Abstract
Reactions of various phosphorylthioformic acid morpholides with hydrazine afford phosphorylthioformhydrazides. The latter react under mild conditions with N, N′-carbonyldiimidazole to form novel 5-phosphoryl-1,3,4(3H)-thiadiazol-2-ones.
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Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 11, pp. 2105–2107, November, 2019.
This work was financially supported by the Russian Science Foundation (project No. 18-73-00321).
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Kozlov, M.A., Volkova, Y.A. & Zavarzin, I.V. Synthesis of 5-phosphoryl-substituted 1,3,4(3H)-thiadiazolones. Russ Chem Bull 68, 2105–2107 (2019). https://doi.org/10.1007/s11172-019-2673-2
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DOI: https://doi.org/10.1007/s11172-019-2673-2