Skip to main content

Advertisement

Log in

Hot isostatic pressing of laser powder bed fusion AlSi10Mg: parameter identification and mechanical properties

  • Metal Additive Manufacturing
  • Published:
Journal of Materials Science Aims and scope Submit manuscript

Abstract

The fatigue crack initiation of as built (AB) laser powder bed fusion (LPBF) AlSi10Mg is highly affected by the presence of large porosities inherent to the process. Hot isostatic pressing (HIP) is a potential means of reduction of this detrimental porosity. Classic high temperature HIP treatments at about 500 °C and 100 MPa pressure lead to significant strength loss that is partially recovered after additional solution and ageing heat treatments, i.e. overall a three-step treatment. In this work, a 350 °C HIP treatment performed under a higher pressure of 300 MPa for 2 h has been identified as a promising post-treatment for LPBF AlSi10Mg using finite element method simulations of the HIP process. This treatment is shown to suppress these large porosities and lead to higher fracture strain and total fatigue life than after the classic three-step treatment (HIP + two steps of heat treatment). Both HIP treatments also present higher fracture strain compared to the AB material. Thus, this new 350 °C HIP treatment efficiently removes the need for post-treatments after HIP. The 350 °C at 300 MPa HIP treatment improves the yield strength weighted fatigue resistance compared to the AB material but not the absolute fatigue life.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6
Figure 7
Figure 8
Figure 9
Figure 10
Figure 11

Similar content being viewed by others

References

  1. Leary M (2019) Design for additive manufacturing. Elsevier

    Google Scholar 

  2. Santos Macías JG, Douillard T, Zhao L, Maire E, Pyka G, Simar A (2020) Influence on microstructure, strength and ductility of build platform temperature during laser powder bed fusion of AlSi10Mg. Acta Mat 201:231–243

    Article  Google Scholar 

  3. Zhao L, Santos Macías JG, Ding L, Idrissi H, Simar A (2019) Damage mechanisms in selective laser melted AlSi10Mg under as built and different post-treatment conditions. Mater Sci Eng A 764:138210

    Article  CAS  Google Scholar 

  4. Santos Macías JG, Elangeswaran C, Zhao L, Van Hooreweder B, Adrien J, Maire E, Buffière JY, Ludwig W, Jacques P, Simar A (2019) Ductilisation and fatigue life enhancement of selective laser melted AlSi0Mg by friction stir processing. Scr Mater 170:124–128

    Article  Google Scholar 

  5. Santos Macías JG, Elangeswaran C, Zhao L, Buffière JY, Van Hooreweder B, Simar A (2021) Fatigue crack nucleation and growth in laser powder bed fusion AlSi10Mg under as built and post-treated conditions. Mater Des 210:110084

    Article  Google Scholar 

  6. Romano S, Beretta S, Brandão A, Gumpinger J, Ghidini T (2017) HCF resistance of AlSi10Mg produced by SLM in relation to the presence of defects. Proc Struct Integr 7:101–108

    Google Scholar 

  7. Romano S, Brandão A, Gumpinger J, Gschweitl M, Beretta S (2017) Qualification of AM parts: extreme value statistics applied to tomographic measurements. Mater Des 131:32–48

    Article  Google Scholar 

  8. Nadot Y, Nadot-Martin C, Kan WH, Boufadene S, Foley M, Cairney J, Proust G, Ridosz L (2019) Predicting the fatigue life of an AlSi10Mg alloy manufactured via selective laser melting by using data from computed tomography. Addit Manuf 32:100899

    Google Scholar 

  9. Atkinson HV, Davies S (2012) Fundamental aspects of hot isostatic pressing: an overview. Metall Mater Trans A 31(12):2981–3000

    Article  Google Scholar 

  10. Chastand V, Quaegebeur P, Maia W, Charkaluk E (2018) Comparative study of fatigue properties of Ti–6Al–4V specimens built by electron beam melting (EBM) and selective laser melting (SLM). Mater Charact 143:76–81

    Article  CAS  Google Scholar 

  11. Rosenthal I, Tiferet E, Ganor M, Stern A (2015) Post-processing of AM-SLM AlSi10Mg specimens: mechanical properties and fracture behaviour. Galaty Univ Press

    Google Scholar 

  12. Hirata T, Kimura T, Nakamoto T (2020) Effects of hot isostatic pressing and internal porosity on the performance of selective laser melted AlSi10Mg alloys. Mater Sci Eng A 772:138713

    Article  CAS  Google Scholar 

  13. Rosenthal I, Shneck R, Stern A (2018) Heat treatment effect on the mechanical properties and fracture mechanism in AlSi10Mg fabricated by additive manufacturing selective laser melting process. Mater Sci Eng A 729:310–322

    Article  CAS  Google Scholar 

  14. Uzan NE, Shneck R, Yeheskel O, Frage N (2017) Fatigue of AlSi10Mg specimens fabricated by additive manufacturing selective laser melting (AM-SLM). Mater Sci Eng A 704:229–237

    Article  CAS  Google Scholar 

  15. Finfrock CB, Exil A, Caroll JD, Deibler L (2018) Effect of hot isostatic pressing and powder feedstock on porosity, microstructure, and mechanical properties of selective laser melted AlSi10Mg. Metall Microstruct Anal 7:443–456

    Article  CAS  Google Scholar 

  16. Tradowsky U, White J, Ward RM, Read N, Reimers W, Attallah MM (2016) Selective laser melting of AlSi10Mg: influence of post-processing on the microstructural and tensile properties development. Mater Des 105:212–222

