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Intercalation of biomolecules into NiAl-NO 3 layered double hydroxide films synthesized in situ on anodic alumina/aluminium support

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Abstract

Layered double hydroxide (LDH) films were synthesized in situ on anodic alumina/aluminium (AAO/Al). Glucose oxidase (GOD) and L-ascorbic acid (vitamin C, VC) were intercalated respectively into the in-situ grown LDH films by anion-exchange in aqueous solutions. Dodecylsulfate (SDS) was used to expand the lamellar structure before GOD intercalation into the LDH film. The resulting products were characterized by scanning electron microscopy (SEM), x-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy and thermo gravimetric analysis (TGA). The results showed that VC and GOD were successfully intercalated into the in-situ synthesized LDH film. These biomolecules loaded LDH films could have potential applications in electrode modification, safe storage and effective delivery of bioactive compounds.

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Authors and Affiliations

  1. Department of Environmental Engineering, Peking University, Beijing, 100871, China

    Hua-Zhang Zhao & Ying-Yue Chang

  2. The Key Laboratory of Water and Sediment Sciences, Ministry of Education, Beijing, 100871, China

    Hua-Zhang Zhao & Ying-Yue Chang

  3. School of Natural Sciences, Shandong Polytechnic University, Jinan, 250353, China

    Jing Yang

  4. Shandong Provincial Key Laboratory of Microbial Engineering, College of Food and Bioengineering, Shandong Polytechnic University, Jinan, 250353, China

    Qin-Zheng Yang

Authors
  1. Hua-Zhang Zhao
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  2. Ying-Yue Chang
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  3. Jing Yang
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  4. Qin-Zheng Yang
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Correspondence to Qin-Zheng Yang.

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Zhao, HZ., Chang, YY., Yang, J. et al. Intercalation of biomolecules into NiAl-NO 3 layered double hydroxide films synthesized in situ on anodic alumina/aluminium support. Electron. Mater. Lett. 9, 251–255 (2013). https://doi.org/10.1007/s13391-012-2148-1

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  • DOI: https://doi.org/10.1007/s13391-012-2148-1

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