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Determination of brominated vegetable oils in soft drinks by gas liquid chromatography

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Journal of the American Oil Chemists Society

Abstract

A method is described for the qualitative and quantitative determination of brominated vegetable oils in soft drinks. The procedure involves treatment of the brominated oils with sodium methoxide followed by GLC analysis of the resulting methyl esters using methyl pentadecanoate as internal standard. Recoveries on known amounts of these oils ranged between 93.7% and 102.4%. The technique, applied to several commercial soft drinks, has shown the content of brominated oil to be in the range 10–45 mg per 10 fluid oz of drink.

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References

  1. Lehman, A. J., “Brominated Olive Oil and Carbonated Beverages,” Assoc. Food and Drug Off. of U.S., Quart. Bull.20, 71 (1958).

    Google Scholar 

  2. “Office Consolidation of the Food and Drugs Act and of the Food and Drug Regulations,” Canada (1954).

  3. Munro, I. C., E. J. Middleton and H. C. Grice, in press.

  4. Stein, R. A., J. Chromatog.6, 118 (1961).

    Article  CAS  Google Scholar 

  5. Landowne, R. H., and S. R. Lipsky, Nature182, 1731 (1958).

    Article  CAS  Google Scholar 

  6. Koehler, W. R., J. L. Solan and H. T. Hammond, Anal. Biochem.8(3), 353 (1964).

    Article  CAS  Google Scholar 

  7. Hanahan, D. J., J. Lipid Res.6, 350 (1965).

    CAS  Google Scholar 

  8. Rogozinski, M., J. Gas Chromatog.2, 163 (1964).

    CAS  Google Scholar 

  9. Gershon, H., and J. A. A. Renwick, J. Chromatog.28(2), 399 (1967).

    Article  CAS  Google Scholar 

  10. Daniels, N. W. R., D. L. Frafe, P. W. Russell Egitt and J. B. M. Coppock, J. Sci. Food Agr.14, 883 (1963).

    Article  CAS  Google Scholar 

  11. Lindgren, B. O., and C. M. Svahn, Acta. Chem. Scand.20, 211 (1966).

    Article  CAS  Google Scholar 

  12. Grimm, R. A., J. E. Menting, A. J. Skirton and J. K. Weil, JAOCS45, 895 (1968).

    Article  CAS  Google Scholar 

  13. Sgoutas, D., and F. A. Kummerow, Ibid.40, 138 (1963).

    Article  CAS  Google Scholar 

  14. Vogel, A. I., “Practical Organic Chemistry,” Longmans Press, 1956, p. 163.

  15. Woodford, F. P., and C. M. van Gent, J. Lipid Res.1, 188 (1960).

    CAS  Google Scholar 

  16. Khan, N. A., JAOCS30, 355 (1953).

    Article  CAS  Google Scholar 

  17. Khan, N. A., Ibid.33, 219 (1956).

    Article  CAS  Google Scholar 

  18. Ucciani, E., Compt. Rend., Ser. C.263, 164 (1966).

    CAS  Google Scholar 

Download references

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Conacher, H.B.S., Chadha, R.K. & Sahasrabudhe, M.R. Determination of brominated vegetable oils in soft drinks by gas liquid chromatography. J Am Oil Chem Soc 46, 558–560 (1969). https://doi.org/10.1007/BF02633183

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  • DOI: https://doi.org/10.1007/BF02633183

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