Abstract
Epoxy-polyamide CNTs reinforced nanocomposites have the excessive ability for their uniform structures and specific properties and have considerable attention owing to their potential applications. In this work, epoxy/polyamide (ER-PA) and CNTs reinforced epoxy/polyamide (ER-PA/CNTs) nanocomposites were prepared by using the solution casting method. Herein, Fourier transforms infrared spectroscopy (FT-IR) was applied to indicate the responsible functional groups, presented in the prepared nanocomposites. Surface morphology and particle dispersion of the prepared nanocomposites were examined by scanning electron microscopy (SEM). The obtained results demonstrated that the CNT’s weight content, dispersion rates, and the surface functionalization of CNTs nanoparticles have a strong influence on the surface morphology of the prepared nanocomposites. The thermal properties and crystalline nature of the ER-PA/CNTs nanocomposites were studied by using thermogravimetric analysis (TGA) and X-ray diffraction (XRD) analyses. The prepared nanocomposites showed good thermal stability and crystalline behavior as compared to the ER-PA nanocomposites network system. From the obtained results, it can be assumed that this effort can help to design other reinforced nanocomposites for promising applications in the nanocomposites materials industry.
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REFERENCES
A. K. Pathak and S. R. Dhakate, J. Polym. Sci. 59, 84 (2021).
A. K. Pathak, M. Borah, A. Gupta, T. Yokozeki, and S. R. Dhakate, Compos. Sci. Technol. 135, 28 (2016).
Z. A. Sheikh, N. Ali, F. Ali, A. Ali, G. Shabir, and M. Bilal, J. Polymer Res. 28, 1 (2021).
K. Ramachandran, V. Boopalan, J. C. Bear, and R. Subramani, J. Mater. Sci., 1 (2021).
S. Wang, Z. Liang, T. Liu, B. Wang, and C. Zhang, Nanotechnology 17, 1551 (2006).
F. L. Jin, X. Li, and S. J. Park, J. Ind. Eng. Chem. 29, 1 (2015).
J. Yu, X. Huang, L. Wang, P. Peng, C. Wu, X. Wu, and P. Jiang, Polym. Chem. 2, 1380 (2011).
Z. Khan, F. Ali, A. Said, U. Arif, K. Khan, N. Ali, et al., Environ. Res. 215, 114148 (2022).
P. K. Balguri, D. H. Samuel, and U. Thumu, Mater. Today: Proc. 44, 346 (2021).
J. Shen, W. Huang, L. Wu, Y. Hu, and M. Ye, Compos. Sci. Technol. 67, 3041 (2007).
W. M. Qian, M. H. Vahid, Y. L. Sun, A. Heidari, R. Barbaz-Isfahani, S. Saber-Samandari, and D. J. Toghraie, Mater. Res. Technol. 12, 1931 (2021).
B. B. Johnsen, T. R. Frømyr, T. Thorvaldsen, and T. Olsen, Compos. Interfaces 20, 721 (2013).
A. Mirmohseni and S. Zavareh, Mater. Des. 31, 2699 (2010).
U. Arif, F. Ali, A. Bahader, S. Ali, A. Zada, and F. Raziq, Inorg. Chem. Commun. 145, 109944 (2022).
Y. Wang and Z. Meng, Carbon 177, 128 (2021).
S. Khammassi, M. Tarfaoui, and K. Lafdi, J. Compos. Mater. 55, 2617 (2021).
L. Fei, F. Ali, A. Said, N. Tariq, F. Raziq, N. Ali, et al., Int. J. Environ. Sci. Technol. 20, 1007 (2023).
G. Demircan, M. Kisa, M. Ozen, and B. Aktas, Iran. Polym. J. 29, 253 (2020).
J. S. Gan, X. B. Li, U. Arif, F. Ali, A. Ali, F. Raziq, et al., Surf. Interfaces 39, 102938 (2023).
N. Ali, F. Ali, Sh. Saeed, A. Said, Z. Ali Sheikh, S. Muhammad Salman, and M. Bilal, J. Appl. Polym. Sci. 2021, e50646 (2021). https://doi.org/10.1002/app.50646
F. Ali, M. Waseem, R. Khurshid, and A. Afzal, Prog. Org. Coat. 146, 105726 (2020).
S. Mehmood, A. Nisar, A. Farman, H. Fazal, H. Muhammad, F. Shah, Zeitschr. Phys. Chem. 235, 649 (2020).
I. Yasaroglu, O. Aras, and Y. Kaya, Polym. Compos. 43, 1462 (2022).
F. Ali, N. Ali, M. Altaf, A. Said, S. S. Shah, and M. Bilal, J. Inorg. Organomet. Polym. Mater. 30, 3869 (2020).
S. A. Xu, G. T. Wang, and Y. W. Mai, J. Mater. Sci. 48, 3546 (2013).
N. Saba, O. Y. Alothman, Z. Almutairi, and M. Jawaid, Constr. Build. Mater. 201, 138 (2019).
N. Ali, F. Ali, A. Said, S. Khurshid, Z. Ali Sheikh, U. Ali, Ph. Nguyen-Tri, and M. Bilal, J. Appl. Polym. Sci. 2021, e51310 (2021). https://doi.org/10.1002/app.51310
M. K. Shukla and K. Sharma, Mater. Res. Express 6, 125323 (2019).
M. Tomić, B. Dunjić, M. S. Nikolić, et al., Prog. Org. Coat. 131, 311 (2019).
W. Wang, W. Dong, G. Tian, et al., Powder Technol. 354, 1 (2019).
A. Afzal, H. M. Siddiqi, N. Iqbal, and Z. Ahmad, J. Therm. Anal. Calorim. 111, 247 (2013).
F. Ali, N. Ishfaq, A. Said, Z. Nawaz, Z. Ali, N. Ali, A. Afzal, and M. Bilal, Prog. Org. Coat. 150, 105962 (2021).
X. Liu, W. Liu, Q. Xia, J. Feng, Y. Qiu, and F. Xu, Composites, Part A 121, 123 (2019).
N. M. Nurazzi, F. A. Sabaruddin, M. M. Harussani, S. H. Kamarudin, M. Rayung, M. R. M. Asyraf, and A. Khalina, Nanomaterials 11, 2186 (2021).
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The author is also thankful for the support from Key Laboratory of Regional Resource Exploitation and Medicinal Research, project nos. LPRK201909 and LPRK202101, National and Local Joint Engineering Research Center for Mineral Salt Deep Utilization, project no. SF201801, Jiangsu Province College Students’ Innovation and Entrepreneurship Training program, project nos. 202111049338 and 202111049352.
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Wang, S., Ali, B., Javed, M. et al. Fabrication, Morphological, and Thermal Investigation of Epoxy-Polyamide Nanocomposites Reinforced with Carbon Nanotubes. Russ. J. Phys. Chem. 97, 3111–3119 (2023). https://doi.org/10.1134/S0036024423130289
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DOI: https://doi.org/10.1134/S0036024423130289