    Article  CAS  Google Scholar 

  17. Ertuğrul O, Öter ZÇ, Yılmaz MS, Şahin E, Coşkun M, Tarakçı G, Koç E (2020) Effect of HIP process and subsequent heat treatment on microstructure and mechanical properties of direct metal laser sintered AlSi10Mg alloy. Rapid Prototyp J 26:1421–1434

    Article  Google Scholar 

  18. Larrosa NO, Wang W, Read N, Loretto MH, Evans C, Carr J, Tradowsky U, Attallah MM, Withers PJ (2018) Linking microstructure and processing defects to mechanical properties of selectively laser melted AlSi10Mg alloy. Theor Appl Fract Mech 98:123–133

    Article  CAS  Google Scholar 

  19. Hastie JC, Kartal ME, Carter LN, Atallah MM, Mulvihill DM (2020) Classifying shape of internal pores within AlSi10Mg alloy manufactured by laser powder bed fusion using 3D X-ray micro computed tomography: influence of processing parameters and heat treatment. Mater Charact 163:110225

    Article  CAS  Google Scholar 

  20. Hastie JC, Koelblin J, Kartal ME, Attalah MM, Martinez R (2021) Evolution of internal pores within AlSi10Mg manufactured by laser powder bed fusion under tension: as-built and heat treated conditions. Mater Des 204:109645

    Article  CAS  Google Scholar 

  21. Kan WH, Nadot Y, Foley M, Ridosz L, Proust G, Cairney JM (2019) Factors that affect the properties of additively manufactured AlSi10Mg: Porosity versus microstructure. Addit Manuf 29:100805

    CAS  Google Scholar 

  22. Schneller W, Leitner M, Leuders S, Sprauel JM, Grün F, Pfeifer T, Jantschner O (2020) Fatigue strength estimation methodology of additively manufactured metallic bulk material. Addit Manuf 39:101688

    Google Scholar 

  23. Schneller W, Leitner M, Springer S, Grün F, Taschauer M (2019) Effect of HIP treatment on microstructure and fatigue strength of selectively laser melted AlSi10Mg. J Manuf Mater Process 3:16

    CAS  Google Scholar 

  24. Tocci M, Pola A, Gelfi M, La Vecchia GM (2020) Effect of a new high-pressure heat treatment on additively manufactured AlSi10Mg alloy. Metall Mater Trans A 51A:4799–4811

    Article  Google Scholar 

  25. Giovagnoli M, Tocci M, Fortini A, Merlin M, Ferroni M, Migliori A, Pola A (2021) Effect of different heat-treatment routes on the impact properties of an additively manufactured AlSi10Mg alloy. Mater Sci Eng A 802:140671

    Article  CAS  Google Scholar 

  26. ABAQUS/Standard User’s Manual Providence, RI (2016)

  27. Uzan NE, Shneck R, Yeheskel O, Frage N (2018) High temperature mechanical properties of AlSi10Mg specimens fabricated by additive manufacturing using selective laser melting technologies (AM-SLM). Addit Manuf 24:257–263

    CAS  Google Scholar 

  28. EOS GmbH-electro optical systems (2014) Material data sheet for EOS aluminium AlSi10Mg, München

  29. Zhou L, Mehta A, Schulz E, McWilliams B, Cho K, Sohn Y (2018) Microstructure, precipitates and hardness of selectively laser melted AlSi10Mg alloy before and after heat treatment. Mater Charact 143:5–17

    Article  CAS  Google Scholar 

  30. Murakami Y (2019) Metal fatigue: effects of small defects and nonmetallic inclusions, 2nd edn. Elsevier, Oxford

    Google Scholar 

  31. Delroisse P (2018) AlSi10Mg lattice structures produced by selective laser melting: from microstructure characterization to impact resistance. PhD Dissertation, Université catholique de Louvain

  32. Galy C, Guen EL, Lacoste E, Arvieu C (2018) Main defects observed in aluminum alloy parts produced by SLM: From causes to consequences. Addit Manuf 22:165–175

    CAS  Google Scholar 

  33. Wu H, Ren Y, Ren J, Liang L, Li R, Fang Q, Cai A, Shan Q, Tian Y, Baker I (2021) Selective laser melted AlSi10Mg alloy under melting mode transition: microstructure evolution, nanomechanical behaviors and tensile properties. J Alloys Compd 873:159823

    Article  CAS  Google Scholar 

Download references

Acknowledgements

The authors acknowledge the support of Guillaume Contzen, Azziz Hocini and Nathan Wiertz.

Funding

JGSM acknowledges the support of the Fonds de la recherche scientifique–FNRS (FRIA grant), Belgium. This research has also been funded (from January 2017) by the European research council (ERC) under the European Union’s Horizon 2020 research and innovation program (grant agreement n°716678). This research work has also been supported from January 2019 by the WALInnov LongLifeAM project, convention n°1810016, funded by the service public de Wallonie économie emploi recherche (SPW-EER).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Aude Simar.

Ethics declarations

Conflict of interest

The authors declare that they have no conflict of interest.

Additional information

Handling Editor: M. Grant Norton.

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Supplementary Information

Below is the link to the electronic supplementary material.

Supplementary file1 (DOCX 616 KB)

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Santos Macías, J.G., Zhao, L., Tingaud, D. et al. Hot isostatic pressing of laser powder bed fusion AlSi10Mg: parameter identification and mechanical properties. J Mater Sci 57, 9726–9740 (2022). https://doi.org/10.1007/s10853-022-07027-9

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10853-022-07027-9

Navigation