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Thermal Stability of Nano-Hydroxyapatite Synthesized via Mechanochemical Treatment

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Abstract

Nano-hydroxyapatite powder was synthesized using phosphorus pentoxide and calcium hydroxide as raw materials, through solid-state reaction via mechanochemical method. The properties of the synthesized nano-hydroxyapatite was characterized by X-ray diffraction, scanning electron microscopy, Fourier transform infrared spectroscopy, thermogravimetry and Williamson–Hall method. Also, the effects of heating rate and temperature on the crystallinity phase, morphology, particle size, composition and thermal stability of hydroxyapatite were investigated. The results show that synthesized nano-hydroxyapatite using solid-state method has good thermal stability and performance for biomedical applications.

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Authors and Affiliations

  1. Department of Industrial Engineering, Lenjan Branch, Islamic Azad University, Isfahan, Iran

    Hamid Reza Javadinejad, Mohsen Saboktakin Rizi & Marzieh Ebrahimian

  2. Advanced Materials Research Center, Department of Materials Engineering, Najafabad Branch, Islamic Azad University, Najafabad, Iran

    Hamid Reza Javadinejad

  3. Department of Engineering New Science, Iran University of Industries and Mines, Tehran, Iran

    Eiman Aghababaei Mobarakeh

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  1. Hamid Reza Javadinejad
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  2. Mohsen Saboktakin Rizi
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  3. Eiman Aghababaei Mobarakeh
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  4. Marzieh Ebrahimian
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Correspondence to Hamid Reza Javadinejad or Mohsen Saboktakin Rizi.

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Javadinejad, H.R., Saboktakin Rizi, M., Aghababaei Mobarakeh, E. et al. Thermal Stability of Nano-Hydroxyapatite Synthesized via Mechanochemical Treatment. Arab J Sci Eng 42, 4401–4408 (2017). https://doi.org/10.1007/s13369-017-2498-y

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  • DOI: https://doi.org/10.1007/s13369-017-2498-y

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