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Effect of Heat Treatment on Microstructure and Properties of Al-7.0Zn-1.5Cu-1.5Mg-0.1Zr-0.1Ce Alloy

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Abstract

To obtain excellent properties in 7××× series aluminum alloys, the heat treatment process used is an important factor. This needs to be chosen according to the different alloy compositions. A 7××× series aluminum alloy with high zinc content (Zn/Mg > 4, Mg/Cu = 1) was prepared. Studying the heat treatment process of the alloy is important to guide companies in its industrial production. The optimum heat treatment process is explored from a microstructure point of view. The alloy was melted and cast in the laboratory using a metallurgical method. The microstructure, fracture morphology, and mechanical properties of the alloy were examined by metallographic microscopy, scanning electron microscopy, transmission electron microscopy (TEM), and tensile testing. Research on the alloy solution treatment was emphasized. The results showed that the solution effect was optimum at 470 °C × 1 h during a single-stage solution treatment. The recrystallization degree was low when the two-stage solution treatment process was 450 °C × 0.5 h + 475 °C × 0.5 h due to the release of deformation energy at low temperature; at the same time, the second-order solid-solution temperature was high, the solid-solution effect was better than in the single-stage solid-solution treatment, and the comprehensive mechanical properties of the alloy were better.

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References

  1. C. Huang, T. Zhao, F. Gao, Research development of heat-treatment process influence on microstructure and properties for 7××× series aluminum alloys. Mater. Rev. A. 29(12), 98–102 (2015)

    CAS  Google Scholar 

  2. X. Zhang, Y. Deng, Y. Zhang, Development of high strength aluminum. Acta Metall. Sin. 51(3), 257–271 (2015)

    Google Scholar 

  3. J. Zhao, X. Xu, Y. Chen, L. Sun, C. Tan, X. Zhang, Microstructures and properties of ultra-high-strength Al-Zn-Mg-Cu-Zr-Sr alloy with pre-deformation. Chin. J. Rare Metals. 40(12), 1193–1199 (2016)

    Google Scholar 

  4. Y. Qunying, L. Wenyi, Z. Zhiqing, H. Guangjie, L. Xiaoyong, Hot deformation behavior and processing maps of AA7085 aluminum alloy. Rare Metal Mater. Eng. 47(2), 0409–0415 (2018)

    Article  Google Scholar 

  5. H. Wu, S.P. Wen, H. Huang, B.L. Li, X.L. Wu, K.Y. Gao, W. Wang, Z.R. Nie, Effects of homogenization on precipitation of Al3(Er,Zr) particles and recrystallization behavior in a new type Al-Zn-Mg-Er-Zr alloy. Mater. Sci. Eng. A 689, 313–322 (2017)

    Article  CAS  Google Scholar 

  6. X. Da, Z. Li, G. Wang, X. Li, X. Lv, Y. Zhang, Y. Fan, B. Xiong, Phase transformation and microstructure evolution of an ultra-high strength Al-Zn-Mg-Cu alloy during homogenization. Mater. Charact. 131, 285–297 (2017)

    Article  Google Scholar 

  7. H. Lin, L. Ye, L. Sun, T. Xiao, S. Liu, Y. Deng, X. Zhang, Effect of three-step homogenization on microstructure and properties of 7N01 aluminum alloys. Trans. Nonferrous Met. Soc. China 28, 829–838 (2018)

    Article  CAS  Google Scholar 

  8. F. Wang, W. Meng, H. Zhang, Z. Han, Effects of under-aging treatment on microstructure and mechanical properties of squeeze-cast Al-Zn-Mg-Cu alloy. Trans. Nonferrous Met. Soc. China 28, 1920–1927 (2018)

    Article  CAS  Google Scholar 

  9. S. Sun, P. Liu, H. Jiaying, C. Hong, X. Qiao, S. Liu, R. Zhang, W. Chengge, Effect of solid solution plus double aging on microstructural characterization of 7075 Al alloys fabricated by selective laser melting (SLM). Opt. Laser Technol. 114, 158–163 (2019)

    Article  CAS  Google Scholar 

  10. L. Wan, Y.-L. Deng, L.-Y. Ye, Y. Zhang, The natural ageing effect on pre-ageing kinetics of Al-Zn-Mg alloy. J. Alloys Compd. 776, 469–474 (2019)

    Article  CAS  Google Scholar 

  11. Z. Zhang, J. Yu, D. He, Influence of contact solid-solution treatment on microstructures and mechanical properties of 7075 aluminum alloy. Mater. Sci. Eng. A 743, 500–503 (2019)

    Article  CAS  Google Scholar 

  12. F. Hongjie, S. Jie, W. Hongbo, Y. Dengfeng, Effects of trace of Ce element on microstructure and properties of 7136 aluminum alloy. J. Chin. Soc. Rare Earths 34(3), 313–319 (2016)

    Google Scholar 

  13. J. Sun, H. Fang, H. Liu, C. Shi, Effect of trace rare earth Ce on microstructure and properties of 7085 aluminum alloy. J. Chin. Soc. Rare Earths 35(4), 501–507 (2017)

    Google Scholar 

  14. K.G. Krishna, K. Sivaprasad, K. Venkateswarlu, K.C. Hari Kumar, Microstructural evolution and aging behavior of cryorolled Al-4Zn-2 Mg alloy. Mater. Sci. Eng. A 535, 129–135 (2012)

