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Microstructure, Mechanical, and Fatigue Strength of Ti-54M Processed by Rotary Swaging

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Abstract

TIMETAL 54M is a newly developed (α + β) titanium alloy with nominal composition Ti-5Al-4V-0.6Mo-0.4Fe. The alloy can provide a cost benefit over Ti-6Al-4V due to improved machinability and formability. In the present work, evolution of mechanical properties in terms of tensile and hardness values is investigated as a function of deformation degrees imposed via rotary swaging (RS). Microstructure, mechanical properties, and fatigue performance of Ti-54M are investigated after severe plastic deformation by RS conducted at 850 °C and after being subjected to two different post-swaging annealing conditions. Optical microscopy and scanning electron microscopy using electron back scatter diffraction were utilized to document the evolution of the microstructure. Tensile tests were conducted to characterize mechanical properties. RS, to a true strain of 3.0, is found to lead to a marked ultrafine-grained structure of about 1 μm grain size with low content of high angle grain boundaries (HAGBs). Post-swaging heat treatment at 800 °C followed by air cooling did not change the grain size but exhibited high content of HAGBs. Post-swaging heat treatment at 940 °C followed by furnace cooling resulted in a grain size of about 5 μm and enhanced work-hardening capability and ductility, which resulted in less fatigue notch sensitivity, but at the same time lower fatigue strength at 107 cycles.

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References

  1. T.S. Srivatsan and M. Kuruvilla, Lisa Park. An investigation of the cyclic fatigue and final behavior of titanium alloy, Key Eng. Mater., 2008, 378–379, p 271–298

    Article  Google Scholar 

  2. V. Venkatesh, Y. Kosaka, J. Fanning, S. Nyakana, in Proceedings of the 11th International World Conference on Titanium (JIMICS5), ed. by M. Niinomi, S. Akiyama, M. Ikeda, M. Hagiwara, K. Maruyama (Kyoto, Japan, 2007), p. 713.

  3. S.L. Nyakana, J.C. Fanning, D.W. Tripp, in Proceedings of the 11th International World Conference on Titanium (JIMICS5), ed. by M. Niinomi, S. Akiyama, M. Ikeda, M. Hagiwara, K. Maruyama (Kyoto, Japan, 2007), p. 749.

  4. Image Taken From Torrington-Machinery, http://www.torrington-machinery.com/images/pic_rotary_swaging1.gifS. Accessed 26 April 2013.

  5. M. Shahzad, Dr.-Ing. Influence of extrusion parameters on microstructure development and mechanical properties in wrought magnesium alloys AZ80 and ZK60 Thesis, TU Clausthal, 2007.

  6. K. Zay, Considering mean stress and environmental effects in understanding the fatigue performance of mechanically surface treated Titanium alloys, Dr.-Ing. Thesis, TU Clausthal, 2011.

  7. W. Wei, K.X. Wei, and Q.N. Shi, Grain refinement of copper sheets through accumulative roll-bonding process at room temperature, Ultrafine Grained Materials IV, Y.T. Zhu, T.G. Langdon, Z. Horita, M.J. Zehetbauer, S.L. Semiatin, and T.C. Lowe, Ed., TMS, Warrendale, 2006, p 209

    Google Scholar 

  8. A.P. Zhilyaev, K. Oh-ishi, G.I. Raab, and T.R. McNelley, Influence of processing parameters on texture and microstructure in ECAPed aluminum. Ultrafine Grained Materials IV, TMS, Warrendale, 2006, p 113

    Google Scholar 

  9. J. Müller, S. Yi, M. Janecek, J. Cizek, and L. Wagner, Effect of equal channel angular pressing on microstructure, texture and high-cycle fatigue performance of wrought magnesium alloys, Int. J. Mater. Res., 2009, 100, p 838

    Article  Google Scholar 

  10. V. Randle and O. Engler, Introduction to texture analysis macrotexture, microtexture and orientation mapping, Gordon and Breach Science, The Netherlands, 2000

    Google Scholar 

  11. F.J. Humphreys and M. Hatherly, Recrystallization and related annealing phenomena, 1st ed., Elsevier, Oxford, 1995

    Google Scholar 

  12. J.I. Goldstein, D.E. Newbury, P.E. Echlin, D.C. Joy, C.E. Lyman, A.D. Romig, C.E. Fiori, and E. Lifshin, Scanning electron microscopy and x-ray microanalysis, Plenum Press, New York, 1992

    Book  Google Scholar 

  13. C. Escher and G. Gottstein, Nucleation of recrystallization in boron doped Ni3Al, Acta Mater., 1998, 46, p 525–539

    Article  Google Scholar 

  14. I.C. Hsiao, S.W. Su, and J.C. Huang, Evolution of texture and grain misorientation in an Al-Mg alloy exhibiting low temperature superplasticity, Metall. Mater. Trans., 2000, 31A, p 2169–2180

    Article  Google Scholar 

  15. T.R. McNelley, D.L. Swisher, and M.T. Perez-Prado, Deformation bands and the formation of grain boundaries in a superplastic aluminum alloy, Metall. Mater. Trans., 2002, 33, p 279–290

