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Mössbauer Spectroscopy with High Spatial Resolution: Spotlight on Geoscience

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Modern Mössbauer Spectroscopy

Part of the book series: Topics in Applied Physics ((TAP,volume 137))

Abstract

Mössbauer spectroscopy is an important tool in geoscience. Samples are often small or heterogeneous, requiring measurements with small beam size. Such measurements can be carried out in the laboratory using a radioactive source, or at a synchrotron facility in either time or energy domain. This chapter covers practical aspects of carrying out Mössbauer measurements with high spatial resolution in a tutorial style that covers radioactive source properties, how to choose between time and energy domain, practical aspects associated with preparing the sample and setting up a measurement, useful free software for data analysis and analytical data mapping, and concludes with a showcase of research questions in geoscience that have been addressed using Mössbauer spectroscopy with high spatial resolution.

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Notes

  1. 1.

    Note that NFS is referred to in some regions as synchrotron Mössbauer spectroscopy, which is a time domain method. This should not be confused with the synchrotron Mössbauer source, which is an energy domain method. This chapter uses the acronym SMS to refer to the synchrotron Mössbauer source.

Abbreviations

APS:

Advanced photon source

EFG:

Electric field gradient

ESRF:

European synchrotron radiation facility

FIB:

Focussed ion beam

GIS:

Geographic information system

GKE:

Goldanskii-Karyagin effect

GUI:

Graphical user interface

NFS:

Nuclear forward scattering

PETRA III:

Positron-electron tandem ring accelerator III

QGIS:

Quantum geographic information system

RPS:

Radioactive point source

RCS:

Radioactive conventional source

SMS:

Synchrotron Mössbauer source

SNR:

Signal to noise ratio

SPring-8:

Super photon ring-8 GeV

XANES:

X-ray absorption near-edge structure

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    Catherine McCammon

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McCammon, C. (2021). Mössbauer Spectroscopy with High Spatial Resolution: Spotlight on Geoscience. In: Yoshida, Y., Langouche, G. (eds) Modern Mössbauer Spectroscopy. Topics in Applied Physics, vol 137. Springer, Singapore. https://doi.org/10.1007/978-981-15-9422-9_5

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