    Article  Google Scholar 

  15. K.S. Ghosh, N. Gao, M.J. Starink, Characterisation of high pressure torsion processed 7150 Al-Zn-Mg-Cu alloy. Mater. Sci. Eng. A 552, 164–171 (2012)

    Article  CAS  Google Scholar 

  16. R. Ghiaasiaan, X. Zeng, S. Shankar, Controlled Diffusion Solidification (CDS) of Al-Zn-Mg-Cu (7050): microstructure, heat treatment and mechanical properties. Mater. Sci. Eng. A 594, 260–277 (2014)

    Article  CAS  Google Scholar 

  17. N. Yazdian, F. Karimzadeh, M. Tavoosi, Microstructural evolution of nanostructure 7075 aluminum alloy during isothermal annealing. J. Alloys Compd. 493, 137–141 (2010)

    Article  CAS  Google Scholar 

  18. D.K. Xu, N. Birbilis, D. Lashansky, P.A. Rometsch, B.C. Muddle, Effect of solution treatment on the corrosion behaviour of aluminium alloy AA7150: optimization for corrosion resistance. Corros. Sci. 53, 217–225 (2011)

    Article  CAS  Google Scholar 

  19. X.M. Li, M.J. Starink, Identification and analysis of intermetallic phases in overaged Zr-containing and Cr-containing Al-Zn-Mg-Cu alloys. J. Alloys Comp. 509, 471–476 (2011)

    Article  CAS  Google Scholar 

  20. H. Lia, P. Chen, Z. Wang, F. Zhu, R. Song, Z. Zheng, Tensile properties, microstructures and fracture behaviors of an Al-Zn-Mg-Cu alloy during ageing after solution treating and cold-rolling. Mater. Sci. Eng. A 742, 798–812 (2019)

    Article  Google Scholar 

  21. H. Li, F. Cao, S. Guo, Y. Ji, D. Zhang, Z. Liu, P. Wang, S. Scudino, J. Sun, Effects of Mg and Cu on microstructures and properties of spray-deposited Al-Zn-Mg-Cu alloys. J. Alloys Compd. 719, 89–96 (2017)

    Article  CAS  Google Scholar 

  22. G. Kaixuan, K. Wang, L. Chen, J. Guo, C. Cui, J. Wang, Micro-plastic deformation behavior of Al-Zn-Mg-Cu alloy subjected to cryocycling treatment. Mater. Sci. Eng. A 742, 672–679 (2019)

    Article  Google Scholar 

  23. S. Qu, M. Li, C. Shi, H. Fang, J. Sun, Homogenizing and solution of Al-8.0Zn-2.3Cu-2.0 Mg-0.2Zr aluminum alloy. Heat Treat. Metals 42(6), 114–118 (2017)

    CAS  Google Scholar 

  24. F. Zhang, X. Wang, W. Yuan, C. Yang, Effects of solution time on microstructures, and properties of 7050 aluminum alloy. J. Hunan Univ. (Nat. Sci.) 45(12), 11–14 (2018)

    Google Scholar 

  25. R. Zhu, Y. Zhang, B. Xiong, Z. Li, X. Li, H. Liu, B. Zhu, F. Wang, Effect of solution treatment on microstructures and mechanical properties of 7136 aluminum alloy. J. Aeronaut. Mater. 32(5), 37–42 (2012)

    CAS  Google Scholar 

  26. W. Sun, Y. Zhang, X. Li, Z. Li, F. Wang, H. Liu, B. Xiong, Effect of solution treatment on microstructures and mechanical properties of 7136 aluminum alloy. J. Aeronaut. Mater. 34(3), 35–41 (2014)

    CAS  Google Scholar 

  27. X. Zhou, Y. Sun, Y. Zhang, W. Wang, Y. He, J. Fu, J. He, Effect of homogenizing treatment on microstructure and mechanical properties of as-cast Al-Mg-Si-Cu alloy. Heat Treat. Met. 42(6), 93–96 (2017)

    CAS  Google Scholar 

  28. A. Rollett, Recrystallization and Related Annealing Phenomena (Elsevier, Amsterdam, 1995)

    Google Scholar 

  29. L.L. Liu, Q.L. Pan, X.D. Wang, S.W. Xiong, The effects of aging treatments on mechanical property and corrosion behavior of spray formed 7055 aluminium alloy. J. Alloys Compd. 735, 261–276 (2018)

    Article  CAS  Google Scholar 

Download references

Funding

This research was funded by Keynote Research and Development Projects of Shandong (No. 2017CXGC0402), Key Projects of Humanities and Social Sciences Program of Colleges and Universities in Shandong (No. J17RZ011), Special Program for the Training of Young Scholars in Social Science Planning of Shandong (No. 17CQXJ03), Science and Technology Project of Colleges and Universities in Shandong (No. J18KB046), and Natural Science Foundation of Shandong Province (Grant No. ZR2017MEM009).

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JC, TL, GW, CW, RC, and DW prepared the Al-Zn-Mg-Cu-Zr-Ce alloy samples and performed the solution treatment system under the supervision of H.F. All authors discussed the results and approved the final manuscript.

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Correspondence to Hongjie Fang.

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Chu, J., Lin, T., Wang, G. et al. Effect of Heat Treatment on Microstructure and Properties of Al-7.0Zn-1.5Cu-1.5Mg-0.1Zr-0.1Ce Alloy. Metallogr. Microstruct. Anal. 9, 312–322 (2020). https://doi.org/10.1007/s13632-020-00639-0

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  • DOI: https://doi.org/10.1007/s13632-020-00639-0

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