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One step hydrothermal preparation of NiFe2O4@g-CN nanosheets for low-cost electrode material storage devices

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Abstract

The increasing interest in spinel ferrites due to their notable characteristics including elevated electrochemical stability, redox states and pseudocapacitive activity which make them suitable for application in supercapacitors. The present research involves synthesis of NiFe2O4@g-CN electrode material using hydrothermal route. The various characterization techniques including, electrochemical and physical were used for NiFe2O4 and NiFe2O4@g-CN nanocomposite. The fabricated NiFe2O4@g-CN nanosheet showed exceptional specific capacitance of 740 F/g energy and power density were 38 Wh/Kg and 305 W/Kg respectively at 1 A/g determined from galvanostatic charge discharge plot. The charge transfer resistance (Rct) value of NFO@g-CN (0.23 Ω) exhibited lower value than NFO (0.35 Ω) and g-CN (0.27 Ω). The electrochemical stability test revealed that after 5000th cycle NiFe2O4@g-CN material maintains a very stable structure. Therefore, improvements in electrochemical efficiency of NiFe2O4 because of inclusion of graphitic carbon nitride which provided larger surface area, synergistic interaction and large number of active sites. These finding indicates that electrodes materials have potential material for energy storage device and it can further used in toward water splitting and various energy storage equipment’s.

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Funding

The authors express their gratitude to Princess Nourah bint Abdulrahman University Researchers Supporting Project (Grant No. PNURSP2024R378), Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia. The Deanship of Scientific Research at King Khalid University is greatly appreciated for funding this work under grant number (R.G.P-1/208/44). A.M.A. Henaish thanks the Ministry of Science and Higher Education of the Russian Federation (Ural Federal University Program of Development within the Priority-2030 Program) is gratefully acknowledged.

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Authors and Affiliations

  1. Department of Physics, College of Science, Princess Nourah bint Abdulrahman University, P.O. Box 84428, 11671, Riyadh, Saudi Arabia

    Albandari. W. Alrowaily, B. M. Alotaibi & Haifa A. Alyousef

  2. Centre of Excellence in Solid State Physics, University of the Punjab, Lahore, 54000, Pakistan

    Mahmood Ali

  3. Nuclear Technologies Institute (NTI), King Abdulaziz City for Science & Technology (KACST), P. O. Box 6086, 11442, Riyadh, Saudi Arabia

    Mohammed F. Alotiby

  4. Department of Chemistry, Government College University Lahore, Lahore, 54000, Pakistan

    Muhammad Abdullah

  5. Research Center for Advanced Materials Science (RCAMS), King Khalid University, 61413, Abha, Saudi Arabia

    Abdullah G. Al-Sehemi

  6. Department of Chemistry, College of Science, King Khalid University, 61413, Abha, Saudi Arabia

    Abdullah G. Al-Sehemi

  7. Physics Department, Faculty of Science, Tanta University, Tanta, 31527, Egypt

    A. M. A. Henaish

  8. NANOTECH Center, Ural Federal University, Yekaterinburg, Russia, 620002

    A. M. A. Henaish

  9. School of Chemical Engineering, Yeungnam University, 280 Daehak-ro, Gyeongsan, Gyeongbuk, 38541, Republic of Korea

    Zubair Ahmad

  10. Institute of Physics, Khwaja Fareed University of Engineering and Information Technology, Abu Dhabi Road, Rahim Yar Khan, 64200, Pakistan

    Salma Aman

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  1. Albandari. W. Alrowaily
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Alrowaily, A.W., Alotaibi, B.M., Ali, M. et al. One step hydrothermal preparation of NiFe2O4@g-CN nanosheets for low-cost electrode material storage devices. J Mater Sci: Mater Electron 35, 608 (2024). https://doi.org/10.1007/s10854-024-12362-5

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