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X-ray reflectivity and photoelectron spectroscopy of superlattices with silicon nanocrystals

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Abstract

The structural properties and features of the chemical composition of SiO x N y /SiO2, SiO x N y /Si3N4, and SiN x /Si3N4 multilayer thin films with ultrathin (1–1.5 nm) barrier SiO2 or Si3N4 layers are studied. The films have been prepared by plasma chemical vapor deposition and have been annealed at a temperature of 1150°С for the formation of silicon nanocrystals in the SiO x N y or SiN x silicon-rich layers with a nominal thickness of 5 nm. The period of superlattices in the studied samples has been estimated by X-ray reflectivity. The phase composition of superlattices has been studied by X-ray electron spectroscopy using the decomposition of photoelectron spectra of the Si 2p, N 1s, and O 1s levels into components corresponding to different charge states of atoms.

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Correspondence to D. M. Zhigunov.

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Original Russian Text © D.M. Zhigunov, I.A. Kamenskikh, A.M. Lebedev, R.G. Chumakov, Yu.A. Logachev, S.N. Yakunin, P.K. Kashkarov, 2017, published in Pis’ma v Zhurnal Eksperimental’noi i Teoreticheskoi Fiziki, 2017, Vol. 106, No. 8, pp. 496–501.

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Zhigunov, D.M., Kamenskikh, I.A., Lebedev, A.M. et al. X-ray reflectivity and photoelectron spectroscopy of superlattices with silicon nanocrystals. Jetp Lett. 106, 517–521 (2017). https://doi.org/10.1134/S0021364017200140

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  • DOI: https://doi.org/10.1134/S0021364017200140

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