Skip to main content
Log in

Dislocation Reduction of HgCdTe/Si Through Ex Situ Annealing

  • Published:
Journal of Electronic Materials Aims and scope Submit manuscript

Abstract

Current growth methods of HgCdTe/Cd(Se)Te/Si by molecular-beam epitaxy (MBE) result in a dislocation density of mid 106 cm−2 to low 107 cm−2. Although the exact mechanism is unknown, it is well accepted that this high level of dislocation density leads to poorer long-wavelength infrared (LWIR) focal-plane array (FPA) performance, especially in terms of operability. We have conducted a detailed study of ex situ cycle annealing of HgCdTe/Cd(Se)Te/Si material in order to reduce the total number of dislocations present in as-grown material. We have successfully and consistently shown a reduction of one half to one full order of magnitude in the number of dislocations as counted by etch pit density (EPD) methods. Additionally, we have observed a corresponding decrease in x-ray full-width at half-maximum (FWHM) of ex situ annealed HgCdTe/Si layers. Among all parameters studied, the total number of annealing cycles seems to have the greatest impact on dislocation reduction. Currently, we have obtained numerous HgCdTe/Si layers which have EPD values measuring ~1 × 106 cm−2 after completion of thermal cycle annealing. Preliminary Hall measurements indicate that electrical characteristics of the material can be maintained.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. E.P.G. Smith, G. Venzor, Y. Petraitis, M. Liguori, A. Levy, C. Rabkin, J. Peterson, M. Reddy, S. Johnson, and J. Bangs, J. Electron. Mater. 36, 1045 (2007).

    Article  CAS  ADS  Google Scholar 

  2. N. Dhar and M. Tidrow, Proc. SPIE 5564, 34 (2004).

    Article  ADS  Google Scholar 

  3. P. Love, K. Ando, R. Bornfreund, E. Corrales, R. Mills, J. Cripe, N. Lum, J. Rosbeck, and M. Smith, Proc. SPIE 4486, 373 (2002).

    Article  ADS  Google Scholar 

  4. P.S. Wijewarnasuriya, M. Zandian, D. Edwall, W. McLevige, C. Chen, J. Pasko, G. Hildebrandt, A. Chen, J. Arias, A. D’Souza, S. Rujirawat, and S. Sivananthan, J. Electron. Mater. 27, 546 (1998).

    Article  CAS  ADS  Google Scholar 

  5. J. Bajaj, Proc. SPIE 3948, 42 (2000).

    Article  CAS  ADS  Google Scholar 

  6. J.B. Varesi, A.A. Buell, J.M. Pererson, R.E. Bornfreund, M.F. Vilela, W.A. Radford, and S.M. Joshnson, J. Electron. Mater. 32, 661 (2003).

    Article  CAS  ADS  Google Scholar 

  7. D. Gulbransen, S. Black, A. Childs, C. Fletcher, S. Johnson, W. Radford, G. Venzor, J. Sienicki, A. Thompson, J. Griffith, A. Buell, M. Vilela, and M. Newton, Proc. SPIE 5406, 305 (2004).

    Article  ADS  Google Scholar 

  8. G. Brill, S. Velicu, P. Boieriu, Y. Chen, N. Dhar, T. Lee, Y. Selamet, and S. Sivananthan, J. Electron. Mater. 30, 717 (2001).

    Article  CAS  ADS  Google Scholar 

  9. M. Carmody, J. Pasko, D. Edwall, E. Piqutte, M. Kangas, S. Greeman, J. Arias, R. Jacobs, W. Mason, A. Stoltz, Y. Chen, and N. Dhar, J. Electron. Mater. 37, 1184 (2008).

