Summary
Existing TLC systems for the separation of dianthrone glycosides (sennosides) and anthraquinone glycosides were found unsatisfactory. Separation of these two groups of glycosides was achieved using a conventional TLC development tank and also in a modern VARIO-KS-Chamber at a relative humidity of 32%. The separation in a VARIO-KS-Chamber was superior.
References
J. K. Crellin, J. W. Fairbairn, C. A. Friedmann, H. H. Ryan, J. Pharm. Pharmacol.13, 639 (1961).
P. Duquenois, R. Anton, Ann. Pharm. Fr.26, 607 (1968).
S. A. T. Rizvi, P. G. Gupta, K. K. Kaul Planta Medica19, 222 (1971).
P. P. Rai, O. M. Obayemi, Curr. Sci.47, 457 (1978).
J. W. Faibairn, Pharm. Weekblad.100, 1493 (1965).
T. J. Betts, J. W. Faibairn, V. K. Mital, J. Pharm. Pharmacol.10, 436 (1958).
L. Horhammer, H. Wagner, H. J. Leue, Deut. Apotheker Ztg.99, 1043 (1959).
J. H. Zwaving, J. Chromatogr.35, 562 (1968).
R. Anton, P. Duquenois, Anals. Pharm. Fr.25, 9 (1967).
L. Horhammer, H. Wagner, G. Bittner, Pharm. Ztg.108, 259 (1963).
S. M. Khafagy, A. N. Girgis, S. E. Khayyal, M. A. Helmi, Planta Medica21, 304 (1972).
P. P. Rai, M. Shok, Chromatographia14, 599 (1981).
P. P. Rai, M. Shok, Abs. THA7, 4th Asian Symposium on Medicinal Plants and Spices, Bangkok (1980).
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Rai, P.P., Shok, M. Resolution of dianthrone glycosides and anthraquinone glycosides by thin-layer chromatography. Chromatographia 15, 249–250 (1982). https://doi.org/10.1007/BF02265657
Received:
Accepted:
Issue Date:
DOI: https://doi.org/10.1007/BF02265657