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Analysis of the Structural Evolution of Zinc Oxide Powders Obtained by Mechanical High-Energy Grinding

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Abstract

Zinc oxide powders made by mechanical high-energy grinding have been investigated using the methods of scanning electron microscopy, thermal nitrogen desorption, and Raman spectroscopy of infrared Fourier spectroscopy. Their structural evolution, including reduction of the average size of crystallites, increase in specific surface area, as well as changes in the number and ratio of adsorption centers, has been demonstrated. The data on the reconstruction of the surface of zinc oxide powders and multiple bond breaking in near-surface areas resulting from long-term dispersion have been presented.

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Funding

The work was received financial support from the Ministry of Education and Science of the Russian Federation (project 16.897.2017/PCh), as well as Scholarships and Grants of the President of the Russian Federation (SP-84.2018.1, SP-3800.2018.1, MK-1882.2018.8).

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Authors and Affiliations

  1. Penza State University, 440026, Penza, Russia

    I. A. Averin, I. A. Pronin, N. D. Yakushova, A. A. Karmanov & V. A. Moshnikov

  2. St. Petersburg State Electrotechnical University LETI, 197022, St. Petersburg, Russia

    I. A. Pronin & V. A. Moshnikov

  3. St. Petersburg State Technological Institute (Technical University), 190013, St. Petersburg, Russia

    M. M. Sychev & S. V. Vikhman

  4. Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences, 199034, St. Petersburg, Russia

    M. M. Sychev

  5. Research and Development Center for Thin-Film Technologies in Energetics, 194064, St. Petersburg, Russia

    V. S. Levitsky

  6. Ioffe Institute, Russian Academy of Sciences, 194022, St. Petersburg, Russia

    E. I. Terukov

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  1. I. A. Averin
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  2. I. A. Pronin
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  3. N. D. Yakushova
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  4. A. A. Karmanov
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  5. M. M. Sychev
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  6. S. V. Vikhman
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  7. V. S. Levitsky
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  8. V. A. Moshnikov
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  9. E. I. Terukov
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Correspondence to I. A. Pronin.

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Translated by N. Petrov

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Averin, I.A., Pronin, I.A., Yakushova, N.D. et al. Analysis of the Structural Evolution of Zinc Oxide Powders Obtained by Mechanical High-Energy Grinding. Tech. Phys. 64, 1330–1335 (2019). https://doi.org/10.1134/S1063784219090020

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  • DOI: https://doi.org/10.1134/S1063784219090020

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