    Article  CAS  ADS  Google Scholar 

  10. K. Jowikowski and A. Rogalski, J. Electron. Mater. 29, 736 (2000).

    Article  CAS  ADS  Google Scholar 

  11. M. Carmody, D. Edwall, J. Ellsworth, J. Arias, M. Grownert, R. Jacobs, L.A. Alemida, J.H. Dinan, Y. Chen, G. Brill, and N.K. Dhar, J. Electron. Mater. 36, 1098 (2007).

    Article  CAS  ADS  Google Scholar 

  12. S.M. Johnson, D.R. Rhiger, J.P. Rosbeck, J.M. Peterson, S.M. Taylor, and M.E. Boyd, J. Vac. Sci. Technol. B 10, 1499 (1992).

    Article  CAS  Google Scholar 

  13. T. Parados, E. Fitzgerald, A. Caster, S. Tobin, J. Marciniec, J. Welsch, A. Hairston, P. Lamarre, J. Riendeau, B. Woodward, S. Hu, M. Reine, and P. Lovecchio, J. Electron. Mater. 36, 1068 (2007).

    Article  ADS  Google Scholar 

  14. P.S. Wijewarnasuriya, Y. Chen, G. Brill, M. Carmody, R. Bailey, J. Arias, and N.K. Dhar, Proc. SPIE, 6206, 620611 (2006).

    Google Scholar 

  15. Y. Chen, S. Farrell, G. Brill, P. Wijewarnasuriya, and N. Dhar, J. Cryst. Growth 310, 5303 (2008).

    Article  CAS  ADS  Google Scholar 

  16. L. He, S.L. Wang, J.R. Yang, M.F. Yu, Y. Wu, X.Q. Chen, W.Z. Fang, Y.M. Qiao, Y. Gui, and J. Chu, J. Cryst. Growth 201/202, 524 (1999).

    Article  CAS  Google Scholar 

  17. S.H. Shin, J.M. Arias, M. Zandian, J.G. Pasko, and R.R. DeWames, Appl. Phys. Lett. 59, 21 (1991).

    Article  Google Scholar 

  18. S.H. Shin, J.M. Arias, D.D. Edwall, M. Zandian, J.G. Pasko, and R.R. DeWames, J. Vac. Sci. Technol. B 10, 1492 (1992).

    Article  CAS  Google Scholar 

  19. T. Sasaki and N. Oda, J. Appl. Phys. 78, 3121 (1995).

    Article  CAS  ADS  Google Scholar 

  20. Y. Chen, G. Brill, and N. Dhar, J. Cryst. Growth 252, 270 (2003).

    Article  CAS  ADS  Google Scholar 

  21. S. Farrell, G. Brill, Y. Chen, P. Wijewarnasuriya, M.V. Rao, N. Dhar, and K. Harris, J. Electron. Mater. 39(1), 43 (2010)

    Google Scholar 

  22. J.D. Benson, P.J. Smith, R.N. Jacobs, J.K. Markunas, M. Jaime-Vasquez, L.A. Almeida, A. Stoltz, L.O. Bubulac, M. Groenert, P.S. Wijewarnasuriya, G. Brill, Y. Chen, and U. Lee, J. Electron. Mater. 38, 1771 (2009).

    Article  CAS  ADS  Google Scholar 

  23. J.D. Benson, R.N. Jacobs, J.K. Markunas, M. Jaime- Vaswuez, P.J. Smith, L.A. Almeida, M. Martinka, M.F. Vilela, and U. Lee, J. Electron. Mater. 37, 1231 (2008).

    Article  CAS  ADS  Google Scholar 

Download references

Acknowledgements

The work at George Mason University is supported by Penn State Electro-Optic Center (EOC) and the Army Research Office (ARO) under Grant Number W911NF-07-2-0055.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to G. Brill.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Brill, G., Farrell, S., Chen, Y.P. et al. Dislocation Reduction of HgCdTe/Si Through Ex Situ Annealing. J. Electron. Mater. 39, 967–973 (2010). https://doi.org/10.1007/s11664-010-1142-3

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11664-010-1142-3

Keywords

Navigation