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Influence of Aging and Thermomechanical Treatments on the Mechanical Properties of a Nanocluster-Strengthened Ferritic Steel

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Abstract

This study investigated the effect of aging and thermomechanical treatments on the mechanical properties of a nanocluster-strengthened ferritic steel, Fe-1.5Mn-2.5Cu-4.0Ni-1.0Al (wt pct). The effect of thermomechanical treatments on the microhardness and tensile properties were measured at room temperature and correlated with microstructural features. Cu-rich precipitates were characterized by transmission electron microscopy and were found to coarsen slowly during long-time aging. The microhardness measurements indicate a typical precipitation hardening behavior during aging at 773 K (500 °C). Tensile tests showed that thermomechanical treatments can improve the mechanical strength and ductility of the nanocluster-strengthened ferritic steel significantly compared with those without the treatments. Fractography results indicated that the high yield strength resulted from precipitation hardening makes the steel more susceptible to grain-boundary decohesion, which can be suppressed by grain refinement. Atmosphere adsorption and diffusion along grain boundaries were found to intensify brittle intergranular fracture, and this embrittlement can be avoided by vacuum heat treatment.

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References

  1. H.R. Habibi Bajguirani: Mater. Sci. Eng. A, 2002, vol. 338, pp. 142-59.

    Article  Google Scholar 

  2. S. Vaynman, D. Isheim, R.P. Kolli, S.P. Bhat, D.N. Seidman, and M.E. Fine: Metall. Mater. Trans. A, 2008, vol. 39A, pp. 363-73.

    Article  CAS  Google Scholar 

  3. S.K. Dhua, D. Mukerjee, and D.S. Sarma: Metall. Mater. Trans. A, 2003, vol. 34A, pp. 241-53.

    Article  CAS  Google Scholar 

  4. M.E. Fine and D. Isheim: Scripta Mater., 2005, vol. 53, pp. 115-18.

    Article  CAS  Google Scholar 

  5. D. Isheim, M.S. Gagliano, M.E. Fine, and D.N. Seidman: Acta Mater., 2006, vol. 54, pp. 841-49.

    Article  CAS  Google Scholar 

  6. E.J. Czyryca, R.E. Link, R.J. Wong, D.A. Aylor, T.W. Montemarano, and J.P. Gudas: Nav. Eng. J., 1990, vol. 102, pp. 63-82.

    Article  Google Scholar 

  7. A.D. Wilson: J. Metals, 1987, vol. 39, pp. 36-38.

    CAS  Google Scholar 

  8. S.W. Thompson, D.J. Colvin, and G. Krauss: Metall. Mater. Trans. A, 1996, vol. 27A, pp. 1557-71.

    Article  CAS  Google Scholar 

  9. M.T. Miglin, J.P. Hirth, A.R. Rosenfield, and W.A.T. Clark: Metal. Trans. A, 1986, vol. 17A, pp. 791-98.

    Article  CAS  Google Scholar 

  10. S.W. Thompson, D.J. Colvin, and G. Krauss: Metal. Trans. A, 1990, vol. 21A, pp. 1493-1507.

    Article  CAS  Google Scholar 

  11. S.K. Dhua, D. Mukerjee, and D.S. Sarma: Metall. Mater. Trans. A, 2001, vol. 32A, pp. 2259-70.

    Article  CAS  Google Scholar 

  12. S.K. Dhua, A. Ray, and D.S. Sarma: Mater. Sci. Eng. A, 2001, vol. 318, pp. 197-210.

    Article  Google Scholar 

  13. G.C. Hwang, S. Lee, J.Y. Yoo, and W.Y. Choo: Mater. Sci. Eng. A, 1998, vol. 252, pp. 256-68.

    Article  Google Scholar 

  14. S. Vaynman, M.E. Fine, S. Lee, and H.D. Espinosa: Scripta Mater., 2006, vol. 55, pp. 351-54.

    Article  CAS  Google Scholar 

  15. S. Vaynman, D. Isheim, M.E. Fine, D.N. Seidman, and S.P. Bhat: 2004 Conf. Proc., vol. 1. New Orleans, LA, AIST and TMS, 2004, pp. 525–30.

