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Structural Changes in the Vanadium Sample Surface Induced by Pulsed High-Temperature Deuterium Plasma and Deuterium Ion Fluxes

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Abstract

The structural changes in the vanadium sample surface are studied as functions of the conditions of irradiation by pulsed high-temperature deuterium plasma and deuterium ion fluxes in the Plasma Focus installation. It is found that processes of partial evaporation, melting, and crystallization of the surface layer of vanadium samples take place in the plasma flux power density range q = 108–1010 W/cm2 and the ion flux density range q = 1010–1012 W/cm2. The surface relief is wavelike. There are microcracks, gas-filled bubbles (blisters), and traces of fracture on the surface. The blisters are failed in the solid state. The character of blister fracture is similar to that observed during usual ion irradiation in accelerators. The samples irradiated at relatively low power density (q = 107–108 W/cm2) demonstrate the ejection of microparticles (surface fragments) on the side facing plasma. This process is assumed to be due to the fact that the unloading wave formed in the sample–target volume reaches its irradiated surface. Under certain irradiation conditions (sample–anode distance, the number of plasma pulses), a block microstructure with block sizes of several tens of microns forms on the sample surfaces. This structure is likely to form via directional crack propagation upon cooling of a thin melted surface layer.

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References

  1. B. A. Kalin, V. I. Pol’skii, V. L. Yakushin, V. I. Basil’ev, Yu. V. Skvortsov, and S. S. Tserevitinov, “Radiation damage and modification of materials under action of pulsed plasma flows,” Fiz. Khim. Obrab. Mater., No. 2, 20–31 (1991).

    Google Scholar 

  2. V. Henc-Bartolic, H.-J. Kunze, E. Kovacevic, and M. Stubicar, “Laser action on magnesium and aluminum targets,” Acta Phys. Slovaca 54, 251 (2004).

    Google Scholar 

  3. V. S. Kovivchak, T. V. Panova, and K. A. Mikhailov, “Formation of periodic structures on the magnesium and aluminum surfaces under action of a power ion beam with nanosecond duration,” Poverkhnost, No. 1, 73–76 (2012).

    Google Scholar 

  4. A. A. Chernov, “Layer–spiral growth of crystals,” Usp. Fiz. Nauk 73 (2), 277–331 (1961).

    Article  Google Scholar 

  5. M. I. Guseva and Yu. V. Martynenko, “Radiation blistering,” Usp. Fiz. Nauk 135 (4), 671–691 (1981).

    Article  Google Scholar 

  6. G. G. Bondarenko, Radiation Physics, Structure and Strength of Solids (Laboratoriya Znanii, Moscow, 2016).

    Google Scholar 

  7. P.-J. Hultgren and T. E. Scott, “Proton-bombardment-induced blistering of vanadium,” J. Appl. Phys. 47, 4394–4400 (1976).

    Article  Google Scholar 

  8. V. N. Pimenov, V. A. Gribkov, L. I. Ivanov, M. Sholts, et al., “On new possibilities of applying Plasma-Focus installations for modification of surface layers of materials,” Perspekt. Mater., No. 1, 13–23 (2003).

    Google Scholar 

  9. V. N. Pimenov, S. A. Maslyaev, E. V. Demina, A. V. Kovtun, et al., “Interaction of power pulsed energy flows with a tungsten surface in the Plasma-Focus installation,” Fiz. Khim. Obrab. Mater., No. 3, 5–14 (2008).

    Google Scholar 

  10. V. A. Gribkov, F. I. Grigor’ev, B. A. Kalin, and V. L. Yakushin, Promising Radiation–Beam Technologies of Material Treatment (Kruglyi God, Moscow, 2001).

    Google Scholar 

  11. A. S. Demin, E. V. Morozov, S. A. Maslyaev, V. N. Pimenov, V. A. Gribkov, E. V. Demina, I. P. Sasinovskaya, V. P. Sirotinkin, G. S. Sprygin, G. G. Bondarenko, A. N. Tikhonov, and A. I. Gaidar, “Influence of power flows of deuterium ions and deuterium plasma on the structural state of a surface titanium layer,” Fiz. Khim. Obrab. Mater., No. 6, 42–50 (2016).

    Google Scholar 

  12. J. R. Asay, L. P. Mix, and F. C. Perry, “Ejection of material from shocked surfaces,” Appl. Phys. Lett. 29 (5), 284–287 (1976).

    Article  Google Scholar 

  13. A. L. Mikhailov, V. A. Ogorodnikov, V. S. Sasik, et al., “Experimental and calculation modeling of ejection of particles from shock-loaded surface,” J. Exp. and Theor. Phys. 145 (5), 892–905 (2014).

    Google Scholar 

  14. M. B. Zellner, M. Grover, J. E. Hammerberg, et al., “Effects of shock-breakout pressure on ejection of micron-scale material from shocked tin surfaces,” J. Appl. Phys. 102, P. 013522 (2007).

    Article  Google Scholar 

  15. E. E. Lin, A. L. Mikhailov, and V. N. Khvorostin, “A solid-phase mechanism of shock-wave formation of dust particles of heavy metals,” Tech. Phys. Let. 42 (8), 804–805 (2016).

    Article  Google Scholar 

  16. L. I. Ivanov, I. V. Borovitskaya, A. I. Dedyurin, S. A. Maslyaev, O. N. Krokhin, V. Ya. Nikulin, A. A. Tikhomirov, I. V. Yaminskii, and O. V. Sinitsina, “Composition and morphology of a sapphire surface after pulsed treatment by high-temperature plasma,” Fiz. Khim. Obrab. Mater., No. 1, 32–37 (2008).

    Google Scholar 

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Correspondence to I. V. Borovitskaya.

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Original Russian Text © I.V. Borovitskaya, V.N. Pimenov, V.A. Gribkov, M. Padukh, G.G. Bondarenko, A.I. Gaidar, V.V. Paramonova, E.V. Morozov, 2017, published in Metally, 2017, No. 6, pp. 30–37.

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Borovitskaya, I.V., Pimenov, V.N., Gribkov, V.A. et al. Structural Changes in the Vanadium Sample Surface Induced by Pulsed High-Temperature Deuterium Plasma and Deuterium Ion Fluxes. Russ. Metall. 2017, 928–935 (2017). https://doi.org/10.1134/S0036029517110064

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  • DOI: https://doi.org/10.1134/S0036029517110064

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