    Article  Google Scholar 

  16. X. Huang, Grain orientation effect on microstructure in tensile strained copper, Scr. Mater., 1998, 38, p 1697–1703

    Article  Google Scholar 

  17. K. Sztwertnia and F. Haessner, Orientational aspects of the morphological elements of the microstructure in highly cold rolled pure copper and phosphorous copper, Mater. Sci. Forum, 1994, 157–162, p 1291

    Article  Google Scholar 

  18. G.C. Kaschner and G.T. Gray, III, The influence of crystallographic texture and interstitial impurities on the mechanical behavior of zirconium, Metall. Mater. Trans., 2000, 31A, p 1997–2003

    Article  Google Scholar 

  19. J.J. Fundenberger, M.J. Philippe, F. Wanger, C. Esling, Modelling and prediction of mechanical properties for materials with hexagonal symmetry (zinc, titanium and zirconium alloys, Acta Mater., 1997, 45, p 4041–4055

    Article  Google Scholar 

  20. N. Gey and M. Humbert, Characterization of the variant selection occurring during the α → β → α phase transformations of a cold rolled titanium sheet, Acta Mater., 2002, 50, p 277–287

    Article  Google Scholar 

  21. S.L. Semiatin and T.R. Bieler, Effect of texture and slip mode on the anisotropy of plastic flow and flow softening during hot working of Ti-6Al-4V, Metall. Mater. Trans, 2001, 32A, p 1787–1799

    Article  Google Scholar 

  22. F. Wanger, N. Bozzolo, O. Van Landuyt, and T. Grosdidier, Evolution of recrystallisation texture and microstructure in low alloyed titanium sheets, Acta. Mater., 2002, 50, p 1245–1259

    Article  Google Scholar 

  23. S. Suwas, R.K. Ray, A.K. Singh, and S. Bhargava, Evolution of hot rolling textures in a two-phase (α2 + β) Ti3Al base alloy, Acta Mater., 1999, 47, p 4585–4598

    Article  Google Scholar 

  24. S. Suwas and R.K. Ray, Effect of rolling on textures of primary and secondary alpha(2) produced by thermomechanical processing of the intermetallic alloy Ti-24Al-11Nb, Scr. Mater., 2001, 44, p 275–280

    Article  Google Scholar 

  25. S. Suwas and R.K. Ray, Evolution of texture in the beta(B2) phase of a two phase titanium aluminide intermetallic alloy Ti-24Al-11Nb, Metall. Mater. Trans., 2000, 31A, p 2339–2350

    Article  Google Scholar 

  26. S.L. Seniatin, P.N. Fagin, M.G. Glavicic, I.M. Sukonnik, and O.M. Ivasishin, Influence on texture on beta grain growth during continuous annealing of Ti-6Al-4V Mater, Sci. Eng. A, 2001, 299, p 225–234

    Article  Google Scholar 

  27. S.V. Divinski, V.N. Dnieprenko, and O.M. Ivasishin, Effect of phase transformation on texture formation in Ti-base alloys, Mater. Sci. Eng. A, 1998, 243, p 201–205

    Article  Google Scholar 

  28. Y.N. Wang and J.C. Huang, Texture analysis in hexagonal materials, Mater. Chem. Phys., 2003, 81, p 11–26

    Article  Google Scholar 

  29. E.A. El-Danaf, M.S. Soliman, A.A. Almajid, and M.M. El-Rayes, Enhancement of mechanical properties and grain size refinement of commercial purity aluminum 1050 processed by ECAP, Mater. Sci. Eng. A, 2007, 458, p 226–234

    Article  Google Scholar 

  30. F.H. DallaTorre, E.V. Pereloma, and C.H.J. Davies, Acta Mater., 2006, 54, p 1135

    Article  Google Scholar 

  31. Z.J. Zhang, X.H. An, P. Zhang, M.X. Yang, G. Yang, S.D. Wu, and Z.F. Zhang, Effects of dislocation slip mode on high-cycle fatigue behaviors of ultrafine-grained Cu-Zn alloy processed by equal-channel angular pressing, Scr. Mater., 2013, 68, p 389–392

    Article  Google Scholar 

  32. H. ALkhazraji, M.Z. Salih, Z. Zhong, M. Mhaede, H.-G. Brokmeier, L. Wagner, and N. Schell, Estimation of dislocation density in cold-rolled commercially pure titanium by using synchrotron diffraction, Metall. Mater. Trans. B, 2014, 45, p 1557–1564

    Article  Google Scholar 

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Acknowledgments

The first author would like to thank the Ministry of Higher Education & Scientific Research, Iraq (MoHESR) and the German academic exchange service (DAAD) for supporting his stay at TU Clausthal. The second author would like to acknowledge the partial support by King Saud University, Deanship of Scientific Research, College of Engineering, Research Centre.

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Correspondence to Hasan Al-Khazraji.

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Al-Khazraji, H., El-Danaf, E., Wollmann, M. et al. Microstructure, Mechanical, and Fatigue Strength of Ti-54M Processed by Rotary Swaging. J. of Materi Eng and Perform 24, 2074–2084 (2015). https://doi.org/10.1007/s11665-014-1283-2

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  • DOI: https://doi.org/10.1007/s11665-014-1283-2

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