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Mechanical, thermal, and fatigue behavior of aloe vera fiber/pistachio shell powder toughened epoxy resin composite

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Abstract

An epoxy resin hybrid composite composed of aloe vera fiber and pistachio shell particles was developed and tested for its mechanical, thermal, and load-bearing properties. The primary aim of this present study was to study the significant effect of adding silane treated aloe vera fiber and pistachio shell particles in the properties of brittle epoxy resin and its composites. The 3-aminopropyltrimethoxysilane was used to treat the surfaces of aloe vera fiber and pistachio shell particles in an aqueous solution and the powerless hand layup process was applied to make composites. In particular, the composites were post-cured in a hot air oven for 12 h to make the composites tougher. The post-cured aloe vera fiber and pistachio shell particle epoxy resin composites were examined in accordance with ASTM standards. The results revealed the PS3 composite outperformed in load-bearing properties. However, the PS4 showed a marginal improvement in wear resistance. Similarly, an increased fatigue resistance was found in an aloe vera fiber and pistachio shell particle composite material PS3 up to 38,725. Adding silane-treated fibers and particles increases both the load-bearing and time-dependent characteristics of the material. Consequently, innovative silane-treated aloe vera and pistachio shell particle reinforcement might be made from biodegradable materials. Using aloe vera fibers and pistachio shell particles, these epoxy bio-composite materials might be employed in a variety of domestic, automotive, structural, and defense applications.

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References

  1. Rangappa SM, Siengchin S, Parameswaranpillai J, Jawaid M, Ozbakkaloglu T (2022) Lignocellulosic fiber reinforced composites: Progress, performance, properties, applications, and future perspectives. Polym Compos 43(2):645–691

    Article  Google Scholar 

  2. Sanjay MR, Madhu P, Jawaid M, Senthamaraikannan P, Senthil S, Pradeep S (2018) Characterization and properties of natural fiber polymer composites: A comprehensive review. J Clean Prod 172:566–581

    Article  Google Scholar 

  3. Prakash VA, Viswanthan R (2019) Fabrication and characterization of echinoidea spike particles and kenaf natural fibre-reinforced Azadirachta-Indica blended epoxy multi-hybrid bio composite. Compos A Appl Sci Manuf 118:317–326

    Article  Google Scholar 

  4. Vinod A, Sanjay MR, Suchart S, Jyotishkumar P (2020) Renewable and sustainable biobased materials: an assessment on biofibers, biofilms, biopolymers and biocomposites. J Clean Prod 258:120978

    Article  Google Scholar 

  5. Ramesh M, Deepa C, Kumar LR, Sanjay MR, Siengchin S (2020) Life-cycle and environmental impact assessments on processing of plant fibres and its bio-composites: a critical review. J Ind Text. 1528083720924730

  6. Neopolean P, Karuppasamy K (2022) Characterization of silane treated Opuntia short fibre and bagasse biosilica toughened epoxy resin composite. Silicon. pp 1–10

  7. Babushkina EA, Belokopytova LV, Grachev AM, Meko DM, Vaganov EA (2017) Variation of the hydrological regime of Bele-Shira closed basin in Southern Siberia and its reflection in the radial growth of Larixsibirica. Reg Environ Change 17(6):1725–1737

    Article  Google Scholar 

  8. ShravanabelagolaNagarajaSetty VK, Govardhan G, MavinkereRangappa S, Siengchin S (2021) Raw and chemically treated bio-waste filled (Limoniaacidissima shell powder) vinyl ester composites: physical, mechanical, moisture absorption properties, and microstructure analysis. J Vinyl Add Tech 27(1):97–107

    Article  Google Scholar 

  9. Prabhu P, Jayabalakrishnan D, Balaji V, Bhaskar K, Maridurai T, Prakash VR (2022) Mechanical, tribology, dielectric, thermal conductivity, and water absorption behaviour of Caryotaurens woven fibre-reinforced coconut husk biochar toughened wood-plastic composite. Biomass Convers Biorefin. pp 1–8

