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Engineering properties of four different rocks after heat treatment

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Abstract

The effect of high temperature on engineering properties of rocks has recently become an important topic for geotechnical engineering applications due to the development in geothermal energy extraction, underground coal gasification, disposal of nuclear waste and deep mining applications. This study aims to investigate the engineering properties of four rocks heated at high temperatures and to identify the corresponding mineralogical changes. Two types of sandstone (Beaudesert sandstone and Jimboomba sandstone), basalt and argillite were subjected to a range of temperatures from 25 to 800 °C and their properties such as porosity and point load index were studied through a series of laboratory experiments. The physical and mineralogical alteration of the heated rock specimens were also investigated to better understand the thermally induced processes that occurred in each rock type using the X-Ray Diffraction, Thermogravimetry (TG), Differential Scanning Calorimetry (DSC) and Derivative Thermogravimetry (DTG) techniques. The obtained data indicated the important role of mineral composition in the thermal behaviour of the studied rocks. Noticeable changes in the mineral compositions at the threshold temperature were observed for each rock type. This behaviour was confirmed with TG/DSC/DTG analysis. This temperature-related process resulted in the formation of cracks, an increase in porosity and a decrease in strength. However, the effects of high temperatures on engineering properties were found to be different in the two sandstone types. While Beaudesert sandstone underwent significant weakening at high temperatures, only a slight change in the strength of Jimboomba sandstone was recorded. The threshold temperatures were identified as 400 °C, 400 °C, 500 °C and 300 °C, for the tested Beaudesert sandstone, Jimboomba sandstone, basalt and argillite samples, respectively. The critical temperatures (obtained using a damage coefficient) were found as 570 °C for both Beaudesert sandstone and basalt, and 440 °C for argillite. Analysis of the laboratory data revealed the difference between the threshold temperatures and the critical temperatures. It is recommended to use both threshold temperature and critical temperature parameters to provide more accurate estimations of the temperature range at which rock undergoes significant changes.

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References

  • Abdulagaov I, Abdulagatova Z, Kallaev S, Omarov Z (2019) Heat-capacity measurements of sandstone at high temperatures. Geomech Geophys Geo Energy Geo Resour 5(1):65–85

    Article  Google Scholar 

  • Becattini V, Motmans T, Zappone A, Madonna C, Haselbacher A, Steinfeld A (2017) Experimental investigation of the thermal and mechanical stability of rocks for high-temperature thermal-energy storage. Appl Energy 203:373–389

    Article  Google Scholar 

  • Brotons V, Tomás R, Ivorra S, Alarcón J (2013) Temperature influence on the physical and mechanical properties of a porous rock: San Julian’s calcarenite. Eng Geol 167:117–127

    Article  Google Scholar 

  • Chaki S, Takarli M, Agbodjan W (2008) Influence of thermal damage on physical properties of a granite rock: porosity, permeability and ultrasonic wave evolutions. Constr Build Mater 22(7):1456–1461

    Article  Google Scholar 

  • Darot M, Reuschlé T (2000) Acoustic wave velocity and permeability evolution during pressure cycles on a thermally cracked granite. Int J Rock Mech Min Sci 37(7):1019–1026

    Article  Google Scholar 

  • Delle Piane C, Arena A, Sarout J, Esteban L, Cazes E (2015) Micro-crack enhanced permeability in tight rocks: an experimental and microstructural study. Tectonophysics 665:149–156

    Article  Google Scholar 

  • Ding QL, Ju F, Song SB, Yu BY, Ma D (2016) An experimental study of fractured sandstone permeability after high-temperature treatment under different confining pressures. J Nat Gas Sci Eng 34:55–63

    Article  Google Scholar 

  • Dmitriyev AP, Kuzyayev LS, Protasov YI, Yamsbcbikov VS (1969) Physical properties of rocks at high temperatures. Nedra Press, Moscow

    Google Scholar 

  • Dong Z, Sun Q, Ranjith PG (2019) Surface properties of grayish-yellow sandstone after thermal shock. Environ Earth Sci 78(14):420

    Article  Google Scholar 

  • Duclos R, Paquet J (1991) High-temperature behaviour of basalts—role of temperature and strain rate on compressive strength and Kic toughness of partially glassy basalts at atmospheric pressure. Int J Rock Mech Min Sci Geomech Abstr 28:71–76

