Abstract
The structure and properties of synthesized massive MgB2-based samples subjected to deformation with Bridgman anvils have been studied. Deformation results in the formation of fine-grained structure of the MgB2 phase, enhancement of interconnection of grains, complete disappearance of friable MgB2-phase areas, and abrupt increase in the microhardness.
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E. I. Kuznetsova, S. V. Sudareva, T. P. Krinitsina, Yu. V. Blinova, E. P. Romanov, Yu. N. Akshentsev, M. V. Degtyarev, M. A. Tikhonovskii, and I. F. Kislyak, “Mechanism of the formation and specific features of the structure of massive samples of compound MgB2,” Phys. Met. Metallogr. 115, 175–185 (2014).
M. Kulich, R. L. Flukiger, C. Senatore, M. Tropeano, and R. Piccardo, “Effect of cold high pressure deformation on the properties of ex situ MgB2 wires,” Supercond. Sci. Technol. 26, 105019 (2013).
N. N. Buinov, M. G. Gaidukov, R. A. Karakhanyan, R. R. Romanova, A. I. Uvarov, and A. N. Uksusnikov, “Effect of low-temperature aging before high-temperature aging on the structure and mechanical properties of EI437B alloy,” Fiz. Met. Metalloved. 31, 1230–1236 (1971).
E. N. Popova, S. V. Sudareva, E. P. Romanov, and L. A. Rodionova, “Fine structure of alloyed multi-filamentary composites based on the A3B-type components and its effects on superconducting parameters,” Phys. Met. Metallogr. 78, 520–528 (1994).
G. Giunchi, L. Malpezzi, and N. Masciocchi, “A new crystalline phase of the boron-rich metal-boride family: The Mg2B25 species,” Solid State Sci. 8, 1202–1208 (2006).
Q. G. Yan, Y. Feng, B. Q. Fu, C. F. Liu, P. X. Zhang, X. Z. Wu, L. Zhou, T. Zhao, and A. K. Pradhan, “Effect of synthesis temperature on density and microstructure of MgB2 superconductor at ambient pressure,” J. Mater. Sci. 38, 4893–4898 (2004).
Y. C. Liu, Q. Z. Shi, Q. Zhao, and Z. Q. Ma, “Kinetics analysis for the sintering of bulk MgB2 superconductor,” J. Mater. Sci.: Mater. Electron. 18, 855–861 (2007).
B. Birajdar and O. Eibl, “Microstructure-critical current density model for MgB2 wires and tapes,” J. Appl. Phys. 105, 033903 (2009).
X. Z. Liao, A. Serquis, Y. T. Zhu, J. Y. Huang, L. Civale, D. E. Peterson, F. M. Mueller, and H. F. Xu, “Mg(B,O)2 precipitation in MgB2,” J. Appl. Phys. 93, 6208–6215 (2003).
T. P. Krinitsina, E. I. Kuznetsova, Yu. V. Blinova, D. N. Rakov, Yu. N. Belotelova, S. V. Sudareva, M. V. Degtyarev, and E. P. Romanov, “Structure and stability of superconducting core of single-core MgB2/Cu,Nb tube composite with a high critical current,” Phys. Met. Metallogr. 115, 538–546 (2014).
M. Takahashi and H. Kumakura, “The enhancement of critical current density of powder-in-tube processed MgB2 tapes by pre-heating of Mg and B mixed powder,” Supercond. Sci. Technol. 26, 075007 (2013).
Y. B. Zhang, X. J. Shan, X. W. Bai, T. Y. Liu, H. M. Zhu, and C. B. Cai, “In situ synthesis and current-carrying characteristics of superconducting MgB2-B4C composites with MgB2 fractions ranging from 18% to 85%,” Supercond. Sci. Technol. 25, 095003 (2012).
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Original Russian Text © Yu.N. Akshentsev, M.V. Degtyarev, V.P. Pilyugin, T.P. Krinitsina, E.I. Kuznetsova, Yu.V. Blinova, S.V. Sudareva, E.P. Romanov, 2015, published in Fizika Metallov i Metallovedenie, 2015, Vol. 116, No. 5, pp. 505–510.
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Akshentsev, Y.N., Degtyarev, M.V., Pilyugin, V.P. et al. Effect of deformation with Bridgman anvils on the structure, hardness, and critical current of a massive MgB2-based sample. Phys. Metals Metallogr. 116, 475–481 (2015). https://doi.org/10.1134/S0031918X15050026
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DOI: https://doi.org/10.1134/S0031918X15050026