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Peculiarities of \(^{57}\)Fe NMR Spectrum in Micro- and Nanocrystalline Europium Orthoferrites

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Abstract

NMR spectra of \(^{57}\)Fe dispersed europium orthoferrite in powder samples with micro- and nanocrystalline particles were studied for the first time. The material was synthesized by glycine–nitrate combustion, which allowed to obtain the specimens with granular diameters of 60 nm (nano-\({\text {EuFeO}}_3\)) and \(1.5\,\upmu {\text {m}}\) (micro-\({\text {EuFeO}}_3\)). It was found out that the spectra are more complex than could be expected for a compound with a single crystallographic position of \({\text {Fe}}^{3+}\) ions, and it was also identified that there is a noticeable difference in samples with different fineness. Assumptions about the possible physical nature of the observed effects are made.

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Acknowledgements

The research was supported by OP RDE project no. CZ.02.2.69/0.0/0.0/16_027/0008495, International Mobility of Researchers at Charles University.

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Authors and Affiliations

  1. Faculty of Mathematics and Physics, Charles University, 18000, Prague 8, Czech Republic

    Anastasia Sklyarova, Helena Štěpánková & Vojtěch Chlan

  2. Hydrogen Energy Laboratory, Ioffe Institute, Saint Petersburg, 194021, Russia

    Vadim I. Popkov

  3. Laboratory of Quantum Electronics, Ioffe Institute, Saint Petersburg, 194021, Russia

    Ivan V. Pleshakov

  4. Faculty of Physics, Saint Petersburg State University, Peterhof, Saint Petersburg, 198504, Russia

    Vladimir V. Matveev

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  1. Anastasia Sklyarova
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  2. Vadim I. Popkov
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Correspondence to Anastasia Sklyarova.

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Sklyarova, A., Popkov, V.I., Pleshakov, I.V. et al. Peculiarities of \(^{57}\)Fe NMR Spectrum in Micro- and Nanocrystalline Europium Orthoferrites. Appl Magn Reson 51, 1701–1710 (2020). https://doi.org/10.1007/s00723-020-01224-y

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  • DOI: https://doi.org/10.1007/s00723-020-01224-y

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