Conclusions
As a result of the successive reaction of galactitol with P(NEt2)3 and sulfur we have obtained diastereomeric galactitol 1,6-bis-O-[di(N-diethylamido)thionophosphate] 2,3:4,5-bis-O-(N-diethylamidothionophosphates) (the structure of one of them was established by x-ray diffraction analysis) and galactitol 1,2:3,4:5,6-tris-O-(N-diethylamidothionophosphates).
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Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 4, pp. 896–903, April, 1983.
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Gurarii, L.I., Litvinov, I.A., Struchkov, Y.T. et al. Structure of some products of the amidothionophosphorylation of galactitol. Russ Chem Bull 32, 815–820 (1983). https://doi.org/10.1007/BF00953485
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DOI: https://doi.org/10.1007/BF00953485