  10. Vinay SS, Sanjay MR, Siengchin S, Venkatesh CV (2021) Effect of Al2O3 nanofillers in basalt/epoxy composites: mechanical and tribological properties. Polym Compos 42(4):1727–1740

    Article  Google Scholar 

  11. Manikandan G, Jaiganesh V, Malarvannan RR, Prakash AV (2021) Mechanical and delamination studies on siliconized chitosan and morinda-citrifolia natural fiber-reinforced epoxy composite in drilling. Polym Compos 42(1):181–190

    Article  Google Scholar 

  12. Ganapathy T, Sathiskumar R, Sanjay MR, Senthamaraikannan P, Saravanakumar SS, Parameswaranpillai J, Siengchin S (2021) Effect of graphene powder on banyan aerial root fibers reinforced epoxy composites. Journal of Natural Fibers 18(7):1029–1036

    Article  Google Scholar 

  13. Sivasaravanan S, Sangeetha M, Prakash S, Reddy TD, Rahul DP (2019) Experimental investigation of composite material laminated with aloe vera fiber in different composite resin. Mater Today: Proceedings 16:832–837

    Google Scholar 

  14. Chaitanya S, Singh I (2018) Ecofriendly treatment of aloe vera fibers for PLA based green composites. Int J Precis Eng Manuf-Green Technol 5(1):143–150

    Article  Google Scholar 

  15. Arun Prakash VR, Viswanathan R (2018) Microwave-shielding behavior of silanized Cu and Cu–Fe3O4 compound particle-reinforced epoxy resin composite in E-, F-, I-, and J-band frequencies. Polym Bull 75(9):4207–4225

    Article  Google Scholar 

  16. Prabhu L, Krishnaraj V, Sathish S, Gokulkumar S, Sanjay MR, Siengchin S (2020) Mechanical and acoustic properties of alkali-treated Sansevieriaehrenbergii/Camellia sinensis fiber–reinforced hybrid epoxy composites: Incorporation of glass fiber hybridization. Appl Compos Mater 27(6):915–933. https://doi.org/10.1007/s10443-020-09840-4

    Article  Google Scholar 

  17. VR AP, Depoures MV (2020) Effect of silicon coupling grafted ferric oxide and e-glass fibre in thermal stability, wear and tensile fatigue behaviour of epoxy hybrid composite. Silicon 12(11):2533–2544

    Article  Google Scholar 

  18. Dinesh T, Kadirvel A, Hariharan P (2020) Thermo-mechanical and wear behaviour of surface-treated pineapple woven fibre and nano-silica dispersed mahua oil toughened epoxy composite. Silicon 12(12):2911–2920

    Article  Google Scholar 

  19. Balaji KV, Shirvanimoghaddam K, Rajan GS, Ellis AV, Naebe M (2020) Surface treatment of basalt fiber for use in automotive composites. Maters Today Chem 17:100334

    Article  Google Scholar 

  20. Ramasamy N, Xavier JF, Ramadoss R, Jayaseelan V, Jayabalakrishnan D (2021) Interfacial performance of treated aluminum and Kevlar fibre on fibre metal laminated composites. In AIP Conf Proc (Vol. 2395, No. 1, p. 020010). AIP Publishing LLC

  21. Ramesh C, Manickam C, Maridurai T, Prakash VR (2017) Dry sliding wear characteristics of heat treated and surface modified hematite particles-EPDXY particulate composite. Rev Romana Mater-Rom J Mater 47(3):401–405

    Google Scholar 

  22. Gokuldass R, Ramesh R (2019) Mechanical strength behavior of hybrid composites tailored by glass/Kevlar fibre-reinforced in nano-silica and micro-rubber blended epoxy. Silicon 11(6):2731–2739

    Article  Google Scholar 

  23. Saravanan R, Sureshbabu A, Maridurai T (2016) Influence of surface modified MWCNT on mechanical and thermal properties of carbon fiber/epoxy resin hybrid nanocomposite. Dig J Nanomater Biostruct 11(4):1303–1309

