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Chromatography-mass spectrometry studies of transarylation and disproportionation reactions of diaryl telluroxides

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Abstract

Electrospray ionization chromatography-mass spectrometry was used to study transarylation and disproportionation reactions of di(4-methoxyphenyl) and di(4-dimethylaminophenyl) telluroxides in refluxing toluene. The reaction mixture compositions were established based on the mass spectrometry data and relative retention times. General schemes for fragmentation of the reaction mixture components were suggested.

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Authors and Affiliations

  1. S. P. Korolev Samara National Research University, 34 Moskovskoe shosse, 443086, Samara, Russian Federation

    E. V. Eliseeva, N. A. Red´kin & V. P. Gar´kin

  2. A. N. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences, Korp. 4, 31 Leninsky prosp., 119071, Moscow, Russian Federation

    I. S. Pytskii & A. K. Buryak

Authors
  1. E. V. Eliseeva
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  2. N. A. Red´kin
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  3. V. P. Gar´kin
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  4. I. S. Pytskii
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  5. A. K. Buryak
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Correspondence to E. V. Eliseeva.

Additional information

Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 4, pp. 0636—0642, April, 2017.

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Eliseeva, E.V., Red´kin, N.A., Gar´kin, V.P. et al. Chromatography-mass spectrometry studies of transarylation and disproportionation reactions of diaryl telluroxides. Russ Chem Bull 66, 636–642 (2017). https://doi.org/10.1007/s11172-017-1784-x

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  • DOI: https://doi.org/10.1007/s11172-017-1784-x

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