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Shear viscosity measurement of highly filled polycarbonate melts using a slit-die rheometer

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Abstract

Viscosity measurement and the flow behavior prediction of reinforced polymer melts have been considered crucial for quality consistency in commercial products where highly filled polymer composites are used. In this study, a slit-die rheometer mounted on an injection molding machine was employed to measure the shear viscosity of a reinforced polymer melt by monitoring the pressure drop in the slit and the ram movement for various melt temperatures and shear rates. Mold filling experiment was also conducted using an injection molding process with two plaque-shaped parts of different thicknesses. Polycarbonate with 40 weight % of glass fibers was investigated in the experiment. A comparative numerical simulation was conducted as well using the measured viscosity in the current study. The pressure drops from the simulation and the experiments were compared, which reveals that the viscosity measured using a slit-die rheometer is relatively accurate.

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References

  • Amano, O. and K. Ainoya, 2000, Pressure dependent viscosity of polymer melts, 2000 ANTEC, Society of Plastics Engineers, Orlando, FL, 2000.

    Google Scholar 

  • Ansari, M., S.G. Hatzikiriakos and E. Mitsoulis, 2012, Slip effects in HDPE flows, J. Non-Newtonian Fluid Mech. 167–168, 18–29.

    Google Scholar 

  • Ansari, M., T. Zisis, S.G. Hatzikiriakos and E. Mitsoulis, 2012, Capillary flow of Low-Density Polyethylene, Polym. Eng. Sci. 52, 649–662.

    Article  CAS  Google Scholar 

  • Autodesk report, 2011, Material testing report (MAT4915, LUPOY GN2403F), Autodesk Moldflow Plastics Labs, Australia.

  • Bagley, E.B., 1957, End corrections in the capillary flow of Polyethylene, J. Appl. Phys. 28, 624–627.

    Article  CAS  Google Scholar 

  • Cross, M.M, 1979, Relation between viscoelasticity and shearthinning behavior in liquids, Rheol. Acta 18, 609–614.

    Article  CAS  Google Scholar 

  • Han, C.D., 1974, On slit- and capillary-die rheometry, Trans. Soc. Rheol. 18, 163–190.

    Article  CAS  Google Scholar 

  • Han, C.D., 1981, Multiphase flow in polymer processing Academic Press, New York.

    Google Scholar 

  • Langelaan, H.C., A.D. Gotsis and A.P. Boer, 1994, On the linearity of the pressure drop during flow of thermotropic LCPs in slits and capillaries, J. Rheo. 38, 1353–1368.

    Article  CAS  Google Scholar 

  • Laun, H.M., 1983, Polymer melt rheology with a slit die, Rheol. Acta 22, 171–185.

    Article  CAS  Google Scholar 

  • Macosko, C.W., 1994, Rheology, VCH Publishers, New York.

    Google Scholar 

  • Mitsoulis, E., S.G. Hatzikiriakos, K. Christodoulou and D. Vlassopoulos, 1998, Sensitivity analysis of Bagley correction to shear and extensional rheology, Rheol. Acta 37, 438–448.

    Article  CAS  Google Scholar 

  • Mitsoulis, E. and S.G. Hatzikiriakos, 2003, Bagley correction: the effect of contraction angle and its prediction, Rheol. Acta 42, 309–320.

    Article  CAS  Google Scholar 

  • Rabinowitsch, R., 1929, Über die Viskosität und Elastizität von Solen, Z. Phys. Chem. A 145, 1–26.

    Google Scholar 

  • Syrjälä, S. and J. Aho, 2012, Capillary rheometry of polymer melts — Simulation and experiment, Korea-Aust. Rheol. J. 24, 241–247.

    Article  Google Scholar 

  • Thomasset, J., P.J. Carreau, B. Sanschagrin and G. Ausias, 2005, Rheological properties of long glass fiber filled polypropylene, J. Non-Newtonian Fluid Mech. 125, 25–34.

    Article  CAS  Google Scholar 

  • Walters, K., 1975, Rheometry, Willy, New York.

    Google Scholar 

  • Williams, M.L., R.F. Landel and J.D. Ferry, 1955, The temperature dependence of relaxation mechanism in amorphous polymers and other glass-formin2g liquids, J. Am. Chem. Soc. 77, 3701–3707.

    Article  CAS  Google Scholar 

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Correspondence to Jeong-Moo Lee.

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Moon, JS., Lee, JM. Shear viscosity measurement of highly filled polycarbonate melts using a slit-die rheometer. Korea-Aust. Rheol. J. 25, 129–135 (2013). https://doi.org/10.1007/s13367-013-0013-x

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  • DOI: https://doi.org/10.1007/s13367-013-0013-x

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