    Article  Google Scholar 

  • Ersoy H, Kolaylı H, Karahan M, Karahan HH, Sünnetci MO (2017) Effect of thermal damage on mineralogical and strength properties of basic volcanic rocks exposed to high temperatures. Bull Eng Geol Environ 78(3):1515–1525

    Article  Google Scholar 

  • Fang X, Xu J, Wang P (2018) Compressive failure characteristics of yellow sandstone subjected to the coupling effects of chemical corrosion and repeated freezing and thawing. Eng Geol 233:160–171

    Article  Google Scholar 

  • Faoro I, Elsworth D, Candela T (2016) Evolution of the transport properties of fractures subject to thermally and mechanically activated mineral alteration and redistribution. Geofluids 16(3):396–407

    Article  Google Scholar 

  • Frolova J, Ladygin V, Rychagov S, Zukhubaya D (2014) Effects of hydrothermal alterations on physical and mechanical properties of rocks in the Kuril–Kamchatka Island Arc. Eng Geol 183:80–95

    Article  Google Scholar 

  • Gialanella S, Girardi F, Ischia G, Lonardelli I, Mattarelli M, Montagna M (2010) On the goethite to hematite phase transformation. J Therm Anal Calorim 102(3):867–873

    Article  Google Scholar 

  • Glover P, Baud P, Darot M et al (1995) α/β phase transition in quartz monitored using acoustic emissions. Geophys J Int 120(3):775–782

    Article  Google Scholar 

  • Gratchev I, Kim DH (2016) On the reliability of the strength retention ratio for estimating the strength of weathered rocks. Eng Geol 201:1–5

    Article  Google Scholar 

  • Gratchev I, Shokouhi A, Kim DH, Stead D, Wolter A (2013) Assessment of rock slope stability using remote sensing technique in the Gold Coast area, Australia. In: Paper presented at the 18th Southeast Asian geotechnical & inaugural AGSSEA conference

  • Gratchev I, Pathiranagei SV, Kim DH (2019) Strength properties of fresh and weathered rocks subjected to wetting–drying cycles. Geomech Geophys Geo-Energy Geo-Resour 5(3):211–221

    Article  Google Scholar 

  • Hager I (2014) Sandstone colour change due to the high temperature exposure. In: Paper presented at the advanced materials research

  • Hajpál M, Török A (2004) Mineralogical and colour changes of quartz sandstones by heat. Environ Geol 46(3–4):311–322

    Google Scholar 

  • Hassanzadegan A, Blöcher G, Milsch H, Urpi L, Zimmermann G (2014) The effects of temperature and pressure on the porosity evolution of Flechtinger sandstone. Rock Mech Rock Eng 47(2):421–434

    Article  Google Scholar 

  • Heuze F (1983) High-temperature mechanical, physical and thermal properties of granitic rocks—a review. Int J Rock Mech Min Sci Geomech Abstr 20(1):3–10

    Article  Google Scholar 

  • Hu J, Sun Q, Pan X (2018) Variation of mechanical properties of granite after high-temperature treatment. Arab J Geosci 11(2):43

    Article  Google Scholar 

  • Jiang G, Zuo J, Li L, Ma T, Wei X (2018) The evolution of cracks in Maluanshan granite subjected to different temperature processing. Rock Mech Rock Eng 51(6):1683–1695

    Article  Google Scholar 

  • Keppert M, Fořt J, Trník A, Koňáková D, Vejmelková E, Pokorný J, Černý R (2017) Behavior of sandstones under heat treatment. Int J Thermophys 38(4):60

    Article  Google Scholar 

  • Keshavarz M, Pellet F, Loret B (2010) Damage and changes in mechanical properties of a gabbro thermally loaded up to 1000 °C. Pure Appl Geophys 167(12):1511–1523

    Article  Google Scholar 

  • Kong B, Wang E, Li Z, Wang X, Liu X, Li N, Yang Y (2016) Electromagnetic radiation characteristics and mechanical properties of deformed and fractured sandstone after high temperature treatment. Eng Geol 209:82–92

    Article  Google Scholar 

  • Kong L, Ostadhassan M, Hou X, Mann M, Li C (2019) Microstructure characteristics and fractal analysis of 3D-printed sandstone using micro-CT and SEM-EDS. J Petrol Sci Eng 175:1039–1048

    Article  Google Scholar 

  • Kumari W, Ranjith P, Perera M, Li X, Li L, Chen B, De Silva V (2018) Hydraulic fracturing under high temperature and pressure conditions with micro CT applications: geothermal energy from hot dry rocks. Fuel 230:138–154

