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Heat Resistance and Electrophysical Characteristics of Polyheteroarylenes and Ferroelectric–Polymer Film Composites Based on Them

  • Macromolecular Compounds and Polymeric Material
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Abstract

Structurally related poly(amido-o-hydroxy amides) derived from 5,5-methylenebis(2-aminophenol) with tetramethylsiloxane and heteroaromatic (benzoxazole and benzotriazole) fragments incorporated in the second amine component or formed by polyheterocyclization of the corresponding prepolymers were prepared. The effect of modifying fragments introduced into the base poly(o-hydroxy amide) on the heat resistance of powders and films and of films of photosensitive compounds based on the synthesized polymers with the naphthoquinone diazide component was analyzed. The electrophysical parameters of the polymer films and film composites with a nanodispersed ferroelectric filler, (PZT: ceramic powder with the composition Pb0.81Sr0.04Na0.075Bi0.075(Zr0.58 Ti0.42)O3, Russian brand PZT-1), prepared on the basis of modified polymer binders, were determined. Introduction of 20 mol % sulfur-containing fragments into the polymer binder ensures a 50–65˚C increase in the heat resistance for all types of films without increasing the level of the dielectric loss for the composite coatings.

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Authors and Affiliations

  1. Ulyanov (Lenin) St. Petersburg State Electrotechnical University LETI, 197376, St. Petersburg, Russia

    D. A. Chigirev & I. M. Sokolova

  2. Institute of Macromolecular Compounds, St., Russian Academy of Sciences, Russia

    M. N. Bol’shakov, G. K. Lebedeva & A. Yu. Marfichev

  3. St. Petersburg State Institute of Technology (Technical University), 190013, St. Petersburg, Russia

    Yu. V. Shagaiko & L. I. Rudaya

Authors
  1. D. A. Chigirev
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  2. M. N. Bol’shakov
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  3. G. K. Lebedeva
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  4. A. Yu. Marfichev
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  5. Yu. V. Shagaiko
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  6. L. I. Rudaya
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  7. I. M. Sokolova
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Corresponding author

Correspondence to L. I. Rudaya.

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ACKNOWLEDGMENTS

The authors are grateful to Cand. Sci. (Phys.-Math.) I.V. Gofman for the assistance in performing thermal gravimetric analysis of the polymers.

FUNDING

The study was supported by the Ministry of Education and Science of the Russian Federation (government assignment nos. 10.7608.2017/8.9 and 3.3990.2017/4.6).

CONFLICT OF INTERESTS

The authors declare that they have no conflict of interest.

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Chigirev, D.A., Bol’shakov, M.N., Lebedeva, G.K. et al. Heat Resistance and Electrophysical Characteristics of Polyheteroarylenes and Ferroelectric–Polymer Film Composites Based on Them. Russ J Appl Chem 93, 188–196 (2020). https://doi.org/10.1134/S1070427220020056

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  • DOI: https://doi.org/10.1134/S1070427220020056

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