Abstract
We present a new method of thermal analysis based on the position change during melting of samples heated in an electromagnetic levitation coil. The temperature is measured with a two-colour pyrometer, subject to appropriate corrections. This method appears to be a useful complement to other investigations such as differential thermal analysis (DTA) or “simultaneous stepwise heating”. The technique has been applied to the determination of the melting temperatures of alloys in the Nb-rich part of the Nb-Ge system.
Similar content being viewed by others
References
E. C. Okress, D. M. Wroughton, G. Gomenets, P. H. Brace andJ. C. R. Kelly,J. Appl. Phys. 23 (1952) 545.
R. Weissberg,Rev. Sci. Instrum. 30 (1959) 135.
H. Bartholin, J. Laforet, R. Lemaire, J. Schweizer andJ. Silvera,Acta Cryst. 21 (1966) A94.
V. Ya. Chekhovskoï, A. E. Sheindlin andB. Ya. Berezin,High Temp. High Pressures 2 (1970) 301.
O. P. Bansal andJ. A. Morrison,Mater. Res. Bull. 10 (1975) 1181.
O. C. Roberts, D. G. C. Robertson andA. E. Jenkins,Trans AIME 245 (1963) 2413.
M. Sunderland, A. E. Hamielac, W. K. Lu andA. McLean,Met. Trans. 4 (1973) 575.
J. Van Audenhove,Rev. Sci. Instrum. 36 (1965) 383.
D.W. Bonnel, J. A. Treverton, A. J. Valerga andJ. L. Malgrave, “Temperature, Its Measurement and Control in Science and Industry”, Vol. 4, Part 1, edited by H. Preston-Thomas, T. P. Murray and R. L. Shepard (Pittsburgh Instrument Society of America, 1972) p. 483.
J. M. Baker, C. E. Mighton andW. R. Bitler,Rev. Sci. Instrum. 40 (1963) 1065.
R. Flükiger andJ. L. Jorda, “Applications of Phase Diagrams in Metallurgy and Ceramics”, Vol. 1, National Bureau of Standards Special Publication 496 (1978) p. 375.
R. W. Cahn, K. D. Krichnanand, M. Laridjani, M. Greenholz andR. Hill,Mater. Sci. Eng. 23 (1976) 83.
A. Stretz andR. C. Bautista,High. Temp. High Pressures 7 (1975) 197.
J. L. Jorda, R. Flükiger andJ. Muller,J. Less-Common Metals 55 (1977) 249.
Idem, ibid. (to be published).
L. N. Latyev, V. Ya. Chekhovskoï andE. N. Shestakov,High Temp. High Pressures 4 (1972) 679.
S. Ackerman, “Temperature, Its Measurement and Control in Science and Industry”, Vol. 3; Part 2, edited by A. I. Dahl (Reinhold, New York, 1962) p. 849.
Handbook of Chemistry and Physics, 53rd edn. (CRC Press, 1972–1973) p. D142.
V. M. Pan, V. I. Latyesheva andE. A. Shishkin, “Metallography, Physics, Chemistry and Metals Physics of Superconductors” (Izd. Mankoa., Moscow, 1967).
A. Müller,Z. Naturforsch. 25A (1970) 1659.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Jorda, J.L., Flükiger, R. & Müller, J. Thermal analysis of levitation-heated samples: Application to the niobium-germanium system. J Mater Sci 13, 2471–2476 (1978). https://doi.org/10.1007/BF00808063
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/BF00808063