Skip to main content
Log in

The critical water activity from dynamic dewpoint isotherms as an indicator of crispness in low moisture cookies

  • Original Paper
  • Published:
Journal of Food Measurement and Characterization Aims and scope Submit manuscript

Abstract

Low moisture cookie snacks are expected to possess a crisp texture when consumed. If this crispness is lost, the product is deemed unacceptable to the consumer. The most important factors influencing the crispness of low moisture cookies are moisture and temperature. Studies have shown that there exists a critical water activity where desirable crispness will be lost. Typically, this critical water activity would be obtained through an extensive texture study. However, high resolution dynamic isotherm curves have recently been shown to identify critical water activity values (RHc) by sharp inflections in the adsorption curve. The purpose of this study was to determine if the dynamic isotherm curves for low water activity snack cookies could similarly be used to identify an RHc and if this RHc could be used as a stability indicator. Dynamic isotherms, developed for two low moisture cookies at three different temperatures, were used to determine the RHc. Then, samples preconditioned to various water activity values and temperatures were analyzed for crispness. The effect of water activity on crispness was more important than temperature. Cookie samples at water activity values less than RHc maintained their crispness, but suffered an abrupt loss in texture at water activity values higher than RHc, yielding a sigmoidal shaped response. Fermi’s equation for sigmoidal response was used to model the response of crispness to water activity and estimate a critical water activity for texture loss. Both the RHc and Fermi’s critical water activity were found in the range of texture loss, but the RHc corresponded with the initial loss in texture, while Fermi’s critical water activity was at the midpoint of the texture loss. Since the RHc can be obtained with much less labor and time than a texture study and provides an effective indication of the loss of crispness, it was concluded that the RHc provides a viable alternative for determining the critical water activity for crispness.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3

Similar content being viewed by others

Reference

  1. G. Hough, Md Pilar-Buera, J. Chirife, O. Moro, J. Texture Stud. 32(1), 57 (2001)

    Article  Google Scholar 

  2. M.C. Bourne, Effects of water activity on textural properties of food, in Water Activity: Theory and Applications to Food, ed. by L.B. Rockland, L.R. Beuchat (Academic press, New York, 1987), p. 75

    Google Scholar 

  3. J.M. Arimi, E. Duggan, M. OΓÇÖSullivan, J.G. Lyng, E.D. OΓÇÖRiordan, Food Res. Intl. 43, 1650 (2010)

    Article  Google Scholar 

  4. J.F.V. Vincent, J. Sci. Food Agric. 78, 162 (1998)

    Article  CAS  Google Scholar 

  5. S. Sahin, S.G. Sumnu, Physical Properties of Foods (Springer, New York, 2010)

    Google Scholar 

  6. E.E. Katz, T.P. Labuza, J. Food Sci. 46, 403 (1981)

    Article  Google Scholar 

  7. C.S. Gaines, P.L. Finney, A. Kassuba, Cereal Chem. 69, 115 (1992)

    Google Scholar 

  8. E.M. Castro-Prada, C. Primo-Martin, M.B.J. Meinders, R.J. Hamer, Tv Vliet, J. Texture Stud. 40, 127 (2009)

    Article  Google Scholar 

  9. S. Heidenreich, D. Jaros, H. Rohm, A. Ziems, J. Texture Stud. 35, 621 (2004)

    Article  Google Scholar 

  10. R. Tesch, M.D. Normand, M. Peleg, J. Sci. Food Agric. 70, 347 (1996)

    Article  CAS  Google Scholar 

  11. L. Slade, H. Levine, A Food Polymer Science Approach to Structure-Property Relationships in Aqueous Food Systems: Non-Equilibrium Behavior of Carbohydrate-Water Systems, in Water relationships in foods Advances in the 1980s and Trends for the 1990s, ed. by H. Levine, L. Slade (Wiley, New York, 1991), p. 29

    Chapter  Google Scholar 

  12. G. Roudaut, Water Activity and Physical Stability, in Water Activity in Foods, ed. by G. Barbosa-Canovas, A.J. Fontana, S.J. Schmidt, T.P. Labuza (Iowa State Press, Ames, 2007), p. 199

    Chapter  Google Scholar 

  13. M. Peleg, Biotechnol. Prog. 10, 385 (1994)

    Article  CAS  Google Scholar 

  14. P. Pittia, M.C. Nicoli, G. Sacchetti, J. Texture Stud. 38, 116 (2007)

    Article  Google Scholar 

  15. M. Harris, M. Peleg, Cereal Chem. 73, 225 (1996)

    CAS  Google Scholar 

  16. L.N. Bell, T.P. Labuza, Moisture sorption: practical aspects of isotherm measurement and use (American Association of Cereal Chemists, St. Paul, 2000)

    Google Scholar 

  17. T.P. Labuza, B. Altunakar, Water activity prediction and moisture sorption isotherms, in Water Activity in Foods, ed. by G. Barbosa-Canovas, A.J. Fontana, S.J. Schmidt, T.P. Labuza (Wiley, Ames, 2007), p. 109

    Chapter  Google Scholar 

  18. B.P. Carter, A.J. Fontana, Dynamic Dewpoint Isotherm verses Other Moisture Sorption Isotherm Methods (Pullman, Decagon Devices, 2008)

    Google Scholar 

  19. S.J. Schmidt, J.W. Lee, Int. J. Food Prop. 15, 236 (2012)

    Article  Google Scholar 

  20. B.P. Carter, G.S. Campbell, Fundamentals of Moisture Sorption Isotherm (Decagon Devices Inc, Pullman, 2008)

    Google Scholar 

  21. X. Yuan, B.P. Carter, S.J. Schmidt, J. Food Sci. 76, 78 (2011)

    Article  Google Scholar 

  22. B.P. Carter, S.J. Schmidt, Food Chem. 132, 1693 (2012)

    Article  CAS  Google Scholar 

  23. A. Savitsky, M.J.E. Golay, Anal. Chem. 36, 1627 (1964)

    Article  Google Scholar 

  24. M.E. Zabik, S.G. Fierke, D.K. Bristol, Cereal Chem. 56, 29 (1979)

    Google Scholar 

  25. Minitab Inc, Minitab 16 Statistical Software (Minitab Inc, State College, 2010)

    Google Scholar 

  26. B.P. Carter, C.F. Morris, J.A. Anderson, Cereal Chem. 76, 907 (1999)

    Article  CAS  Google Scholar 

  27. Y.H. Roos, Phase Transitions in Foods (Academic Press, San Diego, 1995)

    Google Scholar 

Download references

Acknowledgments

The authors would like to thank Decagon Devices, Inc. for providing the funding for this study. Also, thank you to Andy Galbraith and other support staff at Decagon Devices for facilitating data collection. Thanks is also given to Dr. Craig Morris and the USDA Western Wheat Quality Lab for use of their equipment. Thanks to Dr. Shyam Sablani for providing feedback.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Brady P. Carter.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Carter, B.P., Galloway, M.T., Campbell, G.S. et al. The critical water activity from dynamic dewpoint isotherms as an indicator of crispness in low moisture cookies. Food Measure 9, 463–470 (2015). https://doi.org/10.1007/s11694-015-9254-3

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11694-015-9254-3

Keywords

Navigation