    Article  Google Scholar 

  • Kumari W, Beaumont D, Ranjith P, Perera M, Isaka BA, Khandelwal M (2019) An experimental study on tensile characteristics of granite rocks exposed to different high-temperature treatments. Geomech Geophys Geo-Energy Geo-Resour 5(1):47–64

    Article  Google Scholar 

  • Lan J (2009) A study of the mechanical properties of sandstone after cyclic thermal action. M.Sc. thesis, National Cheng Kung University, Taiwan, 4548

  • Li M, Mao X, Cao L, Pu H, Mao R, Lu A (2016) Effects of thermal treatment on the dynamic mechanical properties of coal measures sandstone. Rock Mech Rock Eng 49(9):3525–3539

    Article  Google Scholar 

  • Liu S, Xu J (2015) An experimental study on the physico-mechanical properties of two post-high-temperature rocks. Eng Geol 185:63–70

    Article  Google Scholar 

  • Liu X, Zhang C, Yuan S, Fityus S, Sloan SW, Buzzi O (2016) Effect of high temperature on mineralogy, microstructure, shear stiffness and tensile strength of two Australian mudstones. Rock Mech Rock Eng 49(9):3513–3524

    Article  Google Scholar 

  • Liu J, Li B, Tian W, Wu X (2018) Investigating and predicting permeability variation in thermally cracked dry rocks. Int J Rock Mech Min Sci 103:77–88

    Article  Google Scholar 

  • Liu Z, Shao J, Xie S, Conil N, Talandier J (2019) Mechanical behavior of claystone in lateral decompression test and thermal effect. Rock Mech Rock Eng 52(2):321–334

    Article  Google Scholar 

  • Lu Y, Wang L, Sun X, Wang J (2017) Experimental study of the influence of water and temperature on the mechanical behavior of mudstone and sandstone. Bull Eng Geol Environ 76(2):645–660

    Article  Google Scholar 

  • Mahanta B, Vishal V, Ranjith P, Singh T (2020) An insight into pore-network models of high-temperature heat-treated sandstones using computed tomography. J Nat Gas Sci Eng 77:103227

    Article  Google Scholar 

  • Maruvanchery V, Kim E (2020) Effects of a high temperature (500 °C) on the fracture processes in calcite-cemented sandstone along bedding-plane orientations. Rock Mech Rock Eng 53:955–966

    Article  Google Scholar 

  • McCabe S, Smith B, Warke P (2010) Exploitation of inherited weakness in fire-damaged building sandstone: the ‘fatiguing’of ‘shocked’stone. Eng Geol 115(3–4):217–225

    Article  Google Scholar 

  • Meng T, Liu R, Meng X, Zhang D, Hu Y (2019) Evolution of the permeability and pore structure of transversely isotropic calcareous sediments subjected to triaxial pressure and high temperature. Eng Geol 253:27–35

    Article  Google Scholar 

  • Ozguven A, Ozcelik Y (2014) Effects of high temperature on physico-mechanical properties of Turkish natural building stones. Eng Geol 183:127–136

    Article  Google Scholar 

  • Ranjith P, Viete DR, Chen BJ, Perera MSA (2012) Transformation plasticity and the effect of temperature on the mechanical behaviour of Hawkesbury sandstone at atmospheric pressure. Eng Geol 151:120–127

    Article  Google Scholar 

  • Rao Q, Wang Z, Xie H, Xie Q (2007) Experimental study of mechanical properties of sandstone at high temperature. J Cent South Univ T 14(1):478–483

    Article  Google Scholar 

  • Rathnaweera T, Ranjith P, Gu X et al (2018) Experimental investigation of thermomechanical behaviour of clay-rich sandstone at extreme temperatures followed by cooling treatments. Int J Rock Mech Min Sci 107:208–223

    Article  Google Scholar 

  • Rong G, Peng J, Yao M, Jiang Q, Wong LNY (2018) Effects of specimen size and thermal-damage on physical and mechanical behavior of a fine-grained marble. Eng Geol 232:46–55

    Article  Google Scholar 

  • Shen YJ, Zhang YL, Gao F, Yang GS, Lai XP (2018) Influence of temperature on the microstructure deterioration of sandstone. Energies 11(7):1753

    Article  Google Scholar 

  • Sirdesai N, Mahanta B, Ranjith P, Singh T (2019) Effects of thermal treatment on physico-morphological properties of Indian fine-grained sandstone. Bull Eng Geol Environ 78(2):883–897

