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Fabrication, Morphological, and Thermal Investigation of Epoxy-Polyamide Nanocomposites Reinforced with Carbon Nanotubes

  • PHYSICAL CHEMISTRY OF NANOCLUSTERS, SUPRAMOLECULAR STRUCTURES, AND NANOMATERIALS
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Abstract

Epoxy-polyamide CNTs reinforced nanocomposites have the excessive ability for their uniform structures and specific properties and have considerable attention owing to their potential applications. In this work, epoxy/polyamide (ER-PA) and CNTs reinforced epoxy/polyamide (ER-PA/CNTs) nanocomposites were prepared by using the solution casting method. Herein, Fourier transforms infrared spectroscopy (FT-IR) was applied to indicate the responsible functional groups, presented in the prepared nanocomposites. Surface morphology and particle dispersion of the prepared nanocomposites were examined by scanning electron microscopy (SEM). The obtained results demonstrated that the CNT’s weight content, dispersion rates, and the surface functionalization of CNTs nanoparticles have a strong influence on the surface morphology of the prepared nanocomposites. The thermal properties and crystalline nature of the ER-PA/CNTs nanocomposites were studied by using thermogravimetric analysis (TGA) and X-ray diffraction (XRD) analyses. The prepared nanocomposites showed good thermal stability and crystalline behavior as compared to the ER-PA nanocomposites network system. From the obtained results, it can be assumed that this effort can help to design other reinforced nanocomposites for promising applications in the nanocomposites materials industry.

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REFERENCES

  1. A. K. Pathak and S. R. Dhakate, J. Polym. Sci. 59, 84 (2021).

    Article  CAS  Google Scholar 

  2. A. K. Pathak, M. Borah, A. Gupta, T. Yokozeki, and S. R. Dhakate, Compos. Sci. Technol. 135, 28 (2016).

    Article  CAS  Google Scholar 

  3. Z. A. Sheikh, N. Ali, F. Ali, A. Ali, G. Shabir, and M. Bilal, J. Polymer Res. 28, 1 (2021).

    Article  Google Scholar 

  4. K. Ramachandran, V. Boopalan, J. C. Bear, and R. Subramani, J. Mater. Sci., 1 (2021).

  5. S. Wang, Z. Liang, T. Liu, B. Wang, and C. Zhang, Nanotechnology 17, 1551 (2006).

    Article  CAS  PubMed  Google Scholar 

  6. F. L. Jin, X. Li, and S. J. Park, J. Ind. Eng. Chem. 29, 1 (2015).

    Article  CAS  Google Scholar 

  7. J. Yu, X. Huang, L. Wang, P. Peng, C. Wu, X. Wu, and P. Jiang, Polym. Chem. 2, 1380 (2011).

    Article  CAS  Google Scholar 

  8. Z. Khan, F. Ali, A. Said, U. Arif, K. Khan, N. Ali, et al., Environ. Res. 215, 114148 (2022).

  9. P. K. Balguri, D. H. Samuel, and U. Thumu, Mater. Today: Proc. 44, 346 (2021).

    CAS  Google Scholar 

  10. J. Shen, W. Huang, L. Wu, Y. Hu, and M. Ye, Compos. Sci. Technol. 67, 3041 (2007).

    Article  CAS  Google Scholar 

  11. W. M. Qian, M. H. Vahid, Y. L. Sun, A. Heidari, R. Barbaz-Isfahani, S. Saber-Samandari, and D. J. Toghraie, Mater. Res. Technol. 12, 1931 (2021).