  16. D. Isheim and D.N. Seidman: Surf. Interface Anal., 2004, vol. 34, pp. 569-74.

    Article  Google Scholar 

  17. T. Harry and D.J. Bacon: Acta Mater., 2002, vol. 50, pp. 209-22.

    Article  CAS  Google Scholar 

  18. J.H. Shim and Y.W. Choo: Appl. Phys. Lett., 2007, vol. 90, p. 021906.

    Article  Google Scholar 

  19. W.M. Kane, U. Krupp, and C.J. McMahon: Mater. Sci. Eng. A, 2009, vol. 507, pp. 58-60.

    Article  Google Scholar 

  20. C.J. McMahon: Interface Sci., 2004, vol. 12, pp. 141-46.

    Article  CAS  Google Scholar 

  21. S.B. Fisher, J.E. Harbottle, and N. Aldrige: Phil. Trans. R. Soc. Lond. A, 1985, vol. 315, pp. 301-32.

    Article  CAS  Google Scholar 

  22. W.M. Kane, U. Krupp, and C.J. McMahon: Mater. Sci. Eng. A, 2009, vol. 507, pp. 61-65.

    Article  Google Scholar 

  23. C.T. Liu and C.L. White: Acta Metall., 1987, vol. 35, pp. 643-49.

    Article  CAS  Google Scholar 

  24. C.T. Liu, C.L. White, and E.H. Lee: Scripta Metall., 1985, vol. 19, pp. 1247-50.

    Article  CAS  Google Scholar 

  25. M. Takeyama and C.T. Liu: Mater. Sci. Eng. A, 1992, vol. 153, pp. 538-47.

    Article  Google Scholar 

  26. R. Zee, C. Yang, Y.X. Lin, and B. Chin: J. Mater. Sci., 1991, vol. 26, pp. 3853-61.

    Article  CAS  Google Scholar 

  27. J.H. Zhu and C.T. Liu: Intermetallics, 2002, vol. 10, pp. 309-16.

    Article  CAS  Google Scholar 

  28. Z.W. Zhang, C.T. Liu, S. Guo, J.L. Cheng, G. Chen, T. Fujita, M.W. Chen, Y.W. Chung, S. Vaynman, M.E. Fine, and B.A. Chin: Mater. Sci. Eng. A, 2011, vol. 528, pp. 855-59.

    Article  Google Scholar 

  29. M.K. Miller and K.F. Russell: J. Nucl. Mater., 2007, vol. 371, pp. 145-60.

    Article  CAS  Google Scholar 

  30. A. Machova: Mater. Sci. Eng. A, 2001, vols. 319-21, pp. 574-77.

    Google Scholar 

  31. S. Sangal and S. Yannacopoulos: Can. Metall. Q., 1992, vol. 31, pp. 55-61.

    CAS  Google Scholar 

  32. B. Hwang and C.G. Lee: Mater. Sci. Eng. A, 2010, vol. 527, pp. 4341-46.

    Article  Google Scholar 

  33. X.M. Deng, F.S. Ma, and M.A. Sutton: Int. J. Damage Mech., 2005, vol. 14, pp. 101-26.

    Article  CAS  Google Scholar 

  34. C.T. Liu, R.W. Carpenter, and H. Inouye: Metall. Trans. A, 1975, vol. 6A, pp. 419-21.

    CAS  Google Scholar 

  35. U. Krupp, W.M. Kane, C. Laird, and C.J. McMahon: Mater. Sci. Eng. A, 2004, vol. 387, pp. 409-13.

    Article  Google Scholar 

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Acknowledgments

This research was supported mainly by internal funding from Auburn University, Hong Kong City University, and together with the NJUST Research Funding (No. 2010GIPY031) and the National Natural Sciences Foundation of China (No. 50871054). Z.W.Z. benefitted from the Visiting Postdoctoral Research Program at the Neutron Scattering Science Division, Oak Ridge National Laboratory, Oak Ridge, TN.

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Correspondence to C. T. Liu.

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Manuscript submitted February 21, 2011.

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Zhang, Z.W., Liu, C.T., Wen, Y.R. et al. Influence of Aging and Thermomechanical Treatments on the Mechanical Properties of a Nanocluster-Strengthened Ferritic Steel. Metall Mater Trans A 43, 351–359 (2012). https://doi.org/10.1007/s11661-011-0835-4

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