Skip to main content
Log in

In-Situ X-Ray Investigations and Computer Simulation during Continuous Heating of a Ball Bearing Steel

  • Published:
Metallurgical and Materials Transactions A Aims and scope Submit manuscript

Abstract

This article presents a comparison between transformation kinetics obtained by in-situ X-ray diffraction during continuous heating of a ball bearing steel AISI 52100 to austenitizing temperature and computer simulation. In order to have acquisition times short enough for good time resolution, X-ray diffraction experiments were done with special equipment such as a rotating anode producing intense X-ray radiation and an area detector. Computer simulations of austenitizing were performed with a Johnson–Mehl–Avrami equation. Besides transformation kinetics, the lattice parameters of ferrite and austenite were also studied. Lattice parameters measured by in-situ X-ray diffraction match calculations from models. Good agreement between phase contents obtained by simulation and by X-ray diffraction was obtained.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10

Similar content being viewed by others

References

  1. T. Hirsch: HTM Z. Werkst. Waermebeh. Fertigung, 2003, vol. 58, pp. 110–26

    Google Scholar 

  2. F. Hoffmann, O. Kessler, Th. Lübben, P. Mayr: Heat Treatment Met., 2004, vol. 2, pp. 27–30

    Google Scholar 

  3. H. Surm, O. Kessler, M. Hunkel, F. Hoffmann, and P. Mayr: Proc. 2nd Int. Conf. on Thermal Process Modelling and Computer Simulation; S. Denis, P. Archambault, J.M. Berghau, and R. Fortunier: J. Phys. IV, 2004, vol. 120, pp. 111–19

  4. M. Rodriguez: in Industrial Applications of X-ray Diffraction, F.H. Chung and D.K. Smith, eds., Marcel Dekker Inc., New York, NY, 2000, p. 891

  5. A. Rocha, T. Hirsch: Mater. Sci. Eng., 2005, vol. A395, pp. 195–207

    CAS  Google Scholar 

  6. W.G. Wood: Metals Handbook, 9th ed. vol. 5, ASM, Metals Park, OH, 1982, pp. 303–09

    Google Scholar 

  7. R.A. Young: in The Rietveld Method, R.A. Young, ed., IUCr Book Series, Oxford University Press, Oxford, United Kingdom, 1993, pp. 1–39

  8. H. Surm, O. Keßler, M Hunkel, F. Hoffmann, and P. Mayr: Proc. 3rd Int. Conf. on Thermal Process Modelling and Computer Simulation, Budapest, 2006, pp. 26–28

  9. A. Jablonka, K. Harste, K. Schwerdtfeger: Steel Res., 1991, vol. 62, pp. 24–33

    CAS  Google Scholar 

  10. G. Reichelt: Ph.D. Thesis, Technical University of Berlin, Berlin, 1982

  11. V. Hauk: Structural and Residual Stress Analysis by Non-Destructive Methods, Evaluation, Application, Assessment, Elsevier, New York, NY, 1997

    Google Scholar 

  12. J. Gegner: Komplexe Diffusionsprozesse in Metallen, Expert Verlag, Renningen, Germany, 2006, pp. 154–63

  13. D.D.L. Chung, P.W. Dehaven, H. Arnold, D. Ghosh: X-Ray Diffraction at Elevated Temperatures, VCH Publishers, New York, NY, 1993

    Google Scholar 

  14. ASM Ready Reference: Thermal Properties of Metals, ASM INTERNATIONAL, Materials Park, OH, 2002, p. 22

  15. W.B. Pearson: Handbook of Lattice Spacings and Structures of Metals, Metal Physics and Physical Metallurgy, New York, 1964, vol. 4

  16. M. Onink, C.M. Brakman, F.D. Tichelaar, E.J. Mittemeijer, S. van der Zwaag: Acta Metall. Mater., 1993, vol. 29, pp. 1011–16

    CAS  Google Scholar 

  17. S.F. Dirnfeld, B.M. Korevaar, F. Van`t Spijker: Härterei-Technische Mitteilungen, 1975, vol. 30, pp. 197–203

    CAS  Google Scholar 

Download references

Acknowledgment

The authors thank the “Deutsche Forschungsgemeinschaft” for their financial support via projects C2 and A5 in the Collaborative Research Center 570 “Distortion Engineering.”

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Jérémy Epp.

Additional information

Manuscript submitted March 13, 2007.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Epp, J., Surm, H., Kessler, O. et al. In-Situ X-Ray Investigations and Computer Simulation during Continuous Heating of a Ball Bearing Steel. Metall Mater Trans A 38, 2371–2378 (2007). https://doi.org/10.1007/s11661-007-9314-3

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11661-007-9314-3

Keywords

Navigation