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In Situ HRTEM Observation of Electron-Irradiation-Induced Amorphization and Dissolution of the E (Al18Cr2Mg3) Phase in 7475 Al Alloy

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Acta Metallurgica Sinica (English Letters) Aims and scope

Abstract

Electron irradiation effects on phase stability of the E (Al18Cr2Mg3) phase have been investigated by high-angle annular dark-field scanning transmission electron microscopy and high-resolution transmission electron microscopy (HRTEM). The in situ HRTEM observations show that the Al18Cr2Mg3 particles with different thickness undergo amorphization and dissolution under 300 keV electron irradiation at 25 °C. The results indicate that the intermetallic compound Al18Cr2Mg3 is unstable under electron irradiation, and structural changes mainly depend on the thickness of particles. Amorphization in the thick particles is caused by a combination of chemical disordering and an increase in point defect concentration. Dissolution after amorphization in the thin particles is attributed to the diffusion of point defect towards the Al matrix.

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References

  1. T. Nagase, A. Nino, Y. Umakoshi, J. Alloys Compd. 509, S202 (2011)

    Article  Google Scholar 

  2. A.T. Motta, L.M. Howe, P.R. Okamoto, J. Nucl. Mater. 270, 174 (1999)

    Article  Google Scholar 

  3. T. Nagase, A. Nino, Y. Umakoshi, Mater. Sci. Eng. A 449, 1111 (2007)

    Article  Google Scholar 

  4. T. Nagase, A. Sasaki, H.Y. Yasuda, H. Mori, T. Terai, T. Kakeshita, Intermetallics 19, 1313 (2011)

    Article  Google Scholar 

  5. M. Ishimaru, I.T. Bae, Y. Hirotsu, Phys. Rev. B 68, 144102 (2003)

    Article  Google Scholar 

  6. I. Jencic, M.W. Bench, I.M. Robertson, M.A. Kirk, J. Appl. Phys. 78, 974 (1995)

    Article  Google Scholar 

  7. T. Nagase, T. Hosokawa, K. Takizawa, Y. Umakoshia, Intermetallics 17, 657 (2009)

    Article  Google Scholar 

  8. T. Nagase, Y. Umakoshi, Scr. Mater. 48, 1237 (2003)

    Article  Google Scholar 

  9. T. Nagase, T. Hosokawa, Y. Umakoshi, Intermetallics 14, 1027 (2006)

    Article  Google Scholar 

  10. C.W. Allen, R.C. Birtcher, S.E. Donnelly, K. Furuya, N. Ishikawa, M. Song, Appl. Phys. Lett. 74, 2611 (1999)

    Article  Google Scholar 

  11. F. Banhart, Rep. Prog. Phys. 62, 1181 (1999)

    Article  Google Scholar 

  12. K.C. Russell, Prog. Mater Sci. 28, 229 (1984)

    Article  Google Scholar 

  13. N.Q. Lam, M.J. Sabochick, P.R. Okamoto, Radiat. Eff. Defects Solids 129, 91 (1994)

    Article  Google Scholar 

  14. G.W. Iseler, H.I. Dawson, A.S. Mehner, Phys. Rev. 146, 468 (1966)

    Article  Google Scholar 

  15. R.F. Egerton, P. Li, M. Malac, Micron 35, 399 (2004)

    Article  Google Scholar 

  16. S. Samson, Acta Cryst. 11, 851 (1958)

    Article  Google Scholar 

  17. P. Hartel, H. Rose, C. Dinges, Ultramicroscopy 63, 93 (1996)

    Article  Google Scholar 

  18. A.T. Motta, D.R. Olander, Acta Metall. Marer. 38, 2175 (1990)

    Article  Google Scholar 

  19. A.T. Motta, J. Nucl. Mater. 244, 227 (1997)

    Article  Google Scholar 

  20. E.P. Simonen, Nucl. Instrum. Methods B 16, 198 (1986)

    Article  Google Scholar 

  21. A.T. Motta, J.A. Faldowski, L.M. Howe, P.R. Okamoto, Paper presented at the 11th international symposium on Zr in the nuclear industry, Garmisch-Partenkirchen 1996

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Acknowledgments

The work was financially supported by the 111 Project (No. B08040) of China and National Natural Science Foundation of China (No. 51071125).

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Correspondence to Mao-Hua Li.

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Available online at http://link.springer.com/journal/40195

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Li, MH., Yang, YQ., Huang, B. et al. In Situ HRTEM Observation of Electron-Irradiation-Induced Amorphization and Dissolution of the E (Al18Cr2Mg3) Phase in 7475 Al Alloy. Acta Metall. Sin. (Engl. Lett.) 28, 147–151 (2015). https://doi.org/10.1007/s40195-014-0176-6

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  • DOI: https://doi.org/10.1007/s40195-014-0176-6

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