    Article  Google Scholar 

  • Somerton WH (1992) Thermal properties and temperature-related behavior of rock/fluid systems. Amsterdam, Netherlands

  • Standards Australia (2005) Methods of testing rocks for engineering purposes: rock porosity and density (AS 4133.2.1.2-2005). Retrieved from SAI Global

  • Standards Australia (2007) Methods of testing rocks for engineering purposes rock strength tests: determination of point load strength index (AS 4133.4.1-2007). Retrieved from SAI Global

  • Sun Q, Zhang W, Su T, Zhu S (2016) Variation of wave velocity and porosity of sandstone after high temperature heating. Acta Geophys 64(3):633–648

    Article  Google Scholar 

  • Sygała A, Bukowska M (2019) Identification of temperature effect on post-critical geomechanical properties of loaded sandstones. Arab J Geosci 12(10):315

    Article  Google Scholar 

  • Takarli M, Prince W, Siddique R (2008) Damage in granite under heating/cooling cycles and water freeze–thaw condition. Int J Rock Mech Min Sci 45(7):1164–1175

    Article  Google Scholar 

  • Tang Y, Okubo S, Xu J, Peng S (2019a) Progressive failure behaviors and crack evolution of rocks under triaxial compression by 3D digital image correlation. Eng Geol 249:172–185

    Article  Google Scholar 

  • Tang ZC, Sun M, Peng J (2019b) Influence of high temperature duration on physical, thermal and mechanical properties of a fine-grained marble. Appl Therm Eng 156:34–50

    Article  Google Scholar 

  • Tian H, Kempka T, Yu S, Ziegler M (2016) Mechanical properties of sandstones exposed to high temperature. Rock Mech Rock Eng 49(1):321–327

    Article  Google Scholar 

  • Tian H, Mei G, Jiang GS, Qin Y (2017) High-temperature influence on mechanical properties of diorite. Rock Mech Rock Eng 50(6):1661–1666

    Article  Google Scholar 

  • Vagnon F, Colombero C, Colombo F, Comina C, Ferrero AM, Mandrone G, Vinciguerra SC (2019) Effects of thermal treatment on physical and mechanical properties of Valdieri Marble-NW Italy. Int J Rock Mech Min Sci 116:75–86

    Article  Google Scholar 

  • Wang F, Frühwirt T, Konietzky H, Zhu Q (2019) Thermo-mechanical behaviour of granite during high-speed heating. Eng Geol 260:105258

    Article  Google Scholar 

  • Wang D, Zhang P, Wei J, Yu C (2020) The seepage properties and permeability enhancement mechanism in coal under temperature shocks during unloading confining pressures. J Nat Gas Sci Eng 77:103242

    Article  Google Scholar 

  • Wawersik WR, Hannum DW (1980) Mechanical behavior of New Mexico rock salt in triaxial compression up to 200 °C. J Geophys Res Solid Earth 85(B2):891–900

    Article  Google Scholar 

  • Wu Z, Qin BD, Chen LJ, Luo YJ (2005) Experimental study on mechanical character of sandstone of the upper plank of coal bed under high temperature. Chin J Rock Mech Eng 24(11):1863–1867

    Google Scholar 

  • Wu Q, Weng L, Zhao Y, Guo B, Luo T (2019a) On the tensile mechanical characteristics of fine-grained granite after heating/cooling treatments with different cooling rates. Eng Geol 253:94–110

    Article  Google Scholar 

  • Wu X, Huang Z, Cheng Z, Zhang S, Song H, Zhao X (2019b) Effects of cyclic heating and LN2-cooling on the physical and mechanical properties of granite. Appl Therm Eng 156:99–110

    Article  Google Scholar 

  • Xiong L, Chen H, Li T, Zhang Y (2018) Experimental study on the uniaxial compressive strength of artificial jointed rock mass specimen after high temperatures. Geomech Geophys Geo Energy Geo Resour 4(3):201–213

    Article  Google Scholar 

  • Xu Y, Sun D, Zeng Z, Lv H (2019) Effect of aging on thermal conductivity of compacted bentonites. Eng Geol 253:55–63

    Article  Google Scholar 

  • Yang SQ, Xu P, Li YB, Huang YH (2017) Experimental investigation on triaxial mechanical and permeability behavior of sandstone after exposure to different high temperature treatments. Geothermics 69:93–109

