 1,3-butanediol on phosphorus trichloride, the cyclic compounds, trimethylene phosphorochloridite and 1-methyltrimethylene phosphorochloridite, have been prepared.
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2.
By reaction of the phosphorochloridites with alcohols in presence of dimethylaniline, the following mixed esters have been synthesized:
Some of their properties have been studied.
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A. E. Arbuzov and V. M. Zoroastrova, Bull. Acad. Sci. Div. Chem. Sci., No. 5, 770 (1952).
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Arbuzov, A.E., Zoroastrova, V.A. Esters of “glycolphosphorus acids” Communcation 2. Compounds having a six-membered ring. Russ Chem Bull 1, 705–712 (1952). https://doi.org/10.1007/BF01198853
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DOI: https://doi.org/10.1007/BF01198853