    Article  CAS  Google Scholar 

  12. B. B. Johnsen, T. R. Frømyr, T. Thorvaldsen, and T. Olsen, Compos. Interfaces 20, 721 (2013).

    Article  CAS  Google Scholar 

  13. A. Mirmohseni and S. Zavareh, Mater. Des. 31, 2699 (2010).

    Article  CAS  Google Scholar 

  14. U. Arif, F. Ali, A. Bahader, S. Ali, A. Zada, and F. Raziq, Inorg. Chem. Commun. 145, 109944 (2022).

  15. Y. Wang and Z. Meng, Carbon 177, 128 (2021).

    Article  CAS  PubMed  PubMed Central  Google Scholar 

  16. S. Khammassi, M. Tarfaoui, and K. Lafdi, J. Compos. Mater. 55, 2617 (2021).

    Article  CAS  Google Scholar 

  17. L. Fei, F. Ali, A. Said, N. Tariq, F. Raziq, N. Ali, et al., Int. J. Environ. Sci. Technol. 20, 1007 (2023).

    Article  CAS  Google Scholar 

  18. G. Demircan, M. Kisa, M. Ozen, and B. Aktas, Iran. Polym. J. 29, 253 (2020).

    Article  CAS  Google Scholar 

  19. J. S. Gan, X. B. Li, U. Arif, F. Ali, A. Ali, F. Raziq, et al., Surf. Interfaces 39, 102938 (2023).

  20. N. Ali, F. Ali, Sh. Saeed, A. Said, Z. Ali Sheikh, S. Muhammad Salman, and M. Bilal, J. Appl. Polym. Sci. 2021, e50646 (2021). https://doi.org/10.1002/app.50646

  21. F. Ali, M. Waseem, R. Khurshid, and A. Afzal, Prog. Org. Coat. 146, 105726 (2020).

  22. S. Mehmood, A. Nisar, A. Farman, H. Fazal, H. Muhammad, F. Shah, Zeitschr. Phys. Chem. 235, 649 (2020).

    Google Scholar 

  23. I. Yasaroglu, O. Aras, and Y. Kaya, Polym. Compos. 43, 1462 (2022).

    Article  CAS  Google Scholar 

  24. F. Ali, N. Ali, M. Altaf, A. Said, S. S. Shah, and M. Bilal, J. Inorg. Organomet. Polym. Mater. 30, 3869 (2020).

    Article  CAS  Google Scholar 

  25. S. A. Xu, G. T. Wang, and Y. W. Mai, J. Mater. Sci. 48, 3546 (2013).

    Article  CAS  Google Scholar 

  26. N. Saba, O. Y. Alothman, Z. Almutairi, and M. Jawaid, Constr. Build. Mater. 201, 138 (2019).

    Article  CAS  Google Scholar 

  27. N. Ali, F. Ali, A. Said, S. Khurshid, Z. Ali Sheikh, U. Ali, Ph. Nguyen-Tri, and M. Bilal, J. Appl. Polym. Sci. 2021, e51310 (2021). https://doi.org/10.1002/app.51310

  28. M. K. Shukla and K. Sharma, Mater. Res. Express 6, 125323 (2019).

  29. M. Tomić, B. Dunjić, M. S. Nikolić, et al., Prog. Org. Coat. 131, 311 (2019).

    Article  Google Scholar 

  30. W. Wang, W. Dong, G. Tian, et al., Powder Technol. 354, 1 (2019).

    Article  CAS  Google Scholar 

  31. A. Afzal, H. M. Siddiqi, N. Iqbal, and Z. Ahmad, J. Therm. Anal. Calorim. 111, 247 (2013).

    Article  CAS  Google Scholar 

  32. F. Ali, N. Ishfaq, A. Said, Z. Nawaz, Z. Ali, N. Ali, A. Afzal, and M. Bilal, Prog. Org. Coat. 150, 105962 (2021).

  33. X. Liu, W. Liu, Q. Xia, J. Feng, Y. Qiu, and F. Xu, Composites, Part A 121, 123 (2019).

    Article  CAS  Google Scholar 

  34. N. M. Nurazzi, F. A. Sabaruddin, M. M. Harussani, S. H. Kamarudin, M. Rayung, M. R. M. Asyraf, and A. Khalina, Nanomaterials 11, 2186 (2021).

    Article  CAS  PubMed  PubMed Central  Google Scholar 

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Funding

The author is also thankful for the support from Key Laboratory of Regional Resource Exploitation and Medicinal Research, project nos. LPRK201909 and LPRK202101, National and Local Joint Engineering Research Center for Mineral Salt Deep Utilization, project no. SF201801, Jiangsu Province College Students’ Innovation and Entrepreneurship Training program, project nos. 202111049338 and 202111049352.

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Correspondence to Song Wang, Farman Ali or Nisar Ali.

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Wang, S., Ali, B., Javed, M. et al. Fabrication, Morphological, and Thermal Investigation of Epoxy-Polyamide Nanocomposites Reinforced with Carbon Nanotubes. Russ. J. Phys. Chem. 97, 3111–3119 (2023). https://doi.org/10.1134/S0036024423130289

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  • DOI: https://doi.org/10.1134/S0036024423130289

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