    Article  Google Scholar 

  • Yang SQ, Yin PF, Huang YH, Cheng JL (2019) Strength, deformability and X-ray micro-CT observations of transversely isotropic composite rock under different confining pressures. Eng Fract Mech 214:1–20

    Article  Google Scholar 

  • Yao M, Rong G, Zhou C, Peng J (2016) Effects of thermal damage and confining pressure on the mechanical properties of coarse marble. Rock Mech Rock Eng 49(6):2043–2054

    Article  Google Scholar 

  • Zhang R-R, Yuan P (2019) Effect of hydrothermal coupling on physical and dynamic mechanical properties of sandstone. Adv Civ Eng 2019:1–14

    Google Scholar 

  • Zhang Q, Zhao J (2013) Determination of mechanical properties and full-field strain measurements of rock material under dynamic loads. Int J Rock Mech Min Sci 60:423–439

    Article  Google Scholar 

  • Zhang Y, Zhao GF (2020) A global review of deep geothermal energy exploration: from a view of rock mechanics and engineering. Geomech Geophys Geo Energy Geo Resour 6(1):4

    Article  MathSciNet  Google Scholar 

  • Zhang L, Mao X, Lu A (2009) Experimental study on the mechanical properties of rocks at high temperature. Sci China Technol Sci 52(3):641–646

    Article  Google Scholar 

  • Zhang Y, Sun Q, Geng J (2017) Microstructural characterization of limestone exposed to heat with XRD, SEM and TG-DSC. Mater Charact 134:285–295

    Article  Google Scholar 

  • Zhang F, Zhao J, Hu D, Skoczylas F, Shao J (2018a) Laboratory investigation on physical and mechanical properties of granite after heating and water-cooling treatment. Rock Mech Rock Eng 51(3):677–694

    Article  Google Scholar 

  • Zhang W, Sun Q, Zhang Y, Xue L, Kong F (2018b) Porosity and wave velocity evolution of granite after high-temperature treatment: a review. Environ Earth Sci 77(9):350

    Article  Google Scholar 

  • Zhang W, Sun Q, Zhu Y, Guo W (2019) Experimental study on response characteristics of micro–macroscopic performance of red sandstone after high-temperature treatment. J Therm Anal Calorim 136(5):1935–1945

    Article  Google Scholar 

  • Zhao Z, Jing H, Shi X, Gao Y (2020) Experimental and numerical research on fracture behaviors of sandstone under different loading rates. Geomech Geophys Geo Energy Geo Resour 6(4):1–17

    Google Scholar 

  • Zheng L, Rutqvist J, Steefel C, Kim K, Chen F, Vilarrasa V, Nakagawa S, Houseworth J, Birkholzer J (2014) Investigation of Coupled processes and impact of high temperature limits in argillite rock. US Department of Energy, Lawrence Berkeley National Laboratory, Berkeley

    Book  Google Scholar 

  • Zhu T, Jing H, Su H, Yin Q, Du M, Han G (2016) Physical and mechanical properties of sandstone containing a single fissure after exposure to high temperatures. Int J Min Sci Technol 26(2):319–325

    Article  Google Scholar 

  • Zhu Z, Tian H, Jiang G, Cheng W (2018) Effects of high temperature on the mechanical properties of Chinese marble. Rock Mech Rock Eng 51(6):1937–1942

    Article  Google Scholar 

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Acknowledgements

The authors would like to acknowledge Miss Yujie Liu for her help with laboratory testing.

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Authors and Affiliations

  1. School of Engineering and Built Environment, Griffith University, Gold Coast Campus, Brisbane, QLD, 4222, Australia

    Savani Vidana Pathiranagei & Ivan Gratchev

  2. Department of Geological Engineering, Lanzhou University, Lanzhou, 730000, China

    Ran Kong

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  1. Savani Vidana Pathiranagei
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  2. Ivan Gratchev
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  3. Ran Kong
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SVP: Conceptualization, Methodology, Software, Validation, Formal analysis, Investigation, Resources, Writing- Original Draft, Visualization, IG: Conceptualization, Methodology, Validation, Resources, Writing- Review & Editing, Supervision, Project administration, RK: Software, Formal analysis.

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Vidana Pathiranagei, S., Gratchev, I. & Kong, R. Engineering properties of four different rocks after heat treatment. Geomech. Geophys. Geo-energ. Geo-resour. 7, 16 (2021). https://doi.org/10.1007/s40948-020-00211-8

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