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Effect of surfactants on phase, crystal growth and photocatalysis of calcium stannate synthesized by cyclic microwave and calcination combination

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Abstract

Calcium stannate (CaSnO3) was successfully synthesized in the solutions containing different surfactants by cyclic microwave and calcination combination. Phase, morphology and vibration mode were characterized by X-ray diffraction, field emission scanning electron microscopy and Fourier transform infrared spectroscopy. Growth mechanism of the products was also explained according to the analytical results. Their photocatalytic activities were tested through methylene blue (MB) degradation induced by UV radiation. In the MB solution with pH 6, the S-CTAB product showed the highest decolorization efficiency of 89.1% and the highest rate constant of 4.374 × 10−3 min−1.

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Acknowledgements

We wish to thank Chiang Mai Rajabhat University, and Prince of Songkla University, Thailand for providing financial support the research, and Center of Excellence in Materials Science and Technology, Chiang Mai University for financial support under the administration of the Materials Science Research Center, Faculty of Science, Chiang Mai University, Thailand.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science and Technology, Chiang Mai Rajabhat University, Chiang Mai, 50300, Thailand

    Patcharanan Junploy

  2. Department of Materials Science and Technology, Faculty of Science, Prince of Songkla University, Hat Yai, Songkhla, 90112, Thailand

    Anukorn Phuruangrat

  3. Department of Physics and Materials Science, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand

    Somchai Thongtem

  4. Department of Chemistry, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand

    Titipun Thongtem

  5. Materials Science Research Center, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand

    Titipun Thongtem

Authors
  1. Patcharanan Junploy
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  2. Anukorn Phuruangrat
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  3. Somchai Thongtem
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  4. Titipun Thongtem
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Correspondence to Patcharanan Junploy, Anukorn Phuruangrat or Titipun Thongtem.

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Junploy, P., Phuruangrat, A., Thongtem, S. et al. Effect of surfactants on phase, crystal growth and photocatalysis of calcium stannate synthesized by cyclic microwave and calcination combination. Res Chem Intermed 44, 5981–5993 (2018). https://doi.org/10.1007/s11164-018-3470-5

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  • DOI: https://doi.org/10.1007/s11164-018-3470-5

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