    Google Scholar 

  24. Hua Y, Gu L, Premaraj S, Zhang X (2015) Role of interphase in the mechanical behavior of silica/epoxy resin nanocomposites. Mater 8(6):3519–3531

    Article  Google Scholar 

  25. KannyTP KM (2013) Surface treatment of sisal fiber composites for improved moisture and fatigue properties. Compos Interfaces 20(9):783–797

    Article  Google Scholar 

  26. Alshahrani H, VR AP (2022) Mechanical, wear, and fatigue behavior of alkali-silane-treated areca fiber, RHA biochar, and cardanol oil-toughened epoxy biocomposite. Biomass Convers Biorefin pp 1–12

  27. Jagadeesh, P., ThyavihalliGirijappa, Y. G., Puttegowda, M., Rangappa, S. M., &Siengchin, S. (2020). Effect of natural filler materials on fiber reinforced hybrid polymer composites: An Overview. J Nat Fibers. pp 1–16

  28. Rangappa SM, Parameswaranpillai J, Siengchin S, Jawaid M, Ozbakkaloglu T (2022) Bioepoxy based hybrid composites from nano-fillers of chicken feather and lignocellulose CeibaPentandra. Sci Rep 12(1):1–18

    Article  Google Scholar 

  29. Jenish I, VeeramalaiChinnasamy SG, Basavarajappa S, Indran S, Divya D, Liu Y, Siengchin S (2020) Tribo-mechanical characterization of carbonized coconut shell micro particle reinforced with Cissusquadrangularis stem fiber/epoxy novel composite for structural application. J Nat Fibers. pp 1–17

  30. ShravanabelagolaNagarajaSetty VK, Goud G, PeramanahalliChikkegowda, S., MavinkereRangappa, S., &Siengchin, S. (2020). Characterization of chemically treated LimoniaAcidissima (wood apple) shell powder: physicochemical, thermal, and morphological properties. J Nat Fibers. pp 1–12

  31. Jayabalakrishnan D, Prabhu P, Iqbal MS, Mugendiran V, Ravi S, Prakash AV (2021) Mechanical, dielectric, and hydrophobicity behavior of coconut shell biochar toughened Caryotaurens natural fiber reinforced epoxy composite. Polym Compos

  32. Arpitha GR, Sanjay MR, Senthamaraikannan P, Barile C, Yogesha B (2017) Hybridization effect of sisal/glass/epoxy/filler based woven fabric reinforced composites. Exp Tech 41(6):577–584

    Article  Google Scholar 

  33. Hemath M, MavinkereRangappa S, Kushvaha V, Dhakal HN, Siengchin S (2020) A comprehensive review on mechanical, electromagnetic radiation shielding, and thermal conductivity of fibers/inorganic fillers reinforced hybrid polymer composites. Polym Compos 41(10):3940–3965

    Article  Google Scholar 

  34. Prakash VA, Rajadurai A (2016) Thermo-mechanical characterization of siliconized E-glass fiber/hematite particles reinforced epoxy resin hybrid composite. Appl Surf Sci 384:99–106

    Article  Google Scholar 

  35. Thiyagu, T. T., Gokilakrishnan, G., Uvaraja, V. C., Maridurai, T., & Prakash, V. R. (2022). Effect of SiO2/TiO2 and ZnO nanoparticle on cardanol oil compatibilized PLA/PBAT biocomposite packaging film. Silicon. pp 1–14

  36. Abhishek S, Sanjay MR, George R, Siengchin S, Parameswaranpillai J, Pruncu CI (2018) Development of new hybrid Phoenix pusilla/carbon/fish bone filler reinforced polymer composites. Journal of the Chinese Advanced Materials Society 6(4):553–560

    Article  Google Scholar 

  37. Ganesan K, Kailasanathan C, Sanjay MR, Senthamaraikannan P, Saravanakumar SS (2018) A new assessment on mechanical properties of jute fiber mat with egg shell powder/nanoclay-reinforced polyester matrix composites. J Nat Fibers

