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Detection of Several Carbohydrates Using Boron-doped Diamond Electrodes Modified with Nickel Hydroxide Nanoparticles

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Abstract

In this work the electrooxidations of glucose, galactose, mannose, rhamnose, xylose and arabinose are studied at a nickel hydroxide nanoparticle modified boron-doped diamond electrode and compared to an unmodified electrode. These carbohydrates are very important in the second-generation ethanol production process. Nickel hydroxide modified borondoped diamond was characterized by scanning electron microscopy and energy dispersive X-ray. Electrochemical impedance spectroscopy was employed to study the interface properties of surface-modified electrodes in the absence and presence of the carbohydrates. Limits of detection were 5.3 × 10#x2212;5, 6.8 × 10−5, 2.7 × 10−4, 6.9 × 10−5, 8.8 × 10−5 and 2.6 × 10−5 mol L−1 for glucose, galactose, mannose, rhamnose, arabinose, xylose, respectively.

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Acknowledgments

The authors acknowledge financial support from Fundação de Amparo à Pesquisa do Estado de São Paulo–FAPESP (Process 2012/00258-5) and Centro Nacional de Desenvolvimento Cientifico e Tecnologico–CNPq (162208/2012-0).

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Authors and Affiliations

  1. Department of Analytical Chemistry, Institute of Chemistry, Universidade Estadual Paulista (UNESP), Rua Prof. Francisco Degni, 55, Araraquara, 14800-060, Brazil

    Graziela C. Sedenho & Nelson R. Stradiotto

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  1. Milena E. Teixeira
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  2. Graziela C. Sedenho
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  3. Nelson R. Stradiotto
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Correspondence to Nelson R. Stradiotto.

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Teixeira, M.E., Sedenho, G.C. & Stradiotto, N.R. Detection of Several Carbohydrates Using Boron-doped Diamond Electrodes Modified with Nickel Hydroxide Nanoparticles. ANAL. SCI. 31, 773–780 (2015). https://doi.org/10.2116/analsci.31.773

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