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High efficient synthesis of pyrimido[4,5-d]pyrimidines and adsorption of CO2 using a novel nanomaterial (MnCoFe2O4@ ovalbumin)

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Abstract

In this study, MnCoFe2O4@ovalbumin nanoparticles were synthesized using MnCoFe2O4 MNPs and egg white nano-ovalbumin. The surface of MnCoFe2O4 MNPs was activated with trisodium citrate anhydrou to improve the fabrication of nano-ovalbumin on MCF MNPs. The structure of these nanoparticles was properly characterized by Fourier-transform infrared spectroscopy (FT-IR), Scanning electron microscope, X-ray powder diffraction, Energy-dispersive X-ray spectroscopy, Transmission electron microscopy, Thermogravimetric, and Vibrating sample magnetometer. The catalytic activity of the MnCoFe2O4@ovalbumin nanoparticles was evaluated for the synthesis of pyrimido[4,5-d]pyrimidine derivatives via multi-component reaction of aldehyde, barbituric acid, urea, or thiourea under solvent-free condition. The desired products were prepared using an environmentally friendly method. Short reaction time, high efficiency, and easy work-up are some advantages of this procedure. This heterogeneous nanocatalyst can be easily recovered by a magnetic field and used at least six times without considerable loss of its activity. Also, MCF@OVL MNPs exhibited a CO2 adsorption capacity about 9.35 mmol/g at 25 °C.

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Acknowledgements

We gratefully acknowledge the financial support of this work by the research council of Arak University.

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All authors declare that no funds or other support were received during the preparation of this manuscript.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, Arak University, Arak, 38156-8-8349, Iran

    Akbar Mobinikhaledi, Najmieh Ahadi, Fatemeh Sadat Hoseini & Fatemeh Sameri

  2. Institute of Nanosciences and Nanotechnology, Arak University, Arak, 38156-88138, Iran

    Akbar Mobinikhaledi, Najmieh Ahadi & Fatemeh Sameri

Authors
  1. Akbar Mobinikhaledi
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  2. Najmieh Ahadi
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  3. Fatemeh Sadat Hoseini
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Design of proposal was performed by AM and NA. The experimental section was performed by FSH. Preparing of the manuscript and its editing were performed by AM, NA and FS.

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Correspondence to Akbar Mobinikhaledi.

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Mobinikhaledi, A., Ahadi, N., Hoseini, F.S. et al. High efficient synthesis of pyrimido[4,5-d]pyrimidines and adsorption of CO2 using a novel nanomaterial (MnCoFe2O4@ ovalbumin). Res Chem Intermed 49, 3501–3518 (2023). https://doi.org/10.1007/s11164-023-05042-2

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