  38. Alsaadi M, Erkliğ A, Albu-khaleefah K (2018) Effect of pistachio shell particle content on the mechanical properties of polymer composite. Arab J Sci Eng 43(9):4689–4696

    Article  Google Scholar 

  39. Gairola S, Gairola S, Sharma H, Rakesh PK (2019) Impact behavior of pine needle fiber/pistachio shell filler based epoxy composite. In J Phys: Conf Ser (Vol. 1240, No. 1, p. 012096). IOP Publishing

  40. Nayak SY, Heckadka SS, Kini UA, Thomas LG, Gupta I (2017) Pistachio shell flakes and flax fibres as reinforcements in polyester based composites. In Int Conf Eng Inf Technol. pp 17–24

  41. Sanjay MR, Siengchin S, Parameswaranpillai J, Jawaid M, Pruncu CI, Khan A (2019) A comprehensive review of techniques for natural fibers as reinforcement in composites: Preparation, processing and characterization. Carbohyd Polym 207:108–121

    Article  Google Scholar 

  42. Madhu P, Sanjay MR, Jawaid M, Siengchin S, Khan A, Pruncu CI (2020) A new study on effect of various chemical treatments on Agave Americana fiber for composite reinforcement: Physico-chemical, thermal, mechanical and morphological properties. Polym Testing 85:106437

    Article  Google Scholar 

  43. Verbruggen S, De Sutter S, Iliopoulos S, Aggelis DG, Tysmans T (2016) Experimental structural analysis of hybrid composite-concrete beams by digital image correlation (DIC) and acoustic emission (AE). J Nondestr Eval 35(1):1–10

    Article  Google Scholar 

  44. Sumrith N, Techawinyutham L, Sanjay MR, Dangtungee R, Siengchin S (2020) Characterization of alkaline and silane treated fibers of ‘water hyacinth plants’ and reinforcement of ‘water hyacinth fibers’ with bioepoxy to develop fully biobased sustainable ecofriendly composites. J Polym Environ 28(10):2749–2760. https://doi.org/10.1007/s10924-020-01810-y

    Article  Google Scholar 

  45. Arun Prakash VR, Xavier JF, Ramesh G, Maridurai T, Kumar KS, Raj R (2020) Mechanical, thermal and fatigue behaviour of surface-treated novel Caryotaurensfibre–reinforced epoxy composite. Biomass Convers Biorefin. pp 1–11

  46. Jayabalakrishnan D, Saravanan K, Ravi S, Prabhu P, Maridurai T, Prakash VR (2021) Fabrication and characterization of acrylonitrile butadiene rubber and stitched E-glass fibre tailored Nano-silica epoxy resin composite. Silicon 13(8):2509–2517

    Article  Google Scholar 

  47. Arun Prakash VR, Rajadurai A (2016) Mechanical, thermal and dielectric characterization of iron oxide particles dispersed glass fiber epoxy resin hybrid composite. Dig J Nanomater Biostruct (DJNB), 11(2)

  48. Rajadurai A (2017) Inter laminar shear strength behavior of acid, base and silane treated E-glass fibre epoxy resin composites on drilling process. Def Technol 13(1):40–46

    Article  MathSciNet  Google Scholar 

  49. Hasselbruch H, Von Hehl A, Zoch HW (2015) Properties and failure behavior of hybrid wire mesh/carbon fiber reinforced thermoplastic composites under quasi-static tensile load. Mater Des 66:429–436

    Article  Google Scholar 

  50. Rahman M, Puneeth M, Aslam DA (2017) Impact properties of glass/Kevlar reinforced with nano clay epoxy composite. Compos B Eng 107:50–61

    Google Scholar 

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Correspondence to Suganya G.

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Suganya G, Senthil kumar S, Jayabalakrishnan D et al. Mechanical, thermal, and fatigue behavior of aloe vera fiber/pistachio shell powder toughened epoxy resin composite. Biomass Conv. Bioref. 14, 3589–3596 (2024). https://doi.org/10.1007/s13399-022-02787-5

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