Abstract
Functionally graded tungsten–copper bimetallic compact with fine microstructure and good mechanical property has been synthesized by employing microwave heating method at a temperature of 800 °C and in a short processing time of 30 min. Scanning electron microscopy and energy dispersive X-ray analysis revealed the graded structure of synthesized sample. The fine microstructure of tungsten in each layer is caused by arrested grain growth because of the short sintering time. The overall relative density of the W/Cu functionally graded sample has reached 87% of the theoretical density. Vickers microhardness measurements, across the length of a compact, show increase in hardness value of the sample with the increase in tungsten content. The experimental hardness values match well with the theoretically calculated hardness values.
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Bever M B and Duwez P F 1972 Mater. Sci. Eng. 10 1
Bykov Y V, Rybakov K I and Semenov V E 2001a J. Phys. D: Appl. Phys. 34 R55
Bykov Y V, Egorov S V, Eremeev A G, Rybakov K I, Semenov V E and Sorokin A A 2001b J. Mater. Sci. 36 131
Demirskyi D, Agrawal D K and Ragulya A 2010 Mater. Lett. 64 1433
Dube C L, Kashyap S C, Dube D C and Agarwal D K 2009a Appl. Phys. Lett. 94 213107–1
Dube C L, Kashyap S C, Dube D C and Agarwal D K 2009b J. Alloys Compd. 488 328
Dube C L, Kashyap S C, Dube D C and Agarwal D K 2013 J. Alloys Compd. 571 75
Itoh Y, Takahashi M and Takano H 1996 Fusion Eng. Des. 31 279
Khirwadkar S S, Singh K P, Patil Y, Khan M S, Buch J J U, Patel A, Tripathi S, Jaman P M, Rangaraj L and Divakar C 2011 Fusion Eng. Des. 86 1736
Larsson C and Oden M 2004 Mater. Sci. Eng. A 382 141
Mondal A, Agrawal D and Upadhyaya A 2010 J. Microwave Power Electromagn. Energy 44 28
Mukhopadhyay A K, Chaudhuri M R, Seal A, Dalui S K, Banerjee M and Phani K K 2001 Bull. Mater. Sci. 24 125
Olevsky E A, German R M and Upadhyaya A 2000 Acta Mater. 48 1167
Pintsuk G and Uytdenhouwen I 2010 Int. J. Refrac. Met. Hard Mater. 28 661
Pintsuk G, Brunings S E, Doring J E, Linke J, Smid I and Xue L 2003 Fusion Eng. Des. 66 237
Sutton W 1992 Mater. Res. Soc. Symp. Proc. 269 3
Wurster S and Pippan R 2009 Scr. Mater. 60 1083
Xu F, Li Y, Hu X, Niu Y, Zhao J and Zhang Z 2012 Mater. Lett. 67 162
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DUBE, C.L., PATIL, Y., KANPARA, S. et al. Microwave synthesis and mechanical characterization of functionally graded material for applications in fusion devices. Bull Mater Sci 37, 1607–1611 (2014). https://doi.org/10.1007/s12034-014-0724-8
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DOI: https://doi.org/10.1007/s12034-014-0724-8