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Crystal structure of 5α-bromo-8β,9α-dimethyl-hydrindane-1,4-dione

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Abstract

The molecular structure of 5α-bromo-8β,9α-dimethylhydrindane-1,4-dione (C11H15BrO2) has been confirmed using three-dimensional X-ray data collected by means of a Picker FACS-1 four-circle diffractometer. The compound crystallized in the space groupC2/c with unit cell constantsa = 26.56(5),b = 6.68(1),c = 12.32(2) Å and β = 90.6(1) °; the density was 1.55 g cm−3 andZ = 8. Least-squares refinement of the positional and anistropic thermal parameters gave a finalR 1 value of 0.083 for 793 significant reflections.

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Authors and Affiliations

  1. Department of Chemistry, Michigan State University, 48823, East Lansing, Michigan

    J. D. Yordy & M. A. Neuman

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  1. J. D. Yordy
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  2. M. A. Neuman
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Yordy, J.D., Neuman, M.A. Crystal structure of 5α-bromo-8β,9α-dimethyl-hydrindane-1,4-dione. Journal of Crystal and Molecular Structure 4, 121–127 (1974). https://doi.org/10.1007/BF01197907

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  • DOI: https://doi.org/10.1007/BF01197907

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